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FINAL REPORT (Project SR-99) onPart J: THE FUNDAMENTAL FACTORS INFLUENCING THE BEHAVIOR OF WELDED STRUCTURES UNDER CONDITIONS OF MULTIAXIAL STRESS AND VARIATIONS OF TEMPERATURE.
Part II: THE EFFECT OF SUBCRITICAL HEAT TREATMENT ON THE TRANSITION TEMPERATURE OF A LOW CARBON SHIP PLATE STEEL.
by
W. M. Baldwin, Jr., and E. B. Evans CASE INSTITUTE OF TECHNOLOGY
Transmitted through NATIONAL RESEARCH COUNCIL'S
COMMITTEE ON SHIP STEEL
Advisory to
SHIP STRUCTURE COMMITTEE
LAFORATORUM VOOR
SCHEEPSCONSTRUCÎES
Division of Engineering and Industrial Research
National Academy of Sciences . National Research Council
Washington, D. C. November 6, 1953 SERIAL NO. SSC-64
LA?.ORitT3RUM \IQOR
,-. .- ,- .',HLrLO1'.J
MEMBER AGENCIES: ADDRESS CORRESPONDENCE TO:
BUREAU OF SHIPS. DEPT. OF NAVY SECRETARY
MILITARY SEA TRANSPORTATION SERVICE, DEPT. OF NAVY SHIP STRUCTURE COMMITTEE
UNITED STATES COAST GUARO. TREA3URY DEPT. U. S. COAST GUARO HEADOUARTERS
MARITIME ADMINISTRATION. DEPT. CF COMMERCE WASHINGTON ss, D. C.
AMERICAN BUREAU OF SNIPPING November
6, l93
Dear Sir:
As part of its research program related to the improvement of hull structures of ships, the Ship Struc-ture Committee is sconsoring an investigation on the fundamental factors influencing the behavior of welded
structures under conditions of multiaxial stress and variations of temperature at the Case Institute of
Tech-nolocy. Herewith is a copy of the Final Report,
ssc-6L.,
of the investigation, entitled "Part I: The Fundamental Factors Influencing the Behavior of Welded Structures
under Conditions of Nultiaxial Stress. Part II: The
Effect of Subcritical Heat Treatment on the Transition Temperature of a Low Carbon Ship Plate Steel," by W. M.
Baldwin, Jr., and
E.
B. Evans.The project has been conducted with the advisory
assistance of the Corrirnittee on Ship Steel of the National
Academy of Sciences-National Research Council.
Any questions, comments, criticism or other matters
pertaining to the Report should be addressed to the
Secre-tary, Ship Structure Committee.
This Report is being distributed to those
indivi-duals and agencies associated with and interested in the work of the Ship Structure Committee.
Yours sincerely,
K. . COWART
Rear Admiral, TI. S. Coast G'uard Chairman, Ship Structure Committee
Final Report (Project SR-99)
on
Part I: The Fundamental Factors Influencing the Behavior of Welded Structures under Conditions of ìultiaxial Stress and Variations of Temperature.
Part II: The Effect of Subcritical Eeat Treatment on the
Transition Temperature of a Lo Carbon Ship Plate steel.
by
W. I. Baldwin, Jr.
E. B,
EvansCASE INSTITUTE OF TECIiNOLOGY
under
Department of the Navy
Bureau of Ships NObs
-BuShips Project No. NS-011-073
for
SHIP STRUCTURE COiITTEE
TABLE OF CONTENTS Page
Introduction . . . , . . . i
PART I: The Fundamental Factors Influencing the Be-havior of Welded Structures.
Selection of Eccentric Notch Tensile Test for
Evaluating the Effects of Welding . . . . 3
Studies with Eccentric Notch Tensile Specimen . 6
Steel Comparison (A and C Steels) 6
Preheat and Postheat 11
Specimen Size. . . , . . . , , 11
Inhomogeneity of Plate
13
Selected Locations in Weld Metal 13
Comparison with Concentric Notch and
tfnnotched Tensile Tests
15
Metallurgical Structures 17
Hardness Surveys 19
Temperature Measurements 21
Subcritical Heat Treatment (Preliminary Work) . 21
Part II: The Effect of Subcritical Heat Treatment on
the Transition Temperature of a Low Carbon
Ship Plate Steel.
Isothermal Studies. . . e 25 Air Cooled 25
FurnaceCooled.
...
27WaterQuenched..
...
27EffectofHeatingMedium....00C
29 Quench-Aging Studies. . . , 29 Microstructures . . o e o o s s . o e e o o 31CoolingRates
... ...
o. oc.
.3+
Interpretation of Results: Weidments and Subcritically Heat Treated Plate , e
36
Appendix A . o o o s e o o e e o o e o o o e o
.
Appendix B . e e
o s e s e s . s . e e s
Bibliography e . . . . .
-ii-LIST 0F FIGURES
No0 TITLE
L
Notch Properties as a Function of Strength Levelfor Various Steels (2)..
...
. . . 5Relations between Concentric and Eccentric Notch
Strength Ratios and Notch Ductility .
5'
Eccentric Notch Strength of the Unaffected Base
Plate as a Function of Testing Temperature. . 8
.
Eccentric Notch Strength of the Unaffected BasePlate as a Function of Testing Temperature. 8
Distribution of Eccentric Notch Strength at -60°F 9
Distribution of Eccentric Notch Strength at -70°F 9
70 Transition Curves of the Region of Lowest
Ductil-ity for Steels "A" and "C". . . , 10
8.
Variation of Transition Temperature with Distancefrom the Weld Centerline . . . 10
90 TransItion Curves of the Unaffected Base Plate of
Steel "C" for Three Welding Conditions. 0 0 12
100 Distribution of Eccentric Notch Strength of "C"
Steel at -80°F for Three Welding Conditions 12
11 Transition Curves of the Region of
Lowest
Ductil-ity for Three Welding Conditions0 . . 12
l2 Effect of Specimen Section Size on the
Distribu-tion of Eccentric Notch Strength at -70°F .
13. Distribution of Eccentric Notch Strength at -80°F 11+
1 Comparison of the Eccentric and Concentric Notch
Properties as a Function of Testing Temperature
Midthickness Tests of "A" Steel Base Plate0 16
15 Distribution of Concentric and Eccentric Notch
Properties at Various Low Temperatures--Mid-thickness tests of "A" Steel Weidments, (100°F
16e Regular Tensile Properties of "A" Steel as a
Function of Testing Temperature . . 18
17. Distribution of Hardness across Weld at Various
Positions Throughout the Thickness of the
Plate o e G O O O O O O e e e O G o a 20
l8 Distribution of Microhardness Values at the
Mid-thickness of 3/1+ Plate Weidments of Steels
t(ii
ja aLJ.L&,q 9A tn
co o o o o e 0 0 G O O G o e O O19 Maximum Temperatures Reached during elding for
Two Welding Conditions0 e e e 22
Heating and Cooling Curves in the Region of
Lowest Ductility for Two 6 Pass Weidments . 22
Heating and Cooling Curves in the Region of
Lowest Ductility for Two Welding Conditions 2+
22 Effect ol' Subcritical Heating and Cooling on
the Eccentric Notch Strength of Unaffected
ease Plate. . . O G G O o e a 2+
23 Eccentric Notch Tensile Transition Temperatures
of "C" Steel as a Function of Time at
Various Subcritical Temperatures. Air Cooled. 26
2+ Charpy V-Notch Transition Temperature as Func-tion of Time at Subcritical Temperatures0 Air Cooled0 Plate II o a o o o o o a o e
25' Transition Temperatures of "C" Steel as a
Func-tion of Time at Subcritical Temperatures.
Water Quenched and Aged One Month at Room
Temperature0 Plate II o o o o o
Transition Temperatures of "C" Steel Resulting
from Various Subcritical Heat Treatments in
Nitrate Salt Bath and in Air, Employing an
Air
Cool0
o Q a o o e o o a o e o Q O O Transition Temperatures of "C" Steel Resultingfrom Beating at 1100°F for Various Times in
Nitrate Salt Bath and in Air, Employing a
Water Quench0 Aged One Month at Room
Tempera-ture0 . , O O C O Q O t O O O O
26
28
30
TITLE PAGE
Effect of Room Temperature Aging Time on the
Transition Temperature and Hardness of "C" Steel after Water Quenching from Temperatures
Indicated. e o e e o e e O
32
Effect of Various Aging Times and Temperatures
on the Hardness of "C" Steel after Water
Quenching from
1300°F
e o o e e e32
30e
Summary Curves Showing Effect of Various Aging Temperatures and Times on the Transition Temperature and Hardness of "C" Steel.Specimens Water Quenched from 13000F before
Aginge o o o o e o e e e o e o e e e e
33
Solution and Room Temperature Aging Effects on the Hardness and Impact Properties of tic,,
Steele o e o e o o e o e e o o o s e
33
Comparison of Cooling Curves in
the Regionof
Lowest Ductility for Two Welding Conditions
with Those Obtained with Heat Treated Test
Specimens, e s
.
e o e e o e e o e O35
Al. Test Specimens. . o e o e e o s e
s e 1+2
A2,
Method of Loading to Obtain 1/1+ Inch Eccentricity. (Eccentricity and the Position of Fixturesare Exaggerated0). s s o e s o e o e s 1+3
A3. Plate Preparation
. . e o o o o o o e 1+3
A1+e Welding Procedure o e e e e
.
e e e o s s o o 1+3Location of Eccentric Notch Specimen at the
SurfaceLevel
e eoo o e. e soe.e
1+1+Location of LTnnotched and Notched Specimens
at the Midthickness of Weidment. . . 1+1+
A7e Preparation of Charpy V-Notch and Notch Tensile
This is the final report on a project sponsored by the
Ship Structure Committee under U. S. Navy Contract NObs-+5*7O
and summarizes the work done in the period from July 1, l97
to December 31, 1952. Five Technical Progress
covered the work completed under this contract.
Three progress were issued entitled, "The
Fundamental Factors Influencing the Behavior of Welded
Struc-tures under Conditions of Multiaxial Stress, and Variations of Temperature, Stress Concentration, and Rates of Strain", The major objectives were to determine the relative notch toughness of various zones in commercially welded ship plate steel and, if such zones could be isolated to determine the dependence of the notch behavior upon material, variations in
the welding process, and heat treatment. Eccentric notch
tensile tests at various low temperatures were used to
eval-uate the ductility of a small volume of metal from any
posi-tion in the weidment. A summary of the work toward these objectives is presented in Part I of this report.
Two progress reports'
were submitted under the title,s'The Effect of Subcritical Heat Treatment on the Transition
Temperature of a Low Carbon Ship Plate Steel", The nrincipal
objectives were to (1) give an insight into the basic
mech-anism which was responsible for the brittle zone found in the
-2-max±murn embrittlement possible in base plate by subcritical
heat treatment; and
(3)
suggest possible methods of minimizIng or eliminating this embrittlement in base plate which
may be applicable to weldments. This work is presented in
Part
The important findings of the two different phases of the investigation are integrated to show that the quench-aging mechanism appears to be responsible for the brittle
zone outside the weld area of low carbon ship plate weld
Selection of Eccentric Notch Tensile Test for
Evaluatg
Fffects of WeiJNumerous investigations have shown that steel structures
may fall in a brittle manner when subjected to certain service
conditions0 The conditions associated with brittle failure include multiaxial stresses, stress concentration, low
tempera-tures section size, and rate of loading.
A combination of these embrittling factors may reduce the
ductility to a low value0 The ductility then dictates a struc
tures resistance to failure rather than the strength, because
it is known that only a small amount of energy is required to
propogate a crack through a region of low ductility0
In view of the fact that the number of brittle failures in ships had increased with the adoption of welding techniques9 it was felt that the welding process altered the properties of the steel. Many investigations employing a number of different specimens have shown that the ductility of a weìdment Is lower
than the ductility of the steel of which the weidment is made.
In selecting a test for locating zones of lowered duc
tility in weldrnents, a specimen was needed which would con
stitute a very fine probe (these critical zones were expected
to be sniall) and still include some of the previously men
tioned embrittling factors, Such a test would serve to lower the ductility of the entire plate to such a point that the
critical regions could be located0
The eccentric notch tensile test met these requirements
±n that a very mal1 volume of metal controlled the reaction *
of the specimen the embrittling factors o± eccentric load
ing multiaxial stress, and a stress-raiser were present and
the factor of low temperature could be added0
This specimen was used in previous investigations to
differentiate among low alloy steels (heat treated to the same
strength levels) which were known to have different service
properties67
ifl Fig0
1 the properties of four steels werecompared. at room temperature by means of concentric and ec
centric notch tests0 The data used to draw these comparison
curves were obtained from
Fig0
2, a plot of notch strength**
ratio as a function of ductility0 The concentric notch
strength seemed to be dependent upon the ductility up to about
two per cent, whereas the eccentric notch strength extended
the dependence of the notch strength upon ductility up to ap
proximately ten per cent by the add±tion of another embrittlng factor, that of eccentric loading.
From
Fig0
1, it can be seen that the eccentrIc notch testwas able to detect differences in the four steels, and rate
them in the same order as the concentric notch test0 The
*The fiber at the notch bottom was subjected to the maximum
tensile stress, and was the fiber in which fracture initiated.
**Notch strength ratio is defined as the ratio between the notch strength and the tensile strength0
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-6-ductility of ship plate steel is too high to show up any regions of lowered ductility at room temperature, but with the added
embrittling factor of low temperature the eccentric notch tensile
test can be
expected to detect differences in the various zonesencountered in a weldment0
*
The specimen design is shown in Fg0 A-1 and the method
of conducting a test illustrated in Fige A20
Studies with EccentrIc Notch Tensile rnn
The ship steels selected for study were A arid C project
steels because they had been shown to have widely different
transition temperatures. although of the same approximate
composition0 The properties reported for these steels are
listed in Table
B-l0
Weidments were made of these steels atthe Battelle Memorial Institute under closely controlled
cori-ditioris0 The details of the plate preparation and welding
procedure are given in
Figs0
A-3 and A+, respectively9 and the welding data in Table B-20 All specimens were taken fromthe weidments as shown in Figs0
Â-5
and A-6 so that the long axis was perpendicular to the rolling direction0 About onemonth elasped between time of welding and testing0
The first tests were conducted on specimens from the mid thickness level of weidments of A and C steel made with 100°F
*The letter "A" or "B" preceding the number refers to the corresponding Appendix0
prehea.t and interpass temperature0 The transition temperature
ranges for the unaffected base plate (2 inches or more from the
weld centerline) are shown in Fig. 3 for C steel, and in Fig. +
for A steel0 The superior properties of A steel were evident in *
a lower transition temperature (_800F), as compared to -6°F for
C steel. The same relative rating was found in the
results of
other investigations.
For both steels the distribution of eccentric notch strength
at selected low temperatures and at various distances from the
weld centerline showed the presence of a minimum at 0.3-0»+ inch
from the weld centerline and a maximum in the vicinity of the
weld junction (0.l--0.2 inch from the weld centerline)0 The mini
mum and maximum positions can be seen in the distribution at '6O°F
for C steel and at -70°F for A steel in Figs. and 6, respectively.
A comparison of the average transition curves determined for the
position of minimum ductility for both
steels,
Fig. 7, showed that
the transition temperature for C steel (_200F) was about 20°F
higher than that for A steel (Li0oF),
More complete data on the C steel weldment showed that the weld metal and the location of the maximum (0.l-0.2 inch from the
weld centerline) did not go through a transition in the range of
testing temperatures which were used. However, the relation
be-tween transition temperature and distance from weld centerline can be represented as shown in Fig. 8. The zone of minimum ductility
was definitely defined by its high transition temperature.
*Traflsitjon temperature is here defined as the temperature at the vertical midpoint of the average notch strength curve
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Preheat and Postheat
In order to investigate the possible beneficial effects
of preheating and postheating, weidments of C steel were made
using a +00°F preheat and interpass temperature, and a
post-heat at 1100°F to a weldment made with 1000F prepost-heat0 A
comparison of the average transition curves for the unaffected
base plate, Fig0 9, showed that
Data for the 100°F and 1+00°F preheat fitted on the same curve0
The postheated plate had almost the same transition
temperature (-75°F) as the plates without postheat
(-65°F)
A. comparison of the distributions of notch strength across the welds determined at -80°F, Fig. 10, showed that the -i-00°F
preheat brought about adefinite improvement, and the 1100°F
postheat a virtual elimination of the region of minimum duc-tility0 The improvement was more clearly revealed in the
average transition curves for this region, Fig0 11. The
tran-sition temperature of -20°F for the 100°F preheat was shifted
to +°F by the +00°F preheat, and to -70°F by the postheat
treatment0
pjnen Size
A smaller specimen than the one used might be expected
to show up greater differences in notch strengths, because the
changes in notch strength were very rapid as the distance from the weld centerline was increased from zero to 0.5 inch.
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similar but with the area of the notched section one-half that
of the standard specimen) were taken from various locations
of the A steel weldment and tested at =70°F0 These results
superimposed on the results from standard specimens, Fig0 12, showed little difference. The small size then offered no
advantage over the standard specimen.
Inhomogene of Plate
To determine any differences due to gross inhomogeneity
of plate, tests were conducted on specimens taken from as
close as possible to the plate surface of a C steel weidment
made with 100°F preheat. The transition temperature of the
unaffected base plate (-60°F) was but 50F higher than that at
the rnidthickness. The distribution of notch strength at various
distances from the weld centerline for a testing temperature of
-80°F,
Fig0
13, showed the same general behavior as the midthickness tests, but the minimum was shifted approximately 0.1 inch further from the weld centerline. This shift was to be
expected due to the geometry of the double-V weld employed.
This same behavior would be expected for the A steel at the
surface level based on the similar behavior of A and C steels
at the midthickness0
Selected Locations in Weld Metal
In order to investigate further the possibility of zones of low ductility in the weld structure, a number of probe tests
200 160 20 80 40
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INTER-PASS TEMPERATURE
A
RANGE OF VALUES FOR PREVIOUS
RESULTS AT THE MIOTHICKNESS.
.
sPLATE SURFACE
0.5 .0 .5 2.0 2.5 3.0
DISTANCE FROM WELD CENTERLINE INCHES
FrG. 13 DISTRIBUTION OF ECCENTRIC NOTCH STRENGTH
T 80° F
'C STEEL
A0 The coarse structure at the weld junction from Pass 5°
B0 The coarse structure at the weld centerline approximately
003 inch from the plate surface0
C0 The coarse structure of Pass 2 at the weld centerline0
At these positions only high notch strength values were obtained,
which, in conjunction with the high values previously obtained
at the midthickness and surface levels, seemed to preclude the
existence of low ductility in the weld metal0
parison with Concentric Notch and Unnotched Tensile Tests
To confirm that the eccentric notch strength was a measure
of concentric notch ductility for ship plate steel as had been previously shown for low alloy steels (see
Figs0
i and 2), the results from a number of eccentric and concentric notch tensiletests from the midthickness level of the A steel weidment were compared0
In Fig0 l+ the notch properties of the unaffected base plate are shown as a function of the testing temperature0 The
concentric notch strength appeared to be dependent upon the
ductility up to a low value (say, two per cent)9 wheras the
eccentric notch s'trength extended the dependence of the notch strength up to approximately 12 per cent0 This was in good
agreement with the previous findings0
In
Fig0 15'
the distribution of notch properties at variousdistances from the weld centerline is shown as a function of
testing temperature0 The concentric notch ductility showed
z z o H 20 80 40 z 20 w lAi 5 I- Ui IO D4
I
O I- o z o 20 80 ECCENTRIC TESTS CONCENTRIC TESTS ONCENTRIC TESTS/7(
-o 40 -340 -260 -180 -lOO -20 TESTING TEMPERATURE°F FIG. 4COMPARISON OF THE ECCENTRIC AND NOTCH PROPERTIES AS A FUNCTION TEMPERATURE. MIDTHICKNESS TESTS BASE
PLATE.
w
60
140
CONCENTRIC OF TESTINC OF 'A" STEEL
120 o o o
I
H z W H (nI
O I- o z 40 20 Io o 20 80 H b' FIG. 5DISTRIBUTION OF CONCENTRIC AND ECCENTRIC NOTCH PROPERTIES AT VARIOUS LOW TEMPER- ATURES-MIDTHICKNESS TESTS OF
' STEEL
WELDMENTS, (P00°F PREHEAT AND INTERPASS TEMPE RAT U R E S)
- ---e--ECdENTRIC TESTS o -70°F -110°F le CONCENTRIC TESTS I 0-40°F s- 110° F CONCENTRIC 0 -40°F -110°F TESTS 2.5 0 05 .0 1.5 20 DISTANCE
centerline) in the saine manner as the eccentric notch strength,
whereas the concentric notch strength did not define this em
brittled zone.
Unnotched tensile tests were also made on the same weld
ment to determine whether this test could be made sufficiently
severe, by the use of very low temperatures, to detect ductility
variations in ship plate steel. For the unaffected base plate,
the tensile strength did not define a transition
range; the
re-duction in area did define this range but only at very low
temperatures, Fig. 16. The tensile properties at -110°F of the zero and 0.3 inch positions were about the same as those for the unaffected base plate at the same temperature. From this
limited data it appeared that the unnotched tensile test was
not sufficiently severe to detect ductility variations in welded
plate.
Metallur ical Structures
A metallographic study of the structural zones at the
mid-thickness level of the C steel weidment made with 100°F
preheat revealed that the weld junction was defined by a sudden large change in grain size at 0.08 inch from the weld centerline.
With increasing distance from the weld centerline,
the
grain size of this structure which was cooled from
above the upper critical decreased0 The structure resulting from trans-formation from the temperature
range between the up-oer and lower
160 40 20 00 80 60 UJ -J :;5 40
z
LU H 20 o 70 60 50 40 30 20 Io o-34°
18-TESTING TEMPERATLIRE-FFIG. 16:
REGULAR TENSILE PROPERTIES OF
'' STEEL
AS A FUNCTION OF TESTING TEMPERATURE.
-
000 FAATURE
STEEL WELDMENT
PREHEAT AND INTERPASS
MIDTH!CKNESS TESTS.
TEMPER-OO,Q
Xt.:
8 UNAFFECTED X 0.0 INCH D 0,35 INCH BASE PLATE FROM WELD FROM WELD CENTERLINE CENTERLINE r-X o___________
g 40-20
60 -180 -lOO -26003 inch from the weld centerline0 There seemed to be no dif
ference in structure between that of the critical zone (0.3-0»+ inch from the weld centerline) and that of the parent plate when examined at either 100 or 2000 magnifications0 The structures
of the 0.3 inch position for the C steel which were pre and
post-heated, respectively, also appeared to be the same as the unaf
fected base plate0
Hardness Survey
Rockwell B hardness distributions were first made at several
levels of a C steel weldment with 100°F preheat,
Fig0
17. Themaximum hardness at the midthlckness level (Rß89) occurred at the
weld junction and was associated with a maximum ductility,
whereas
a lower hardness (RB83) was found at the zone of minimum ductility0
To obtain the hardness distribution at more closely
spaced intervals, microhardness tests were conducted across all the welds at the center of the plates, Fig. 18. A number of hardness peaks
were found, the highest one being at the weld junction.
The other peaks were due to the composite heat affected zone caused by the six weld passes0 For the C steel weldrnents, the overall
level of the distribution was decreased, in order, with
increas-Ing preheat and with postheat. The decrease in hardness
in the
zone of minimum ductility (0.30.1+ inch from the weld
center-line) appeared to correlate with the decrease in transition temperature in this zone brought about by the pre and postheat treatmentS0
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47 -;5'-,+7'Z'..W/C)4'/Jr 0/ -'--1 J72-W»-.-'ZJ' :7_.___J>2'j
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--*
. ¡-._../ 1 I.. .1._
.-IA/d C "-"9/i9 /,VC,y ¿'.-/7I/2.'IIWT 1 1-,
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If
/
i t I ---I I-to that of the C steel with 100°F preheat, but the peaks were
lower and the overall curve was lower0
Temperature Measurements
The results of the temperature measurements made during
the welding of the C steel (at the midthickness level) are
given in Figs0 19, 20, and 21. In Fig0 19, the maximum
tempera-tures reached during the welding process are shown as a function of the distance from the weld centerline for the weidments with 100°F and +0O°F preheat respectively. In the region of low
ductility (0.30.+ inch from the weld centerline) the tempera
ture evidently never reached the lower critical temperature (Ac1) for either weidment.
In Fig. 20, the complete heating and cooling history is given for both welding conditions. A comparison of the
heat-Ing and cooling cycles for the first pass for the two welding
conditions, Fig. 21, showed that the 100°F preheat weldment had
a faster cooling rate. This difference can be shown for all the weld passes.
Subcritical Heat Treatment (Preliminary Work)
An attempt was made to duplicate the embrittlement in the
region of low ductility by means of subcritical heat treatment of base plate of C steel. Specimen blanks were cooled from
9500F
to give three different cooling rates-air cool, oil quench, and water quench. The notch strengths determined at&4
.'
ç
-j'
W íZ'
__f,lJP f
Vó/?'&
<P,_- -ç#4,_ ,l_,
ri,'
-, ,1J,J. ' -7.22-Z'24'- 7? AfeW flÇ''
-i
442
L
-2ó 2-'»6
-l' ¿--'
__-__'7_--
;6-6' 6-lJ'.P
71'-J 4 o o L of4rp
1_'_ - ---8O0F for all three cooling rates were low, and when compared
to the spread of values for the base plate at 8O0F, Fige, 22
it was seen that the material was substantially embrittied by
this heating and cooling0
PART II THE EFFECT OF SUBCRITICAL HEAT TREATMENT ON THE TRANSITION TEMPERATURE OF A LOW CARBON SHIP PLATE
ST EEL0
The detection of a brittle zone in ship plate weldments
in a region which was not heated above the lower critical
temperature, and the preliminary work which showed that base
plate could be embrittled by subcritical heating and cooling
led to an intensive study of the embrittlement of base plate
by subcritical heat treatment0 The effects of the following
factors were studied isothermal solution time and
tempera-ture, cooling rate, and aging time and temperature0
The embrittlement was evaluated by means Of the eccentric
notch tensile test, and also because it has such a wide degree
of acceptance as a standard, by means of the Charpy V-notch
test0 This work was supplemented by ha?dness tests and
microscopic examinations0
The studies were carried out with C steel because it
was felt that its inferior as-received properties portended
a higher degree of embrittlement0 The test specimens were
prepared from the base plate as shown in
Fig0
A-70 Unless otherwise noted, all testing was done one month after heat'9g
9
-'9
¿2f
c& 5
4g::7/tf .'2''9
-f-?Jt/'- .-, -
,Ç/-I.#'
3Pf
'-'5z
,_9cff
- - - -- - -. 4 - A -Ç-& 2/. 414%?df
7»-¿:72df
_-'_7_.--'9
2%
- - u','2 -' 4J.6 -4,*C2/ / /
4«// / /4.f4d /4
J///' J2
40' - ,',y_4_ --- -- 4?-
'Wz
--7& 2-'9 -l'
W-'9.
treating in order to maintain approximately the same aging
interval as used in the weidment study.
Isothermal Studies
Prior to determining the effects of time and
tempera-ture, a check was made on the within-heat variation in
transi-tion properties of the two different la?ge plates which supplIed notch tensile specimens0 The transition temperature of Plate
I (-6°F) used in the earlier work on weidments was lower than
that of Plate II (+00F). Due to this appreciable difference,
the results obtained with subcritically heat treated plate have
*
been separated as to plate number
Air Cooled
The relationship between notch tensile transition tempera-ture and time at various temperatempera-tures in the 700°--1200°F range
is plotted in Fig. 23. With the properties of the as-received
plate as a basis of comparison, the magnitude of the maximum
embrittlement appeared to be independent of the temperature,
amounting to a 10°F increase In transition temperature for Plate
II and a 25°F increase for Plate I. Time at temperature had
lIttle effect, other than an improvement in properties at very
long times due to a slightly spheroidized structure0
In Fig. 21, the transition temperature--isothermal time relationship for impact specimens heated at 11000 and l2OO°F
u-
I
-50 -70 -Io -3011
-50 o - Io -30.
-50 -70 -Io-30--.
50f-70L
o PLATEI
o PLATE I AS RECEIVED 0.I-o
800°F 950°F 1100°F 1200° F.
I0 looISOTHERMAL TIME'-) HOURS
1000
FIG.23: ECCENTRIC NOTCH TENSILE TRANSITION
TEM-PERATURES OF "C" STEEL AS A FUNCTION OF TIME AT VARIOUS SUBCRITICAL TEMTEM-PERATURES. AIR COOLED.
u- o 160_\ 140 Cr
u
criû-20-u
LUZo
1 80
W Z ct % 01200°F .1100°F RECEIVED ,-AS Ç--
--4----01 I IO lOO 000ISOTHERMAL TIME- HOURS
FIG. 24: Ct-IARPY V-NOTCH
TRANSITION TEMPERATURE
AS A FUNCTION OF
TIME
AT SUBCRITICAL
TEMPERATURES. AIR COOLED.
indicated no embrittlement at the shorter times; however, at * the longer times a slowly increasing ernbrlttlement was evident accompanied by a gradual softening0
Furnace Cooled
Spot checks with impact specimens indicated that no sig
nificant difference in transition properties can be expected
from specimens comparably heat treated and air cooled0 Although
no checks were made with notch tensile specimens, it is believed
that a furnace cool would result in no embrittlement because the
cooling rate would be less than the critical necessary to intro duce quench-aging effects0
Water Quenched
The transition temperature-time curves for notch tensile
specimens quenched from ll00F and 1200°F and aged one month
at room temperature, Fig0 25, were displaced to much higher transi-tion temperature than the comparable air cooled curves,
indicat-ing a severe embrittlement, and with the magnitude of the embrit=
tlement amounted to about a 500F increase in transition tempera
ture above that of the as-received plate; and for the 1200°F
series, an average of about 100°F increase in transition
tempera-ture0
With impact specimens, Fig0 25, the transition temperature
*It should be recalled that although embrittlement was
indicated by three different criteria, the upper level of "energy
absorbed" was raised, indicating an improvement in properties at
'Io
u-o LiJ90
CrD
70u
HO-
50uJ
30 Io cf)z
F-220 os 200D
r
180w
-û-160I-U..Z
140LO°
H
(1) 120z
F--30---4---
- ±
-AS RECEIVED-50
L Io,
o-28-ECCENTRIC NOTCH TENSILE
2. o CHARPY V-NOTCH i
4-o 1100°F 1100°F -40
o AS RECEIVED ç I 0.1 I IO lOO 1000ISOTHERMAL TIME'-HOURS
FIG.25: TRANSITION TEMPERATURES
OF "C" STEEL AS
A FUNCTION OF TIME AT
SUBCRITICAL
TEMPER-ATURES. WATER QUENCHED
AND AGED ONE
25°F
and the 1200°F series about55°F
above their respective air cooled curves.Effect of Heat in Medium
In the first stages of this investigation, both air and
a nitrate salt bath were used as the heating medium0 It was
noticed that, generally, test specimens heated in salt had higher transition temperatures and hardnesses than specimens
similarly treated in air0 This anomalous behavior was revealed
in both the Charpy V-notch and eccentric notch tensile data0
Both the impact and notch tensile transition temperatures
revealed that the magnitude of embrittlement accompanying an
air cool from the salt heat treatments was increased with
temperature, and time at temperature, as evident in the corn
parison with the results obtained after heat treating in air,
Fig. 26. The impact data also revealed that the embrittlement
increased with an increase in cooling rate, Fig0 27
Metallographic examination9 chemical analyses, and Xrays
showed the embrittling agent to be nitrogen, introduced by dif
fusion into the specimens through a scaling reaction of the
metal with the salt0
flçAin Studies
In order to determine the room temperature aging effects,
impact specimens were tested after various aging times after
u) IL o uJ I-200 180 160 40 20 80L4 20 00 80 60 40 20 o -20 -40 -60 -80
/
S RECEIVED VA CHARPY V-NOTCH I,/
/
II00E-AIRiiiiiiui:iiiiii
.700°F-320 280 240 200 60 th -J 120 u- LO 80-lt
V-NOTCH/
/
I,
J-
I
/
/
/
/
yJ
AIR XAS RECEIVED I J' ECCENTRIC j ¡ NOTCH TENSILE I I"y
/
/
'I
¿I
IA
A..)4//i
0/
/
/
#1
'y/
./
---950°F AIR k..1, "AS RECEIVED 1100°F AIR o 0.1 lO lOO 000ISOTHERMAL TIME AT IIOO°Fç-HOURS
FIG.27: TRANSITION TEMPERATURES OF "C" STEEL
RESULT-ING FROM HEATRESULT-ING AT 1100°F FOR, VARIOUS TIMES IN NITRATE SALT BATH AND IN
AIR, EMPLOYING
A WATER QUENCH. AGED ONE MONTH AT ROOM TEMPERATURE.
0.1
IO
lOO
000
ISOTHERMAL TIME HOURS
FIG. 26. TRANSITION TEMPERATURES OF
'G' STEEL RESULTING
FROM VARIOUS SUBCRITICAL HEAT TREATMENTS
IN
NITRATE SALT BATH AND IN
AIR,
EMPLOYING AN
temperature and hardness increased with increasing solution
temperature and with increasing aging time, reaching a
maxi-mum level, Fig. 28G
To determine the maximum embrittlernent due to
quench-aging, and how to minimize it, hardness tests were first made
after water quenching from 1300°F and aging for various periods
of time in the 35° to 1100°F range, Fig. 29. The peak hardness
reached and the time to attain this peak decreased with increas-ing agincreas-ing temperature. Similar changes were observed with the
impact transition temperature, Fig. 30, when employing aging
temperatures from room temperature to 600°F.
To obtain a quantitative measure of the solid solution
and aging effects as a function of solution temperature from
room temperature to 1300°F, Fig, 31 was prepared. Below
solu-tion temperatures of 650°F, the quench-aging effects were
absent, but then increased with increasing solution
tempera-ture0 The maximum embrittlement induced in C steel by the
quench-aging mechanism amounted to a 90°F increase in impact
transition temperature and 25 points increase in Rockwell B
hardness.
Nicrostructures
To afford a possible explanation of the embrittlement
obtained during subcritical heat treatment, numerous structures were examined at 2000X0 All specimens which were air or furnace
cooled showed no difference in structure from that of the as-re-ceived plate except a slight spheroidization which set in at
200 90 80 mOE 150 Li 140 130
t
20 U) z OE IO I-lOO 90 80 loo 95 90 85 80 75 70 65 60 AS RECEIVED CHARPY V-NOTCH 1300°F 0°°/
200°F 105 loo 95 90 65 25°F -_._ 200°F -_ 250°F AS QUENCHED FROM 300°F--u
- 600°F -900 °F>( .
m ° 85 -I -J W 80 o 75 > --;---1100°F AS- RECEIVED COOLED FROM 1300° F)
-: /
It -' o 35°F 80°F 350°F ALL SPECIMENS AIR COOLED FROM AGING TEMPERATURE/
1300°F -1200°F 0°D o <.-__-AS RECEIVED _AA o 0I Io 00 000 0,000LOG AGING TIME ---' HOURS
FIG. 28:
EFFECT OF ROOM TEMPERATURE AGING TIME
ON THE TRANSITION TEMPERATURE AND HARDNESS OF C STEEL AFTER WATER QUENCHING FROM TEMPERATURES
INDICATED. 0 0.1 IO lOO 1000 10,000
LOG AGING TIME-"HOURS
FIG. 29: EFFECT OF VARIOUS AGING TIMES AND TEMPERATURES ON THE
u- Ui
I-.4
W I.-2
w I-'I) z o I- u, z 4 1°-200 -h CHARPY V-NOTCH 125F----_. 190 - 180 170 60 150 140 130 20 'Io 100 90OR AIR COOLED FROM 1300°F
80 lOO 95 25°F--350°F AS QUENGED
o
::
r AS RECEIVED 70><.--AIR COOLED FROM 1300°F 65 60 00 80°F 80°FFIG. 301 SUMMARY CURVES SHOWING EFFECT OF
VARIOUS
AGING TEMPERATURES AND TIMES ON THE
TRANSITION TEMPERATURE AND HARDNESS OF "C' STEEL. SPECIMENS WATER QUENCHED FROM 1300°F BEFORE AGING.
-Jo: loo 95 90 85 80 75 70 65 190 180 u-170 .-150 ¿ 140 130 120 l'o 100 90 80 AS RECEIVED
/H0
AS RECEIVED HARDNESS o AIR COOLED O AS QUENCHED I WATER)(QUENCHED AND AGED AT ROOM TEMPERATURE FOR ONE MONTH.
CHARPY V-NOTCH AG IN EFFECT0
'
SOLID 1"SOLUTION, ///, EFFECTS .1//
'/, /, AGING\ EFFECT L--0.1 IO lOO 1000 10,000 0 200 400 600 800 1000 1200 LOG AGING TIME -'H0URS SOLUTION TEMPERATURE -'--j FIG. 31: SOLUTIONAND ROOM TEMPERATURE
AGING
EFFECTS
ON
THE
HARDNESS AND IMPACT
PROPERTIES
OF "C" STEEL.
the longer times at the higher temperatures0 No difference
in microstructure from that of the base plate was detected
In the series water quenched from either 1100° or 1200°F and
aged at room temperature, again with the exception of
spheroi-dization setting In at the longer times0 The first indication
that a precipitation reaction was operative was obtained in a
series aged at 1+00°F after water quenching from 1200°F, which
showed a general precipitation throughout the ferite grains0 A study of the structures after quenching from 1300°F and aging at various temperatures for various times, indicated
that the precipitation from the supersaturated solution was a
two-stage process0 At low aging temperatures the precipitate
was detected as a mottling of the ferrite grains; at the
higher aging temperatures, where an 'overaged' condition was
rapidly reached, the precipitate had grown so as to be resolvable,
2Q
The results of the temperature measurements made during the cooling of subcritically heated test specimens from 1200°F
are shown in
Fig0
32, in comparison with the cooling curvesassociated with the zone of minimum ductility for the first
weld pass for the two welding conditions0 With an air cool the
impact specimens cooled at a slightly slower rate than the notch tensile specimens due to the larger mass of metals but at a rate which was still slower than that obtained in the +00°F preheat
weldment0 Although the 100°F preheat weldment had a faster
1400 1200 800 600 400 200
\
'D
LEGEND
WELDME NT TEST SPECIMENS(0.3 INCH FROM WELD )
A.... FURNACE COOLED
B... .AIR COOLED (IMPACT) E.. ..400°F PREHEAT & INTER-C....AIR COOLED (NOTCH TENSILE) PASS TEMP., iST WELD PASS. D....WATER QUENCHED F.... 100°F PREHEAT & INTER- I
PASS TEMP., IST WELD PASS
15 30 45
TIME'- SECONDS
60 75 90
FIG. 32: COMPARISON OF COOLING CURVES IN THE REGION
OF LOWEST DUCTILITY FOR TWO WELDING
CONDI-TIONS WITH THOSE OBTAINED WITH HEAT TREATED
TEST SPECIMENS.
1000
-36-both these welding conditions were intermediate to the air cooled
and water quenched test specimens0
INTPP1ETATION OF RESULTS
In the weidment s.tudy the variations in ductility across
the weld area were represented by the distribution of notch
tensile transition temperature,
Fig0
8 It was believed thatthe maximum ductility observed near the weld junction was associated with a tempered martensitic structure, whose
duc-tility was higher than that of pearlite0
The location of the ductility minimum corresponded to a region which was not heated above the lower critical temperature, which, coupled with a relatively fast cool, pointed to embrit-tiement by the subcritical precipitation of carbide from ferrite
(quench-aging)0 That this mechanism was operative appeared to
be corroborated by the beneficial effects of higher preheat and
of postheat treatments The improvement of the ductility in this
critical region with higher preheat was attributed to a slower cool, allowing less solid solution and subsequent aging pcst heat effects, while the virtual elimination of embrittlemert
by postheat was believed due to
overagigt0
Due to a difference in the general types of microstructure across the weld area, the hardness could not be used as a
meas-ure of ductility0 The peak in hardness was associated with the
maxImum notch strength at the weld junction, but the minimum in notch strength occurred in a subcritically heated region, where
the hardness was leveling off0 However, considering the critical
region which had the same general type of microstructure, the
hardness appeared to be correlated with the ductility, 10e0, a
higher hardness signified a higher transition temperature0
From the complexity of the time, temperature, cooling rate
conditions ir a multi-pass weidment, it was impossible to deter=
mine the exact quench-aging cycle experienced in the critical
region0 It was believed that each weld pass contributed to the solid solutIon and aging effects, but that the first few weld
passes controlled the amount of carbon initially retained in
solution, while the following passes served mainly as short accelerated aging treatments0
In the subcritical work, the investigation of the effects of solution time and temperature, cooling rate, and aging time
and temperature revealed significant changes in ductility,
hard-ness, and microstructure0 These changes were largely
reconciled with the quench-aging mechanism0
The isothermal studies showed that no appreciable varia
tion in ductilIty can be expected by varying the time at tem= perature with the exception that at long times at the higher
subcritical temperatures softening set in due to slight spheroI
dization0 This stability with time indicated that the critical
region in weldments was not the result of decay of
an unstable
condition0
Air cooling or furnace cooling from subcritical tempera=
-38-.
enibrittlement that was obtained by air cooling notch tensile
specimens was about the same as that found in the critical
region of the C steel weidment made with +000F preheat, and a
was shown in FIg0 32, the cooling rates were about the same0
WIth an air or furnace cool, it was reasoned that the degree of supersaturation was low or nIl due to the fact that pre-clpitation occurred largely during cooling; consequently, no apprecIable change in ductility was realized on subsequent
aging0
A consideration of the quench-aging results showed that the degree of embrittlement was influenced by the subcrItical
temperature and the aging time and temperature0 The solubility
of carbon in ferrite increased with increasing solution tempera-turo, resulting in a greater 'as-quenched' hardness, andy ap-parently, a greater initial transition temperature due to the
higher degree of supersaturation0 Upon subsequent room
tempera-ture aging, the magnitude of the peak embrittleinent reached also
increased9 the higher was the solution temperature,
Fig0
28ThIs WaS in line with other quench-aging systems which showed
that a greater change in properties can be expected with in
creasing solution temperature0
With accelerated aging, the changes in transition
tempera-ture and hardness,
Figs0
29 and 30, revealed characteristicaging curves, 10e0, the maximum embrittlement attained and the time to reach this maximum decreased with increasing aging
FTCm trie metalioraphic changes that occurred during aging,
it appeared that a twostage precipitation reaction was opera=
tiVeo
The first stage (evident as a mottling of the ferrite)was responsible for the greater degree of embrittlement9 while
the second stage in which a resolvable precipitate was detected9
was associated with an improvement in properties corresponding
to a rapid Uoveraged condItion0 No attempt at identification
of the precipitate was made however., the sequence of changes
appeared to be the same as reported in a recent paper (8) The
first stage was identified as the hexagonal g-iron
carbde while
the second stage overlapped the first and was associated with a
Ttharge in the crystal lattice to cementite (orthorhombic Fe1C)0
insofar as microstructural changes were concerned9 the
brittle zone found in the suberitically heated region in weld
merits was not identified with a precipitation reaction0 It
was speculated that because the cooling rate In this region was
such that the ferrite was riot supersaturated to the maximum pos
sible as in water quenched test specimens9 less carbon was avail
able for th subsequent aging reaction and the resulting small amount of precipitation was not detected0
In regard to the changes in transition temperature arid hardness the results of the subcritical work gave the maximum
embrittiemerit. possible y quenchaginge Any treatment designed to remoue those effects in base plate should be applicable to the suberitically embrittled region of weldments OveragIng cr
postheating treatments at about 6500F would minimize the embrittle
improvement if a slow cool were employed; however, another quench-aging cycle could be initiated upon fast cooling from
A 7/16-20 TMDS
f
/2II
0.300"00408
,
600A. R 0.001CONCENTRIC NOTCH TENSILE SPECIMEN
l-l/2'
1/I6'"40
t-l/2
-1/16UNNOTCHED
TENSILE SPECIMEN
I / 6" I-1/2" -1/16"
ECCENTRIC NOTCH TENSILE SPECIMEN
FIG. AI: TEST SPECIMENS
LII4E
or
TEr4SON ORCL /4' ECENTRICITY 0.030 60° 5/16,4 d(-.- 3/8" »'--3/ 8 5/ l6 -1/2".-l/4--.
4-- I / 2
ADAPTERS LEFT HAND THREAD FIBER IN MAXIMUM TENSION TENSION TENSION NOTCH SPECIMEN
FIG. A2 METHOD OF LOADING TO OBTAIN
1/4
INCH
ECCENFRICITY.
(ECCENTRICItY AND THE
POSITION OF FIXTURES ARE EXAGGERATED.)
EDGES MACHINE-BEVELED
FIG. A3:
PLATE PREPARATiON
ELECTRODE - 3/16' EGOIO PASSES PASSES
FIG. A4 :
¶ q
REFERENCE SURFACE
FIG. 1x5
:
LOCATION OF ECCENTRIC NOTCH
SPECIMEN AT THE SURFACE LEVEL REFERENCE
SURFACE
FIG. 1x6
LOCATION OF UNNOTCHED AND NOTCHED SPECIMENS AT THE MIDTHICKNESS OF WELDMENT
ROLLING DIRECTION
HEAT TREAT
FIG 1x7
PREPARATION OF CHARPY V-NOTCH AND NOTCH TENSILE SPECIMENS FROM
hOu STEEL PLATE. CENTERLINE OF HEAT AFFECTED CENTERLINE OF PLATE SPECIMENS ZONE
AND FIBER IN MAXIMUM TENSION ON ECCENTRIC
C Steel
A Steel Yield Point P si39,000
37,950
-+6--TABLE B-1
Properties of
Aand
CSteel Plate*
Chemica1 Composition .
a
han1cal ProDertles Tensile StrengthP si
67,o0
59,910Noteg Both steels were semi-killed, 3/-f" plate in the as-rolled condition.
*Technical Progress Report of the
Ship
Structure Committee,Welding Journal, Vol. 13 (July, 198), p. 377s.38+s.
Elongation er Cent
25.5
(8t1 gage)
33°5
(2
gage)
C Steel 02+
O.8
0.012
0.026
0.05
0.016
0.02
A Steel 0.26
0»5O0.012
0.039
0.03
0.012
0.02
i
C Steel 003
0.03
0Q005
0.003
0.009
0.02
0.01
A Steel 0.03 0.03 0.006 0.003o.00+
0.02 0.01Wat
Harnischfeger
D0 C0 Welder
E1ectrode
3/16
E6010
Reversed Polarity
Current
150 amps
Pass i
160 amps
Passes 2-6
Voltage
25 voits
Passes l-6
W9lding Speed
36 in/min0
Pass i
+8 1r/:iin0
Passes 2-6
Electrode
Btirn Off Rate
85 in/min0
Passes 1-6
BIBLIOGRAPHY
l "The Fundamental Factors Influencing the Behavior of
Welded Structures under Conditions of Multiaxial Stress, and Variations of Temperature, Stress Concentration, and
Rates of Strain", by G0 Sachs,
L0 J0
Ebert, and A0 W0Dana, First Progress Report, Ship Structure Committee, Serial Number SSC2+, 10 May l91+9
2 "The Fundamental Factors Influencing the Behavior of
Welded Structures under Conditions of Multiaxial Stress,
and Variations of Temperature9 Stress Concentration,
and Rates of Strain", by
L0 J0
Klingler,L0 J0
Ebertand W0 M0 Baldwin
Jr09
Second Progress Report, Ship Structure Committee1 Serial Number SSC-3+, 28 November l9+93 "The Fundamental Factors Influencing the Behavior of Welded Structures under Conditions of Multiaxial Stress,
and Variations of Temperaturefl, by E0 B0 Evans and L0
J0
Iüingler Third Progress Report, Ship Structure Committee, Serial Number SSC-5.+9 1+ Octoberl952
"The Effect of Subcritical Heat Treatment on the
Transi-tion Temperature of a Low Carbon Ship Plate Steel", by
L
B0 Evans andL0 J0
Klingler, Fourth Progress Report, Ship Structure Committee, Serial Number SSC-60,30 October 193
5 "The Effect of Subcritical Heat Treatment on the
Transi-tion Temperature of a Low Carbon Ship Plate Steel", by
E0 B0
Evans andD0 J0
Garibotti, Fourth Progress Report, Ship Structure CommIttee, Serial Number SSC-6l,30 October
i953
6 "Comparison of Various Structural Alloy Steels by Means of the Static Notch-Bar Tensile Test" by G0 Sachs, L0 J0 Ebert, and W0 F0 Brown9
Jr0
Trans0 Am0 Inst0 Mining andMet0
Engr0,
Vol0 171 (19-7L Po 6o562l
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