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Material testing CTOD.tests on: Local pipe specimens, material: API.5L.X60

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SHIP STRUCTURES LABORATORY.

REPORT N°,

SSL 334

DATE: 20 FEBRUARY 1991

PROJECT: SC 90.02

MATERIAL TESTING

CTOD.TESTS ON:

local pipe specimens

material: API.SL.X60

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i CONTENTS page i. Introduction. i

Material and specimens; i

Precracking and bend tests. i

Results. 2

a. Tables. 3

b. Recordings. 9

(3)

INTRODUCTION

This report gives the CTOD-values for six series of three specimens tested at -10°C in accordance with ES 5762:1979. The tests have been carried out on request of the Apparaten- en Ketelfabriek AKF EV in Goes on behalf of AKF-order no. 31706/7.

MATERIAL AND SPECIMENS

According to the information from AKF the specimens are taken from

bended pipe material.

Material API 51 * 60. Yield strength (0.5%) 413-550 N/mm2. Form Heat no. Specimens: series 6: series 16: series 26: series 27: series 34: series 35:

3.. PRECRACKINC AND BEND TESTS

The specimens are supplied by Nieuwstraten Proefstaven EV in Poeldij k.

Specimens size: B 25 mm. W 25 mm.

Machined notch 5 mm.

Precracking and bend tests have been carried out in 3-point bending, in accordance to ES 5762:1979.

A 100 kN load-controlled servo-hydraulic testing machine has been

used forthe realisation of the fatigue precracking under constant

amplitude loading at room temperature. In order to expedite crack

initiation, the last two specimens (35.2 and 35.3) have been fatigued under a fatigue pre-cracking force Pf which has been

reduced as the crack front progressed. Besides, preceding to the

fatigue loading one load cycle of the same magnitude and of opposite sign has been applied.

The CTOD-tests have been carried out in a 350 kN load-controlled servo-hydraulic testing machine with a cryogene box.

Ø 773.8 mm * 29.5 mm. Radius 2286 mm. 532718.

place of sampling:

external axis - straight pipe

external axis - bend area

weld axis line straight pipe

weld axis line straight pipe

weld axis line bend area

weld axis line bend area

transverse base metal transverse base metal - transverse weld metal - transverse weld H.A.Z. - transverse weld metal - transverse weld H.A.Z.

(4)

Cooling and stabilisation on the test temperature is obtained by accurately controlled liquid nitrogen injection through a solinoid

valve. Via a ducting system the nitrogen is distributed

homogeneously in the cryogene box, without influencing the measuring devices.

The temperature is measured using thermocouples in contact with the test piece surface at the crack tip location in front and at the back side of the test piece.

The test temperature for all specimens has been -10°C. The tests were started at a temperature of about 1°C below the test

temperature. Depending on the amount of plastic deformation the measured temperatures rose to a value of -10°C ± 0.5°C at the moment of failure.

The COD's have been measured with a MTS clip gauge, type

632.020-20, serial no. 675. The calibration values over ranges of 0.5 and 2.6 mm are given in the tables and graphs on page 27.

4. RESULTS

The results are presented in the tables and graphs on page 3 up to 26. From the recording of specimens 34.1 it can be noted that the testing has been interrupted due to a fall out of the loading equipment. The interruption is considered to be of no influence on the result and validity of the test.

All tests are valid according to BS 5762:1979.

DELFI UNIVERSITY OF TECHNOLOGY

Department of Mechanical Engineering and Marine Technology Ship Structures Laboratory

2

OELFT U

i1fiii

F TECHNOL

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3

DELF UNIVERSITY OF TECHNOLOGY SHIP STRUCTURES LABORATORY

FRACTURE MECHANICS TEST (CTOD-test) cf. BS-5762-1979

PROJECT SC 90 02 Date: 20 febr 91

CLIENT: Apparaten en Ketelfabriek A.K.F. BV - Goes

Specimen data

Specimen nr 52761 52762 52763

W (height) (mm) 26.50 26.60 26.60

B (thickness) (nun) 26.60 26.50 26.50

Fatique precracking data 3 point bending

Testing machine (kN) 100 100 100 Test temperature (°C) 20 20 20 Span (mm) lOO 100 100 Loading (kN) 24.0 24.0 24.0 R (stress ratio) 0.1 0.1 0.1 Kf (Nmm-3/2) 1073 1044 1037

Number of cycles (*10A3) 44.44 41.40 41.00

aO (mm) 8.0 7.7 7.4 a4 (nun) 7.3 7.4 7.4 al (nun) 8.5 8.6 8.4 a2 (mm) 8.6 8.5 8.3 a3 (mm) 8.8 8.1 8.3 a average / W 0.33 0.32 0.31

COD-test data 3 point bending

Testing machine (kN) 350 350 350 Test temperature (°C) -10 -10 -10 Span (mm) 102 102 102 dK/dt (N mm-3/2 s-1) 55.5 54.3 54.2 Vi (mm) Vc (mm) Vu (mm) Vmax (mm) 3.240 3.690 3.330 Pl (kM) Pc (kN) Pu (kN) Pmax (kM) 76.8 81.3 80.5 Calculated results CTODi (nun) CTODc (mm) CTODu (mm) CTODmax (mm) 1.532 1.782 1.623

Yield strength used in calculations: 413 N/mm2

(6)

4

DELFT UNIVERSITY OF TECHNOLOGY SHIP STRUCTURES LABORATORY

FRACTURE MECHANICS TEST (CTOD-test) cf. BS-5762-1979

PROJECT SC 90 02

Date: 20 febr 91

CLIENT:

Apparaten en Ketelfabriek A.K.F. By - Goes

Specimen data

Specimen nr

527161

527162

527163

W (height)

(mm)

25.10

25.10

25.20

B (thickness)

(mm)

25.00

25.10

25.10

u-UI C

Fatique precracking data

3

point bending

Testing machine

(kN)

100

100

100

Test temperature

(°C)

20

20

20

Span

(mm)

100

100

100

Loading

(kN)

24.0

24.0

24.0

R

(stress ratio)

0.1

0.1

0.1

Kf

(Nmm-3/2)

1335

1325

1267

Number of cycles (*10A3)

28.78

29.58

27.87

aO (mm)

7.5

7.3

7.8

a4

(nun)

7.3

7.9

7.3

al

(msi)

8.5

8.4

8.5

a2

(mm)

9.1

9.1

8.5

a3

(mm)

9.0

9.0

8.6

a average / W

0.35

0.35

0.34

COD-test data

3

point bending

Testing machine

(kN)

350

350

350

Test temperature

(°C)

-10

-10

-10

Span

(mm)

102

102

102

dK/dt

(N min-3/2 s-l)

56.9

56.7

55.6

Vi

(nun) Vc (mm) Vu (mm) Vmax (mm)

3.650

3.680

3.700

Pi

(kN)

Pc

(kN)

Pu

(kN)

Pmax (kN)

57.5

58.5

59.3

Calculated results

CTODi (mm) CTODc (nun) CTODu (nun) CTODmax (mm)

1.599

1.618

1.677

Yield strength used in calculations:

413 N/mm2

(7)

DLi'UNvERsiTy;oF TECHN0LOGY

FRACTURE MECHANICS TEST (CTOD-test) cf BS-5762-1979

' PROJECT SC 90 02 Dáte: 20 febr 91

CLIENT Apparaten en Ketelfabriek A K F BV - Goes

Specimèn data

Speçimen 'nr' W (height)' B (:thI.ckness)

Fatiqiiè cràcing 'data

Testing machine (kN) Test temperature (°C)

Spn

.' ' (mm) Loading

()

R (stress ratio) Kf (NflUU3/2) Number öf cycles

40

a4 al á2-. a3 al' average: ;

COD -tel t:, lata

Testing machine Test te ,eíáture. ,Span (mm) dK/dt (N mm-3/2 s-1) ,T527261

52262

26.60 26.50 26.i3O ' 26.5Ö' point bending poLn't, bending

SHIP STRUCTURES LABORATORY

52.92 7.4 7.8,' 8' .'5 8.'S,\ : 0.32 5272 6:'., 26.5Ò 50.39 7.3 7:5 350' -10 41 3 min va'1id

iOo

P100 100 20 2Ó 2Ò 100 1OQ

iOo

24.0'

240

24.0 '0:1 0.1 0.1 1060 1053 1032

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6

DELFT UNIVERSITY OF TECHNOLOGY SHIP STRUCTURES LABORATORY

FRACTURE MECHANICS TEST (CTOD-test) cf. BS-5762-1979

PROJECT SC 90 02

Date: 20 febr 91

CLIENT:

Apparaten en Ketelfabriek A.K.F. BV - Goés

Specimen data

Specimen nr

527271

527272

527273

W (height)

(mm)

26.60

26.60

26.50

B (thickness)

(nun)

26.60

26.70

26.50

Fatiue precracking data

3

point bending

Testing machine

(kN)

100

100

100

Test temperature

(°C)

20

20 20

Span

(mm)

100

100

100

Loading

(kN)

24.0

24.0

24.0

R

(stress ratio)

0.1

0.1

0.1

Kf

(Nnim-3/2)

1026

1059

1039

Number of cycles (*1O"3)

50.09

41.10

48.51

aO (nun)

7.8

7.5

7.3

a4

(nun)

7.9

7.4

7.7

él

(mm)

8.4

8.6

8.3

a2

(mm)

8.5

9.0

8.6

a3

(mm)

7.9

8.3

7.9

a average / W

0.31

0.32

0.31

COD-test data

3

point bending

Testing machine

(kN)

350

350

350

Test temperature

(°C)

-10

-10

-10

Span

(mm)

102

102

102

dK/dt

(N mm-3/2 s-1)

53.8

55.8

53.8

Vi

(nun)

---Vc - (mm)

---

0.520

Vu (mm)

1.000

1.260

Vniax (mm)

-Pi

(kN)

Pc

(kN)

69.5

Pu

(kN)

73.3

76.0

Pflax

(kN)

Calculated results

CTODJ. (mm) CTODc (mm)

0.294

CTODu (mm)

0.524

0.635

CTODmax (mm)

Yield strength used in calculátions:

413 N/nun2

(9)

7

DELFT UNIVERSITY OF TECHNOLOGY SHIP STRUCTURES LABORATORY

FRACTURE MECHANICS TEST (CTOD-test) cf. ES-5762-1979

PROJECT SC 90 02 Date: 20 febr 91

CLIENT: Apparaten en Ketelfabriek A.K.F. EV - Goes

Specimen data

Specimen nr 527341 527342 527343

W (height) (mm) 26.60 26.60 26.60

B (thickness) (mm) 26.60 26.60 26.60

The testing of specimens 34. 1 has been interrupted wIthout ïnfliieñce

on the result and validity of the test.

Fatique precracking data 3 point bending

Testing machine (kN) 100 100 100 Test temperature (°C) 20 20 20 Span (mm) 100 lOO 100 Loading (kN) 24.0 24.0 24.0 R (stress ratio) 0.1 0.1 0.1 Kf (Nmm-3/2) 1142 1084 1067

Number of cycles (*lO'3) 54.32 52.80 50.00

aO (mm) 7.9 7.7 7.3 a4 (mm) 7.8 7.8 7.8 al (mm) 9.4 8.6 8.6 a2 (mm) 9.6 9.1 8.7 a3 (mm) 9.1 8.8 8.7

a average W

0.35 0.33 0.33

COD-test data 3 point bending

Testing machine (kN) 350 350 350 Test temperature (°C) - lo -10 - lo Span (mm) 102 102 102 dK/dt (N mm-3/2 s-l) 59.3 56.9 55.7 Vi (mm) Vc (mm) Vu (mm) Vmax (mm) 3.370 3.440 3.420 Pi (kN) Pc (kN) Pu (kN) Pmax (kN) 73.0 78.0 78.8 Calculated results CTODI. (mm) CTODc (mm) CTODu (mm) CTODmax (mm) 1.495 1.602 1.617

Yield strength used in calculations: 413 N/mm2

(10)

FRACTURE MEÇ}IÄNICS TEST (CTÒD-test) cf. BS-5762-1979

PRÌECT Sc 9Ó 02 Date: 20 fébr 91

Fatiaue precracking data 3 point bending

Testing machine (kN) 100 100 100 Test temperature (°C) 20 20 20 Spaú . (mm) 100 100 100 Loading (kN) 24.0 28.0 28,0 R (stress ratio) 0.1 0.1 0.1 Kf (Nmm3/2) 1072 12,72 1237

'Nûmber 'of cycles (*10A3) 44.15 19.02 29.21

aO (mm)

72

78

74

a4 (uhU) 8.1 .7:9 7.8 al (mm)

84

88

86

'a2 ' ' (mm) .

87

8.8, 8.6 a3 . (mm) 8.9 8.8 8.6

aaverage/W

033

033

032

.Testingmathine (kN)

Testtemperàtuie

. Span ." ' : ÇmmY dK/dt' N. mm-3/2 ' s-1)', Vc (mm) Vu (mm) Vinax ' (mm), Pi (kN) Pc (kN) (kN)" Pmax (kN) 8 350 350 -10

-19

102 102 55$:' ''56.4.: 80.0 80.8 7.9.5 CTOD± CTODc CTODu CTODmax .409' :,Y2.,366 '

Yield strength used in calculations 413 N/mm2

:Välid valid: . :' 'ial id'

CLIENT: .Apparatenen Ketelfabriek A.K.F. BV - GOes

Specimen data

Specirner' nr ':' 527351 527352 527353

W (height) (mm) 26 50 26 50 26 60

B ('thckness)' '(mm). 26.70 '26.60:. 26.60

DELFT UNIVERSITY OF TECHNOLOGY SHIP STRUCTURES LABORATORY

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Calibration of MTS clip gauge 2 5 mm 27 Clip sauge

t.M!Í'S.

1632-012C-2Ò' erial number: 675 .

aringaè2.5 mm

60micoV/V rañge

Calibration device LSC microspan

Clock gauges 0 0 5 mm with 0 001 mm accuracy

:0 - 2Y5nim

ith:o.;l:mm acçuracy..

The clip gauge/óôncÏÏ.ioner combinatiìàri hsbeèii calibrated on thé 8 h of Fehruáry 1991

The results:are:

o - 0.5 iii L916Volts peEinm, iiiacburacy '0.004 mm, 1% of f.s.r

o - 2.5 1.930 Volts e:thm, inaccuracy 0,016 nm, 0.7 % of f.s..r..

(30)

C1ip,gaug type MTS 632-02C-20

Serial number 675

Measuring ratìgé:, 2. 5mm

Calibration of MTS clip gauge 2 5 nun

Gauge conditionr Peekel MCA100 in 5000 microV/V range (

Calibration device LSC microspan

Clock

ues

0 - -05 nvitiiûfltmi mm

iO 2 5 smi with O OL mm accuracy

The clip gauge/conditioner combination has been calibrated on the 21st of February

1991 L

The results are:

O - 0 5 mm 919 Volts per mm, inaccuracy 0 003 mm, 0 6 % of f s r

Cytaty

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