• Nie Znaleziono Wyników

Chemical & Metallurgical Engineering, Vol. 50, No. 8

N/A
N/A
Protected

Academic year: 2022

Share "Chemical & Metallurgical Engineering, Vol. 50, No. 8"

Copied!
140
0
0

Pełen tekst

(1)

S. D . KIRKPATRICK . . . Editor JAMES A . LEE...M a n a g in g Editor THEODORE R. O L IV E .. . . .A s s o c ia te Editor HENRY M. BATTERS... M a rk et Editor JOHN R. CALLAHAM A s s is ta n t Editor NORMAN G. FARQUHAR. .A s s is ta n t Editor LESTER B. PO PE... A s s is ta n t Editor

EDITORIAL REPRESENT. "IVES

E. S. STATELER...C h icag o R. S. McBRIDE... , + .W a s h in g to n EARLE M A U L D IN ....,

i

... A tla n ta

M. A . W ILLIAM SO N . . . P u b lish er DISTRICT MANAGERS

E. H. BEDELL...N e w Y ork R. G . FREDERICK...N ew York FRED GRANT ... C le v e la n d L. A . CUNNINGHAM ...C hicago W . D. BOYD... Boston J. R. VAN ARSDALE...P h ila d e lp h ia

»u b lished m o n th ly . P rice 35 c en ts p e r co p y , id d r e s s c o m m u n ic atio n s a b o u t su b sc rip - io n s to D irector of C irc u la tio n , C hera. &

Viet., 330 W est 42 St., N ew York, N. Y.

Subscription r a te s : U n ited S ta te s , M exico, C entral a n d S outh A m e ric a n c o u n trie s, $3 it y e a r , $4 for tw o y e a r s , $5 for th re e / e a r s . C a n a d a , $3.50 a y e a r , $5 for tw o y e a rs, $6 fo r th r e e y e a r s (p a y a b le in C an ­ a d ia n fu n d s). G re a t B ritain a n d B ritish P o ssessio n s, 30 sh illin g s a y e a r , 60 s h illin g s to r th re e y e a r s . A ll o th e r c o u n trie s, S5 a y e ar, $10 for th re e y e a r s . E n te re d a s seco n d s la s s m a tte r, S e p te m b e r 3, 1936, a t Post o ff ic e a t A lb a n y , N. Y., U. S. A ., u n d e r a ct

¡of M arch 3, 1879. C o n ten ts c o p y rig h te d ,

|9 4 3 , b y M cG raw -H ill P u b lish in g C o m p an y ,

^ c . B ra n c h offices: 520 N orth M ich ig an flv e n u e , C h ic ag o ; 68 Post S tree t, S a n F r a n ­ cisco; A ld w y c h H o u se, A ld w y c h , London, V. C. 2; W a s h in g to n ; P h ila d e lp h ia ; C le v e ­ l a n d ; D etroit; St. Louis; B oston; Los A n ­

geles; A tla n ta .

R etu rn P o s ta g e G u a ra n te e d

cGRAW -HILL PUBLISHING C O ., INC.

JAMES H. McGRAW F o u n d er a n d H o n o ra ry C h a irm a n u b lic a tio n Office

99-129 N orth B ro a d w a y , A lb a n y , N. Y.

to ria l a n d E x ecu tiv e O ffices

330 W est 42 S tree t, N ew York, N. Y.

SS H . M cGRAW , J r ... P resid e n t -OWARD EHRLICH.Executive V ice-P resid en t IA SO N B R IT T O N ... V ice-P resid en t CURTIS W . M cG R A W ...T r e a s u re r GERARD I ...S e c re ta ry

% E. BLACKBURN, Jr., D irector of C irc u la tio n

$ M em b er AJB.P. M em b er A 3 .C .

" a b le A d d re ss McGRAWHILL, N ew York

ENGINEERING

A U G U S T , 1 9 4 3

War Lesson No. 1 ...

EDITORIAL FOREWORD

G lass Cellulation Produces Lightweight Insulation.

By NORMAN G. FARQUHAR

95

98 Liquid Chlorine S y stem s... 102

By WILLIAM H. MAGEE

Making Apple Syrup, a Glycerine and Sugar Substitute. . . . 104

EDITORIAL STAFF

Infra-Red Penetrates Many Process Industries.. 105

By E. H. ROBINSON

N ew Approach to Continuous Reactor Design-II...107

By A . BROTHMAN, A . P. WEBER a n d E. Z. BARISH

Corrosion of Iron b y A m m onia... m

By HUGH J. McDONALD a n d MORRIS FELLER

Fallen Animals, A Little-Known Process Industry 112

By W . MERLE ROBINSON

Fluorescent Method Detects Leaks in Process V essels 116

By FRANKLIN CATLIN

Alcohol for W ar and Postwar... n g

A CHEM. & MET. REPORT

Salicylic Acid and S a licyla te... 132

A CHEM. i MET. PICTURED FLOWSHEET

C h e m .

&

M e t . P l a n t N o t e b o o k . . . . . 1 1 7 F r o m th e L o g o f E x p e r ie n c e ... 1 6 7 P ro c e s s E q u ip m e n t N e w s ... . . 127 M e e t in g s a n d C o n v e n t io n s . . 1 73 C h e m ic a l E n g in e e r in g N e w s . . 139 N e w s F r o m A b r o a d ... 186 N e w s F r o m W a s h i n g t o n ... . . 141 C h e m .

&

M e t . B o o k s h e lf ... 197 I n t e r p r e t i n g W a s h i n g t o n ... . . 145 C h e m ic a l E c o n o m ic s a n d M a r k e t s . 2 0 7 N e w P r o d u c ts a n d M a t e r i a l s . . . . 151 C u r r e n t P r ic e s ... 2 1 3 P e r s o n a lit ie s ... . . 159 N e w C o n s tru c tio n ... 2 1 6

A n in d ex to a d v e rtis e rs w ill b e fo u n d on p a g e 344

A M c C S A W - H I U P U B L IC A T IO N

M cG R A W -H ltL PUBLISHING COMPANY 330 W est 42nd S tree t, N ew York, N. Y.

D irecto r of C ircu latio n :

P le a se c h a n g e m y a d d re s s o n C h em ical 6 M e ta llu rg ic a l E n g in ee rin g

From

To

S ig n e d

(2)

G R I N D I N G S C R E E N I N G

C R U S H I N G

C y lin d ric a l m ills.ball o r r o d m e­

d ia , b atch o r contin uo us type.

V ib r a t in g & ro ta ry screens, w e t

& d r y — la rg e st line in U. S.

Jaw , g y ra to ry , roll & ham m er crushers — f o r o re & rock.

HERE ARE FOUR O F THE M O S T

ivwr,

Unexpected Breakdowns?

Labor Shortage?

Me n

W

anted

NO EXPlRIENCt

HtCtSSWt't

H o w m a n y o f yo u r key m achines were d e s ig n e d f o r 2 4 - h o u r - d a y se rvice ? G o o d point to check to d a y l

D o e s p a rt o f yo u r p r o c e ss use m en n e e dlessly? Rem em ber, proce ssing is

a machine industry!

WHICHEVER IT IS —

M

E N m u s t w o r k t o g e th e r b t h a n e v e r b e f o r e to wir w a r . . . a n d s o m u s t m a c h i n e !

I f f a i l u r e o f m a c h i n e s to t o g e t h e r p r o p e r l y i s a t t h e ro y o u r w a r t i m e p r o c e s s i n g p r d r e m e m b e r t h e r e ’ s o n e com ] t h a t

specializes

i n m a k i n g c h i n e s “ t e a m u p ” . . . A llis - C h a h Collaboration of specialists is basic in A -C Cooperative Engineering.

A U G U S T 19J,S • C H E M I C A L & M E T A L L U R G I C A L E N G I N E E R 1

(3)

CHEMICAL

t m e t a l l u r g i c a l

ENGINEERING

ESTABLISHED 1902

A U G U S T , 1943

S. D. KIRKPATRICK, Editor

OUR WAR LESSON N O . 1

V

V H E N th e com plete h isto ry of th is w a r is w ritte n , one of its m ost in te re s tin g a n d d ra m a tic c h a p te rs w ill deal w ith th e c o n trib u tio n s o f A m e ric a n sc ien tists a n d en g in eers. T he little know n b u t h ig h ly im p o rta n t w ork b ein g done on w a r p roblem s in u n iv e rs ity and in d u s tria l re se a rc h la b o ra to rie s wil 1 some d a y m ake an am azing re c o rd o f achievem ent. M eanw hile, te n s of th o u san d s o f m en an d w om en, in te r r u p tin g th e ir careers in science a n d in d u s try , a re g iv in g u n s tin t- ingly of th e ir tim e a n d effort. W h a t ’s to become of this w ork a f te r th e w a r? A re we going to close th e book, as we d id a f te r W o rld W a r I, a n d let someone else w o rry a b o u t th e science a n d technology of national d efen se?

Some of th e e m in e n t m en who a re hig h in th e councils o f th e Office of S cientific R esearch a n d D evelopm ent believe i t w ill be difficult, or im possible to hold su ch a n o rg a n iz a tio n as th e irs to g e th e r once the w a r is won. T h ey sa y t h a t th e c o u n tr y ’s scien tists and technologists are w illin g to accep t coercion an d re g im e n ta tio n o n ly as lo n g as th e ir services a re im ­ m ediately n eed ed by th e a rm e d forces. A f te r th a t th e y w ant to s c a tte r to th e f o u r w inds, to p ick u p th e ir peaceful p u rs u its , to fo rg e t a b o u t th e ir w a r w ork—

except p e rh a p s to w rite some books o r p u b lish some scientific p a p e rs on su b je c ts 110 lo n g e r u n d e r secrecy orders.

All th is is a v e ry n a tu r a l re a c tio n to a v e ry u n ­ n a tu ra l s ta te of affairs. T he sc ie n tis t is an in d iv id u a l.

W hile he m a y s h u n p e rso n a l p u b lic ity , he w a n ts an d u su ally d e m a n d s c re d it f o r h is p ro fe ssio n a l achieve­

m ents. H e is o fte n a n id e a list, se n sitiv e to criticism of his m otives. H e rese n ts th e idea o f h is w ork being p ro s titu te d to w h a t some one m ay call an unsocial or in h u m a n ita r ia n end.

I t is n o t s tra n g e , th e re fo re , th a t before th e w a r our u n iv e rsitie s w ere o fte n th e m e e tin g places f o r the p ro fessio n al pacifists. O rg a n iz a tio n s like W oi'ld Peace- ways b o asted of th e p ro fe sso rs a n d college p re sid e n ts in th e ir m em b ersh ip . T he sam e s itu a tio n o b tain ed in

G reat B rita in . A d m iral B lan d y , U. ¡S. C h ief of N av al O rd n an ce, in a re c e n t a n d classic a d d re ss on “ R e­

search fo r W ar, ’ te lls ab o u t a B ritish a irp la n e m a n u ­ f a c tu r e r who in 1935 a tte m p te d to c o n trib u te £10,000 fo r an a e ro n a u tic al fellow ship at, C am b rid g e an d th ereb y ro u sed a storm of p ro te s t because he w as accused o f tr y in g to p ro m o te w a r re se arch . S u ch con­

tro v ersie s w ere n o t a risin g a t th a t tim e in G e rm an y a n d J a p a n — o r in R ussia, eith er. O nly one y e a r b efore H itle r cam e in to pow er, a c h a ir w as set u p in th e U n iv e rsity of B e rlin f o r th e s tu d y of w a r economics.

G eopolitics k e p t a b re a st o f m ilita ry science a n d a d d e d to th e b r u ta l success of G erm an m ig h t in 1939 a n d 1940. W e in th e dem ocracies h a d to le a rn , alm o st too late, th a t to ta l w a r affects ev ery p a r t o f o u r econom y.

F o rtu n a te ly , the M achiavellian p la n s of o u r enem ies have all b u t failed. The ev en tu a l triu m p h of o u r cause w as n ev er m ore certa in . Y et, in a ll h o n esty , we should ask ourselves w h e th e r o r n o t we h a v e le a rn e d a n d a re s till le a rn in g lessons fro m th is w a r t h a t w ill h elp us to be b e tte r p re p a re d in th e f u tu r e . I f o u r experience th is tim e h as convinced us th a t we m a d e a m istake a f te r th e la s t w a r w hen we ab a n d o n e d all w a r research except th a t in a few h a lf-s ta rv e d a rsen als, th e n we sh o u ld s ta r t now in a p ro g ra m o f p u b lic education.

T he lay m an , w ho in th e en d d e te rm in e s bo th o u r m ilita ry a n d ed u catio n al policies, m u st be m ad e to realize th a t o u r d e s tin y as a N a tio n d e p e n d s on th e use we m ake of science a n d technology. I f in s p ite of o u r ideals we are to be ch allen g ed p e rio d ic a lly by enem ies who have p lo tte d o u r d e s tr u c tio n ,.th e n p r a c ­ tic a l idealism calls fo r p re p a re d n e s s. I t calls fo r a re a liz a tio n th a t we m u st n e v e r a g a in n e g le c t th e th in g s th a t are m ost im p o rta n t f o r o u r n a tio n a l de­

fense. R esearch is c e rta in ly one of these. I f we have le a rn e d o u r lesson w ell, we w ill in s is t on th e c o n tin u a ­ tion of some o f th e c o n tra c ts w ith e d u c a tio n a l in s titu ­ tions w h ereb y y o u n g m en a re tr a in e d a n d k e p t a b re a s t of th e science a n d technology of w ar.

(4)

IMPENDING CHANGES IN A.S.T.P.

%

A

rmy

dem ands fo r chemical engineers in the m ilitary service are so few th a t no more young men are to be assigned fo r tra in in g u n d e r the A rm y Specialist T ra in in g P rog ram . This decision was reached d u rin g J u ly a fte r a resurvey of the needs fo r chemical engi­

neers in uniform .

T hat th ere is a continuing dem and for m en of such tra in in g in the chemical process industries, however, is fu lly recognized in W ashington as well as th ro u g h ­ ou t the country. The A rm y is stu d y in g m ethods by which it m ight assist in m eeting this in d u strial need.

One proposal is th a t the A rm y should continue to tra in young men as chemical engineers through the A .S.T .P. arran g em en t w ith the u n d ersta n d in g th a t such trainees, on completion of courses, would be assigned on furloughs to in d u stria l positions. The positions w ould be those in in d u stry in which O rd­

nance, Chemical W a rfa re, A ir Corps and other A rm y u n its are d irec tly interested because the research or m a n u fa c tu rin g th u s aided by young engineers would be of direct concern to th e m ilitary.

U p to A u g u st 1, no specific program had been form ulated which h ad fu ll approval of both in d u strial and m ilita ry executives. I t is hoped th a t the M anu­

fa c tu rin g C hem ists’ Association can serve as a liaison between the two groups in the form ulation of a work­

able scheme. Such resu lts would enable p ro p erly p re ­ pared and com petent young train ees taken by the A rm y to go ahead w ith th e ir chemical engineering education. In cidentally, the q u a lity of the tra in in g would be guided by jo in t action of A rm y, in d u strial and educational leaders. T hus the men would be of a q u ality suited to the jobs to which th ey would be assigned. Num erous difficulties lie ahead of the com­

pletion of the p ro g ra m ; b u t early in A u gust the p ro ­ ponents were hopeful as to results.

FLUID FUEL INSURANCE

F

luid

fuels can be m ade from solid m inerals. This fact has long been known. B u t we still do no t know w hat technology will best serve fo r the processing of oil shale, bitum inous coal and lig n ite when a petroleum su b stitu te is the objective. Som ething should be done about this.

A specific proposal is now being considered by the S enate Committee on P ublic Lands. The proposal is th a t a sub stantial sum be authorized fo r use of the II. S. B u reau of Mines in the investigation of m ethods fo r p roducing synthetic liquid fuels from coal and other solid m ineral m aterials. L ed by S ecretary Iekes, an im pressive group of officials has appeared before the Senate Committee u rg in g the enactm ent of this bill, S. 1243.

E xperienced chemical engineers w ill not agree w ith all of the alarm in g predictions about petroleum short- age, n o r will they accept all of the super-optim istic forecasts of success for a n y experim ents in liquefac­

tion of coal u n d e r A m erican conditions. B u t th ere is am ple evidence to su p p o rt the general idea th a t m ore fu nd am en tal studies should be made. These should encompass the best proposals fo r m aking eith er gase-

ous or liquid p ro du cts from oil shale, bitum inous coal, or lignite. Investm ent in sound research w ill be good insurance against fluid-fuel shortage in the years tc come. One needs to be n eith er an alarm ist nor a p o lit­

ical p ro p a g an d ist to accept the broad p rin cip le of this bill provided the m anagem ent of th e engineering studies can be le ft w ith the com petent technical staff of the B ureau.

WHICH W A Y OUT?

E

quitable

policies fo r the term in atio n of w ar con­

tra c ts a t the cessation of hostilities are alread y de­

m anding increased atten tio n. Several proposals are before Congress in clu d in g a s ta n d a rd term in ation clause th a t is being developed by th e P rocu rem ent Policy Division of th e W .P.B . A recen t business con­

ference held w ith the s u p p o rt of the U. S. Cham ber of .Commerce, has suggested (1) an overall term in a­

tion procedure grou pin g contracts and su bcontracts;

(2) p ro m p t paym en t of 75 p ercen t of all claims w ith ­ out a u d it; (3) avoidance of d u plicatio n in a u d its ; (4) review of both facts and law in d isp u ted cases; (5) allowances fo r costs of am ortizable facilities, postw ar conversion, losses on other contracts an d o rd in ary business expenses; (6) adoption of the prin cip le of settlem ent b y negotiation an d (7) reasonable lim ita­

tions on establishm ent an d uses of reserves.

M any p riv ate in d u stries suffered alm ost in te r­

m inable delay in th e ir con tract settlem ents a fte r the first W o rld W ar. L et us hope we m ay be b e tte r p re ­ p ared this time.

DANGEROUS STOCKPILE LEGISLATION

A

bloc o f A v estern s e n a t o r s i s m a k i n g a n e a r l y s t a r t o n p l a n s f o r a p o s t w a r m i n e r a l s t o c k p i l e . T h e y r e c it e t h e s e r io u s d i f f i c u lt i e s i n g e t t i n g m i n e r a l s f o r

Avar

u se a n d a r g u e t h a t U n c l e S a m s h o u l d n e v e r a g a i n ris k s u c h s h o r t a g e . T h e i r a r g u m e n t s a r e s o u n d , b u t o n ly i n s o f a r a s t h e y r e l a t e t o t h e n e e d f o r m i n e r a l r e s e r v e s . T h e t e c h n i q u e f o r c o r r e c t i o n s A vhich t h e y p r o p o s e is a n a p p a l l i n g d i s t o r t i o n o f s o u n d e c o n o m ic s a n d t e c h ­ n o l o g y .

T h e ir p r o p o s a l is t h a t d o m e s t i c m i n i n g i n t e r e s t s b e s u b s id iz e d f o r a c e r t a i n p e r i o d a f t e r t h e w a r i n o r d e r to s t i m u l a t e p r o d u c t i o n o f s t r a t e g i c a n d c r i t i c a l m a t e ­ r ia l s . T h e y h a v e i n m i n d b o t h t h e p r e s e n t w a r e f fo r t a n d p o s t w a r p r e p a r e d n e s s . B u t , c l e a r l y r u n n i n g t h r o u g h t h e S c r u g h a m b i l l ( S . 1 1 6 0 ) i s a p l a n t o s u b ­ s i d i z e m a r g in a l a n d s u b - m a r g in a l m i n i n g e n t e r p r i s e s i n t h i s c o u n t r y . I n f a c t , o n e o f t h e s t a t e d p u r p o s e s o f t h e b i l l i s “ t o a v o i d t h e w i d e s p r e a d e c o n o m ic d i s ­ t r e s s a n d f a i l u r e a m o n g s m a l l o r m a r g i n a l m in e OAvners . . . ”

A n u n m i n e d m i n e r a l r e s o u r c e is a l r e a d y a f o r m o f s t o c k p il e . T h e p r o d u c t o f s u c h a m i n e i s o f t e n n o m o r e v a l u a b l e i f i n s o m e r e s e r v e s t o r a g e t h a n i t w o u l d b e i f s t i l l i n t h e g r o u n d a s a p r o v e n r e s o u r c e . I n m a n y e a s e s , w i t h c h a n g e o f p o l i t i c a l p o l i c y , a r e s e r v e i n a s t o c k p i l e m a y b e d i s s i p a t e d , A vh ereas a r e s o u r c e i n t h e g r o u n d w o u l d n o t b e . T h e s e a r e A v e ll- e s t a b lis h e d f a c t s . T h e y a r e f a c t s w h i c h a r e i g n o r e d i n t h e p l a n f o r

9 6 A U G U S T 1 9 J fS C H E M I C A L & M E T A L L U R G I C A L E N G I N E E R I N G

(5)

m ining o u t these m arginal ore reserves irrespective of cu rre n t use and needs.

The chemical process industries are am ong th e p rin ­ cipal users of m any strateg ic an d critical m aterials, w hether produced in this co u n try or im ported from abroad. They are, therefore, directly concerned w ith any postw ar plans fo r stockpiles. P erh a p s if th e ir selfish needs as consumers w ere balanced again st the equally selfish interests of the m ineral producers, b etter legislation would result. In an y event they should be consulted.

MORE PLANT CONSTRUCTION

C h e m ic a l p la n t construction will not stop. In fact, in the stric tly chemical in d u stries it m ay be g reater next y ear th an last. This p o in t is em phasized because some readers have m isunderstood

Chem . & M et. ’s

edi­

torial of last m onth which sta rte d with the statem ent

th a t “ B uilding w ar factories is nearin g com pletion.”

O ur com m ent was inten ded to re fe r to general con­

stru ctio n and n o t to specialized jobs fo r chemical m an ufactu ring . M any of these la tte r p ro jects are still to be built. I n fa c t some W ashington officials estim ate th a t we will spend m ore m illions on new chemical m an u fa ctu rin g facilities d u rin g the n ex t twelve months th a n d u rin g the last.

However much we spend, and w hatever the chem­

icals m ay be th a t we shall plan to make, th ere still rem ains the im p o rtan t point we have freq u en tly em­

phasized. C onstruction from now on should be b u ilt w ith a view to its postw ar service to A m erican in dus­

try . T h at objective cannot supersede questions of im m ediate w ar value, however, b u t such consideration can an d should be taken into account so th a t both w ar and postAvar will be served to the m axim um possible extent as Ave expand m an u factu rin g facilities or as we m odernize them.

WASHINGTON HIGHLIGHTS

COAL STORAGE m u s t b e c a r e f u l l y p la n n e d . I t i s n o t e n o u g h to g e t p l e n t y o f c o a l i n t o s t o r a g e , a lt h o u g h t h a t is im p o r t a n t r i g h t n o iv . S o a ls o i s p r o p e r p i l i n g a n d v e n t i la t i o n o f t h e p i l e s , e s p e c i a l ly o f c o a ls w h ic h te n d t o h e a t in th e s t o c k p ile . E v e n t h o s e c o a ls t h a t do n o t h e a t b a d ly e n o u g h to c a u s e s p o n t a n e o u s c o m b u s t io n m a y d e p r e c i­

a te m u c h m o r e t h a n n e c e s s a r y d u r in g s to r a g e Avhen in c o r r e c t ly p ile d .

ENRICHMENT o f fo o d s b y a d d itio n o f vitam in s an d nutritiA^e m in e r a l in ­ gred ien ts is n o w r eq u ired f o r bread and certain o th er im p o r ta n t com m od i­

ties. W a r F o o d A d m in is tr a tio n is also tr y in g to d ecid e h o w a ll flour u sed in the h ou seh old sh all he sim ila r ly en ­ riched. T h u s, avc m u st e a t o u r A’ita - m ins and m in e r a ls Avhether avc w a n t them or n o t. B u t it m ea n s b u sin e ss fo r th ose c o m p a n ie s th a t m a k e s y n ­ th etic v ita m in s a n d p r e p a r e th e fo o d m in era ls in th e sp e c ia l fo r m s req u ired . POSTWAR LABOR w ill Avork u n d e r a 3 0 -h o u r Aveek i f C .I .O . h a s i t s Avay.

A ls o , i t w i l l b e g o v e r n e d b y t h e l e g i s ­ la tio n o f a s t r o n g la b o r C o n g r e s s , a c ­ c o r d in g t o Avell la id p l a n s o f la b o r le a d e r s. T h e s e a r e m a t t e r s Avhich c a n w e ll b e d is c u s s e d Avith p r e s e n t m e m b e r s o f C o n g r e s s Avhen t h e y a r e h o m e t h is su m m e r a m o n g t h e ir c o n s t it u e n t s .

DEFERMENT c a s e s o f c r i t i c a l c h a r a c t e r sh o u ld b e r e f e r r e d m o r e o f t e n f o r th e a s s is t a n c e o f t h e N a t i o n a l R o s te r . S h o r ta g e s o f t e c h n ic a l m a n p o w e r in in d u s t r y a n d in r e s e a r c h a r e b e c o m in g m o re o f a t h r e a t t o t h e Avar e ffo r t th a n a s h o r t a g e o f c h e m ic a l m anp oA ver in th e a r m e d f o r c e s . O ffic ia l W a s h in g t o n

w ill be v e r y g la d to h a v e e m p lo y er s r e ­ q u est r ev iew o f d ifficu lt d e fe rm e n t ea se s b y th e C o m m ittee on C h em ists a n d C h em ical E n g in e e r s o f th e N a ­ tio n a l R o s te r o f S p e c ia liz e d P e r s o n ­ n e l, W a sh in g to n ,

D.

C. L o ca l h o a rd s sh o u ld a lso be u r g e d to u se th is so u rce o f im p a r tia l, c o m p e te n t a d v ice.

GOVERNMENT OWNERSHIP o f a g r e a t m a n y e s t a b lis h m e n t s a t t h e e n d o f th e Avar p e r io d is c e r t a in . A b o u t 1 5 b illio n d o lla r s Avorth o f s u c h p l a n t s h a d b e e n fin a n c e d A\rith p u b lic m o n e y b e f o r e th e e n d o f M a r c h , 1 9 4 3 , a n d t h e t o ta l groAvs m o n t h ly . N e a r l y 1 0 p e r c e n t o f t h is t o t a l i s m a d e u p o f p l a n t s m a k in g

“ c h e m ic a ls , p e t r o le u m a n d c o a l p r o d ­ u c t s .” I t i s e v id e n t , t h e r e f o r e , th a t c h e m ic a l executiA -es a r e g o i n g t o h a v e a b i g j o b o f n e g o t ia t io n w h e n postA var s e t t le m e n t c o m e s. I t w ill b e im p o r ta n t to k n o w Avho fix e s t h e p o l i c y a n d hoAv m u c h c o n t in u a n c e o f g o v e r n m e n t o w n ­ e r s h ip o r g o v e r n m e n t c o m p e t it io n Avith p r i v a t e b u s in e s s Avill th e n b e s o u g h t . S e e t h e W a s h in g t o n N e w s p a g e s f o r so m e t h o u g h t f u l c o m m e n t b y J e s s e J o n e s .

CASEIN PRICES h a v e been raised to e n ­ c o u ra g e th e sa le o f sk im m ilk from fa r m s. O .P .A . took th is a ction b e­

ca u se o f th e u r g e n t n eed f o r c a sein in p la s tie s , p a in ts , in secticid es, glu e, p a p e r c o a tin g a n d o th er in d u stria l a p p lic a tio n s. T hu s a t le a s t on e g r o u p o f la w y e rs a n d eco n o m ists in th is u n ­ p r e d ic ta b le a g e n c y c o n fe sse s th a t the la w o f s u p p ly a n d dem an d m u st f u n c ­ tio n in ord er to m ove g o o d s fr o m on e u se to an oth er, even in w a r tim e.

W o u ld th a t oth e rs th ere w ere e q u a lly sm a rt.

RUBBER p r o b le m s o f l a r g e im p o r t a n c e a n d o f c o n s id e r a b le n u m b e r r e m a in t o b e s o lv e d . B u t i t is n o w eA’i d e n t t h a t b y a lm o s t s u p e r h u m a n e f fo r t o n th e p a r t o f c h e m ic a l e n g in e e r s in t h e r u b ­ b er, c h e m ic a l a n d p e t r o le u m in d u s t r ie s , s y n t h e t ic r u b b e r p r o d u c t io n i s g e t t i n g u n d e r w a y o n a h u g e s c a le in a n u n ­ b e lie v a b ly s h o r t t im e . W a s h i n g t o n i s d e lig h te d . I t f e e l s t h a t t h i s i s o n e o f in d u s t r y ’s o u t s t a n d in g A vartim e a c h i e v e ­ m e n ts . I t i s e v e n t a l k i n g a b o u t h o w s o o n th e r e Avill b e p l e n t y o f t ir e s f o r e v e r y b o d y . T h is i s a b it u n f o r t u n a t e , to b e s u r e , b e c a u s e t ir e s f o r e v e r y j a l ­ l o p y a r e n o t l i k e l y t o b e a A 'ailab le f o r m a n y m o n t h s t o c o m e . B u t t h e “ w e ll d o n e ” w h ic h o n e h e a r s s o f r e q u e n t l y in W a s h in g t o n o f l a t e i s a n h o n e s t , s i n ­ c e r e , a n d Avell d e s e r v e d t r ib u t e .

RAYON V S . COTTON is o n e o f the s ta r co n tro v ersies o f the d a y . T h e issu e is : W ill sc ien tific f a c ts o r p o litic a l p r e s ­ su re d eterm in e Avhat k in d o f fa b r ic

(c o r d ) is to be u sed in m a k in g h e a v y - d u ty tir e s? F o r the s a f e t y o f th ose Avho u se the v e h ic le s, all te ch n ica l m en e a rn e s tly h o p e that th e f a c ts w ill w in .

CHARCOAL p r ic e s h a v e been in crea sed m a te r ia lly u n d er th e n ew c e ilin g s e t b y O .P .A . T h is avill g iv e te m p o r a r y r e lie f to the ch a rco a l p ro d u cers, b u t it c er­

ta in ly w ill a lso inA-ite v ig o r o u s n e w co m p e titio n . S o m e u ser s are fin d in g th a t certa in ty p e s o f n o n -e a k in g b itu ­ m in o u s co a l w ill d o a lm o st a s Avell a s ch a r co a l in so m e fu r n a c e r e d u c in g - r e a g e n t jo b s . H e n c e ch a rco a l p r o ­ d u cers w h o ta k e a d v a n ta g e o f th e 50 p e r ce n t in c re a se in c e ilin g p r ic e s m a y la te r find th e m se lv es e n tir e ly Avithout b u sin e ss a m o n g su ch cu sto m ers.

C H E M I C A L & M E T A L L U R G I C A L E N G I N E E R I N G A U G U S T 1 9 Ą S

9 7

(6)

Glass

C ellalation Produces Lightweight Insulation

To insure a uniform product, m oisture is elim in ated from the sp e c ia lly p rep ared cullet in this gas-fired rotary d ryer at the v e r y start of the p ro cess.

After drying, the cu llet is ground in a la r g e b a ll mill

N O R M A N G . F Ä R Q U H Ä R A ssista n t Editor, Chem ical & M etallurgical E ngineering

--- C h em . & M e t I N T E R P R E T A T I O N - ... ... ..

Of the m a n y products d e v e lo p e d during the la st y e a r or so, F o a m g la s, Pittsburgh-Corning's c ellu la r g la s s , is o n e w h ich w ill b e w id e ly u sed in the y e a r s to com e. W hether for air-conditioning of b u ild in gs, for co ld sto ra g e fa c ilitie s or for in su lation of industrial equipm ent, there w ill b e nu m erou s a p p lica tio n s for this lig h tw eig h t insulator w h ich a lso p rovid es re sista n c e a g a in st g a s , m oisture, fire and verm in. Its production a n d properties are d escrib ed here for our r ea d ers—

Editors.

G

l a s s , a l r e a d y w i d e l y u s e d in the field o f h ea t in su la tio n , n o w o f ­ f e r s a rem ark ab le, n e w c ellu la r in s u ­ la tio n m a teria l o f ab ou t th e sa m e d e n s ity a s co m m ercia l b a lsa w o o d or cork. P ro d u c ed by th e P itts b u r g h - C o rn in g C orp ., th e n e w p ro d u ct k n ow n a s F o a m g la s is m a d e b y a chem ical r ea c tio n so m e w h a t a n a la g o u s to the r a is in g o f b read d o u g h w ith y e a s t.

C erta in o x id e s in m o lte n g la s s rea ct w ith a sm a ll q u a n tity o f c a rb o n to m a k e carb on m o n o x id e and d io x id e g a s e s w h ich a r e tr a p p e d w ith in the g la s s a n d fo rm t in y sea led a ir ch am ­ b ers n u m b erin g m ore th a n 5 m illio n in o n e cu b ic fo o t.

S in c e its str u c tu r e is cellu la r rath er th an p o ro u s, F o a m g la s is im p e r ­ v io u s to both w a te r a n d v a p o r s, a p r o p e r ty n ot a v a ila b le in a n y oth er

k n o w n m a ter ia l e x ce p t som e o f the o r g a n ic cellu la r ru b b ers. T h e com b i­

n a tio n o f in o r g a n ic g la ss, th e v a p o r - tig h t c ellu la r stru ctu re, lig h t w e ig h t, h ig h c o m p r ess iv e stren g th and p o te n ti­

a lly lo w m a n u fa c tu r in g c o sts is r e ­ sp o n s ib le f o r P itts b u r g h -C o r n in g ’s e n ­ th u siasm a n d w illin g n e s s to incur h e a v y d e v e lo p m en t c o sts in s p it e o f w a r tim e d ifficu lties a n d h azard s.

P r o b a b ly th e b e st k n o w n a p p lic a tio n o f F o a m g la s is its u se a s th e b u o y a n t elem en t in s e v e ra l ty p e s o f flo ta tio n a p p a r a tu s f o r th e U . S. N a v y . H o w ­ ever, it is e x p e cte d th a t th ere w ill be m a n y oth er u s e s f o r th is n e w p ro d u ct in o u r p e a c etim e eco n o m y . O ne im ­ p o r ta n t field w h ich F o a m g la s h a s a lr e a d y in v a d e d is th a t o f lo w -tem - p e r a tu r e in su la tio n w h ere its p erm a ­ n e n t r es is ta n c e to w a te r is a v ita l

fa c to r . I t se e m s lik e ly th at F o a m - g la s w ill b e u sed a s a s tr u c tu r a l in su ­ la tin g ele m en t in p r e fa b r ic a te d wall, floor and r o o f se c tio n s f o r th e b u ild ­ in g s o f th e fu tu r e . E v e n u n d er to d a y ’s co n d itio n s m a in te n a n c e e n g in e er s are fin d in g it an id ea l a n sw e r to the very r e a l p ro b lem o f g e t tin g a n insulated r o o f th a t w ill r e ta in it s o r ig in a l re­

s ista n c e to h e a t tr a n s fe r w ith o u t re­

q u ir in g fr e q u e n t r e p la c e m e n t or re­

p a ir s. I n th is u se it is becom ing cu sto m a ry to la y sta n d a r d b u ilt-u p r o o fin g o v er 2 in . or m o re o f th e glass.

F o a m g la s w ill s u p p o r t its ow n w eight in a n y t y p e o f w a ll c o n str u c tio n w ith ­ o u t d a n g er o f c r u sh in g or packing, w h ich m a k e s it id ea l f o r b u ild in g up s e lf - s u p p o r t in g p a r titio n s or curtain w a lls o f so lid in s u la tin g m a ter ia l. It sh o u ld n o t, h o w ev e r, be u sed fo r load- b ea rin g w a lls.

T h e Chem ical p r o c e s s in d u str ie s w ill b e q u ick to find n e w a p p lic a tio n s in co n n ectio n w ith e q u ip m e n t, su ch as s tills , co lu m n s, a n d o th e r h e a t ex ­ ch a n g e a p p a r a tu s . On o v en s, fu r­

n a ces a n d o th er h ig h tem p eratu re u n its, F o a m g la s ca n b e u s e d fo r hot- sid e te m p er a tu r e s u p to a b o u t 1,0 0 0 deg. F ., p r o v id e d th e se r v ic e condi­

tio n s do n o t im p o se su d d en o r violen t therm al sh o ck s. T h is p e r m its its use in a la r g e n u m b er o f p r o c es ses in vari­

ous in d u stries.

9S A U G U S T 1 9 .’, S C H E M I C A L & M E T A L L U R G I C A L E N G I N E E R I N G

(7)

DEVELOPMENT OF THE PROCESS F o r a b o u t fifte e n y e a r s p r io r to 1 9 4 1 , o n ly in te r m itte n t in te r e s t in th e p r o c e s s f o r m a k in g c e llu la te d g la ss h a d been sh o w n b y in v e s tig a to r s in F r a n c e , E n g la n d a n d th e U . S . A . H o w e v e r , e a r ly in 1 941, a se r io u s d e­

v e lo p m en t p r o je c t w a s b e g u n b y the P it t s b u r g h C o rn in g C o rp o r a tio n a t a n e w ly co n str u c ted p ilo t p la n t in P o r t A lle g a n y , P a . H e r e , su ch r a p id s tr id e s w e re m ad e th a t in a f e w m o n th s c o n str u c tio n w a s s ta r te d o n a f u ll- s c a le p la n t a lo n g sid e th e e x is tin g g la ss b lock fa c to r y .

T h e n ew p la n t c o n sists o f a o n e - s t o r y b u ild in g c o n ta in in g a p p r o x i­

m a te ly 5 0 ,0 0 0 s q .f t . o f floor sp a c e . I t i s o f m odern c o n str u c tio n w ith a ste e l fr a m e on r ein fo r ce d co n crete fo u n d a ­ tio n s . F lo o r s a re a lso co n crete, w a lls a r e o f brick , g la s s block a n d corru ­ g a te d a sb esto s, p a r titio n s o f tile , and r o o fin g o f tar a n d f e lt o v er g y p s u m p la n k in on e p o r tio n a n d w a te r ­ p r o o fe d co rru g a ted a sb esto s o v er the fu r n a c e s . T h ree c o m p lete p r o c e s s u n its h a v in g a co m b in ed c a p a c ity o f a b o u t 2 5 ,0 0 0 b d .ft. p e r d a y h a v e b een i n ­ s ta lle d in o n e -h a lf o f th e p la n t, the la y o u t h a v in g been p la n n e d to p e r m it in s ta lla tio n o f th ree a d d itio n a l u n its w h en e x p a n s io n is req u ired . A t p r e s ­ e n t a ll th ree u n its arc r u n n in g a t c a ­ p a c ity r a te w ith th e ir e n tire o u tp u t g o in g in to e sse n tia l u ses, m a in ly fo r flo ta tio n a p p lic a tio n s f o r th e U n ite d S ta te s N a v y , an d a s a lo w -tem p er a tu r e in s u la tio n m a ter ia l.

R AW MATERIALS

T h e tw o e sse n tia l r a w m a ter ia ls u sed are a s p e c ia lly p r e p a r e d fo r m o f c u lle t a n d fin e ly d iv id ed carb on . T h e fo r m e r is o b ta in e d fr o m th e p r im a r y m e ltin g fu r n a c e in th e a d ja c e n t g la ss b lock fa c to r y a n d sto r ed in b u lk , w h ile the la tte r is rec eiv e d a n d sto r e d in 1 0 lb. p a p e r b a g s. P a r tic u la r ca re is e x er cise d to p r e v e n t f o r e ig n m a tter, e s p e c ia lly o f a n o r g a n ic n a tu re, fro m c o n ta m in a tin g th e c u lle t, a n d to th is end a s p e c ia lly c o n str u c ted sto r a g e s p a c e h a s b ee n p r o v id e d w ith in the p la n t. O th erw ise, im p u r itie s in the batch w o u ld a ffec t th e c e llu la tin g r e a c ­ tio n a n d th e p r o d u c t w o u ld be im p r o p ­ e r ly fo r m e d w ith b lo w h o les a s in im p e r fe c t m e ta l c a stin g s.

PREPARATION OF BATCH T o in su r e u n ifo r m ch em ical r ea c ­ tio n s in th e fu r n a c e , th e c u lle t is th or­

o u g h ly d ried a n d g ro u n d . D r y in g is a c co m p lish e d in a co u n ter-cu rren t r o ta r y -ty p e d ry er, co n stru cted o f steel, a n d fired b y n a tu r a l g a s. T h e d ryer is f e d b y m ea n s o f b u g g ies k n o w n as

“G eo rg ia b u g g ie s” w h ich b r in g the c u lle t fr o m sto r a g e a n d ch arge it a t a r a te o f a p p r o x im a te ly 60 lb . p e r m in.

D r ie d c u lle t d isch a rg ed fro m th e d ryer is p ic k e d u p b y b u ck ets on a b elt e le v a to r a n d carried to the c u lle t h o p ­ p e r , a n e le v a ted ste e l b in u sed f o r a n in te r m e d ia te s to r a g e a n d fe e d e r s u p - p ly .

G r in d in g the c u lle t a n d m ix in g th e carb on w ith it are co m p leted in on e

c o n tin u o u s o o p e r a tio n in a la r g e b all m ill d riven b y a 1 5 0 -h p . m o to r th ro u g h a sile n t ch a in d riv e. A b a tc h -w a y fe e d e r c o n s is tin g o f a s m a ll s te e l h o p ­ p e r in sta lled o n sc a les a n d f e d fr o m the c u lle t bin d isc h a r g e s 1 5 0 lb. to the ball m ill th ro u g h a sc o o p fe e d e r a t in te rv a ls o f five m in u te s. T h e carb on is w e ig h ed m a n u a lly a n d f e d to the m ill in a r a tio o f le s s th a n 1 p e r ce n t o f the g la s s c h a r g e. T h e b a ll m ill it s e lf is a ste e l sh ell 8 f t . in d ia m eter by 1 4 f t . lo n g , lin e d w ith 4 to 5 in . o f b u h rsto n e. T e x a s flin t p eb b les a b o u t 2 in . in d ia m e ter a re u sed to g r in d th e m ix tu r e a s it tr a v e ls dow n th e le n g th o f th e m ill in a p e r io d o f a b o u t five h ou rs. A p p r o x im a te ly 95 p e r ce n t o f th e fin a l m ix w ill p a s s th rou gh a 325 m esh screen , th e la r g e r p a r tic le s b e in g r ecy cled f o r fu r th e r g r in d in g .

A f t e r g r in d in g , a n o th er b u ck et e le ­ v a to r p ic k s u p th e m ix ed b a tch a n d d isch a rg es it to a ste e l b a tch b in w h ere it is a v a ila b le f o r th e firin g o p e r a tio n . A v ib r a tin g fe e d e r c o n v e y s th e fin e ly p u lv er iz e d m ix tu r e to a u to m a tic w eig h sc a le s w h ich a re lo ca te d n e a r th e f u r ­ n a ce e n tra n ce. P a s s in g u n d er th e sc a les is a r o lle r c o n v e y o r b r in g in g m old s w h ich c a rr y th e c h a r g e th ro u g h the fu r n a c e . T h e m o ld s a re m a d e o f

¿ -in . s ta in le s s s te e l in tw o se c tio n s c o n ­ s is t in g o f u p p e r a n d lo w e r h a lv e s a n d are ta p e r ed in b o th w id th a n d le n g th to f a c ilit a te r e m o v in g th e b lo c k a f t e r firin g. E ach m old is a lso co a ted w ith a d e x tr in -k n n lin m ix tu r e to b eep the p o w d e red g la s s fr o m s tic k in g to it A b atch of ab ou t 10 lb. of the fin e ly ground cullet

an d carbon is m ea su red b y th e se autom atic w e ig h s c a le s, dropped into sta in le ss s te e l m olds an d fed

to the firing fu rn a ces

A fter firing for ap p ro x im a tely three hours, the b lock s a re "stripped"

from the m olds b y "strippers" and im m ed iately p la c e d in a n n e a l­

in g leh rs for a thirty hour h ea t treatment w h ich is c lo s e ly con ­ trolled b y instruments

C H E M I C A L & M E T A L L U R G I C A L E N G I N E E R I N G A U G U S T 1 9

9 9

(8)

w h en h ea ted . A c h a r g e o f a b o u t ten p o u n d s se e m s to j u s t a b o u t cover the b ottom o f th e m old , b u t p r o d u ce s a F o a m g la s b lo ck w h ich , a fte r trim m ing, m e a su r es 6 in . x 1 2 x 1 8 in.

CELLULATION

T h e fu r n a c e in to w h ich the ch arge is fe d o n a r o lle r d riv e is a b o u t CO ft.

lo n g a n d g a s-fired b y m ea n s o f 80 se p a r a te b u rn ers. T h is la r g e nu m ber o f b u rn ers is n e c e s sa r y to in su r e u n i­

fo r m ity o f te m p er a tu r e , on e o f the m o st im p o r ta n t p r o c es s c o n d itio n s.

E n te r in g th e fu r n a c e a t a tem p era tu re o f 1 ,2 5 0 d eg . P ., the g la s s a n d carbon m ix tu r e is su b je cte d to a co n tro lled th ree-h o u r h e a tin g . A s th e m o ld s p a s s s lo w ly th ro u g h th e fu r n a c e on ca st a llo y ro llers, th e te m p e r a tu r e is first in c re a se d to a m a x im u m o f a b o u t 1,550 d eg. F ., th en lo w ered a g a in to 1,150 d eg. F . n e a r th e p o in t o f d isch a rg e.

A s p e c ia l d ev ice a u to m a tic a lly co n ­ tro lled b y p h o to e le c tr ic c e lls c om es in to p la y h ere a n d su b je c ts th e m old to a te m p er a tu r e o f 1,350 d eg . F . f o r th ree m in u te s b e fo r e r in g in g a b ell to n o t if y th e o p e r a to r th a t th e m old is r ea d y f o r r em o v a l fro m th e fu r n a c e . T h is final b o o st in te m p er a tu r e c a u se s the s ta in le s s ste e l to e x p a n d s lig h t ly and se p a r a te fr o m the F o a m g la s w h ich h a s n o w b low n u p to fill the m old . A t th is p o in t th e F o a m g la s B lo c k c lo s e ly r e ­ sem b les a b la ck m a ss o f fo a m , a n d its d e n s ity h as c h a n g e d fro m a b o u t 5 0 lb.

p e r c u .ft. to 1 0 lb. p e r c u .ft.

T h e m o ld s a re m o v ed o u t o f the fu r n a c e on r o lle r s to th e o p e r a to r s, or

“ s tr ip p e r s ,” w h o a re r e a d y w ith a sb es­

to s g lo v e s to “s tr ip th e m o ld s” and

Physical Properties of PC Foam glas

S p ecific'G rav ity ... 0.17 (10 to 11 lb.

p er C u. F t.) K (C o n d u ctiv ity a t 70°F .)____ 0.45 B .t .u ./ H r ./

S q .f t./° F ./I n . K (C o n d u ctiv ity a t 300“F .) .. . 0.70 B .t .u ./ H r ./

, S q .f t./° F ./In .

Coefficient of

E xpansion (°F.) ...0000046 Specific H e a t ... 16 to .19 B .t.u.

p e r lb. p e r °F.

C rushing S tre n g th ... 150 lb. p e r sq. in.

M odulus of R u p tu re ... 90 lb. p er sq. in.

Im p a c t S tren g th (C en ter D ro p -in crem en t m ethod, on 8* x 1 0 ' x y th ic k specim ens

su p p o rte d on a 1 2 ' s p a n ) 66 f t.—lb.

A bsorption (24 H r. Im m ersion

in W a te r )... 0.4% b y Volume—

2% b y W eight (All a t surfaces) Air In filtratio n or

P e rm e a b ility ... 0 C a p illa rity ... 0 Volume Change w ith

M o istu re ... ... 0 Standard Sixes and Packing

Pieces p e r A pproxim ate G lass size carto n w eig h t P er carto n 12 x IS x ...2 ... 12 3S.0 lb.

1 2 x 1 3 x 3 ... S 37.51b.

12 x IS x ... 6 41.3 1b.

12 x IS x 6 ... 4 37.01b.

A v ie w of the n e w F o a m g la s p la n t at Port A lle g a n y , P en n a . T y p ica l of g la s s plant construction is the h u g e monitor w h ic h p ro v id es ven tilation lor the hotter parts in the b u ildin g. A lso in e v id e n c e are the w a lls of

g la s s b lock s m a d e in the ad ja c en t plant

p la c e the block s in a leh r f o r a n n e a l­

in g . D o o rs and ro llers on fu r n a c e s and leh rs are c o n tro lled b y p u sh b u tto n s c o n v e n ien tly lo ca ted n e a r the o p e ra to rs.

T h e str ip p e d m old s are p la c ed on a ro ller c o n v ey o r and carried back to the lo a d in g sc a les via a s p r a y b ooth . In th is booth each m old is th o r o u g h ly c lea n ed and s p r a y e d w ith th e d ex tr in - k a o lin m ix tu re describ ed above. To p r o te c t the o p e r a to r o f th e sp r a y a p p a r a tu s fro m fu r n a c e r a d ia tio n an in s u la tin g w a ll o f F o a m g la s b lo ck has b een in sta lle d b etw een th e fu r n a c e and s p r a y booth.

ANNEALING THE BLOCKS A n n e a lin g F o a m g la s block s is a c­

co m p lish ed in gas-fired r e c ir c u la tin g leh rs 1 1 0 f t . lo n g an d o f a h ig h ly s p e c ia l d e sig n . On a ste el w ire b elt 1 0 f t . w id e, tw e lv e block s u p o n end a re ca rried a b r e a st th ro u g h a tem ­ p e r a tu r e g r a d ie n t fr o m 1,0 5 0 d eg . F . to 1 2 5 d eg. F . T h e tim e req uired f o r a n n e a lin g v a r ie s, o f cou rse, w ith th e th ic k n e ss o f th e sla b s a n d th e ra te o f co o lin g , w ith a m a x im u m cycle, u n d er p r e s e n t o p e r a tin g co n d itio n s, o f a b o u t 30 h ou rs. One o u tsta n d in g p o in t in th e d esig n o f th e leh rs is the 2 6 -in . fr e e tu n n el h e ig h t w h ich is u n u s u a lly la r g e f o r th e g la s s in d u str y a n d g iv e s g r e a tly in crea sed ca p a c ity . G en er a lly , th e d ifficu lty o f m a in ta in in g u n ifo r m te m p er a tu r e a t a ll p o in ts in th e e n tir e e ro ss-se etio n o f the leh r n e c e s sita te s k e e p in g th e tu n n el h e ig h t to a c o n sid e r a b ly sm a ller d im en sion .

FINISHING A ND PACKOUT A n n e a le d r o u g h b lock s o f F o a m g la s fro m th e leh rs a re m a n u a lly loaded

o n to sk id p la tfo r m s or tr a v e lin g c o n ­ v e y o r s f o r d e liv e r y to th e fin a l trim ­ m in g m ach in es. H e r e each block is in d iv id u a lly c u t a n d sh a p e d , first in a fa c e trim m er a n d th en a n e d g e tr im ­ m er. T h ese trim m ers cu t the b lock s by m ea n s o f r o ta tin g w h eels, th e fa ce trim m er b e in g e q u ip p e d w ith two 3 6 -in . ste el-c en ter e d carb oru ndum w h eels. T h e b a se s iz e o f th e blocks is 6 in . x 1 2 in . x 18 in ., h u t th e y are e a s ily slic e d o n a h a n d sa w to p ro d u ce les se r th ic k n e ss e s su ch a s in ., 3 in.

o r 2 in. S ta n d a r d card b oard cartons are u sed to p a c k th e fin a l p ro d u ct fo r s h ip m e n t a f t e r an in s p e c tio n o f each b lock h a s b een m ade.

T a ilin g s fr o m th e trim m in g and s lic in g o p e r a tio n s a re ca rried a w a y on a c o n v e y o r b elt to a s tir r u p cru sher in a p it b elo w floor lev e l a n d th en d is­

ch a rg ed in to a h o p p e r . W h e n the h o p p e r is filled , a m o n o r a il a n d trolley h o ist rem o v e i t to a d u m p o u ts id e the b u ild in g . A s y e t th ese t a ilin g s have n o t been p u t hack in to th e p ro cess.

VENTILATION

T y p ic a l o f g la s s p la n t co n stru ctio n is th e h u g e m o n ito r v e n tila to r above th ose p a r ts o f th e p la n t w h ere m ost o f th e h e a t is c o n c en tra te d in p ro ces­

s in g . I n a d d itio n , a m o d ern d u st col­

lec to r s y s tem k e e p s th e e n tire p lan t e ffe c tiv e ly clea n a n d f r e e fr o m dust in s p it e o f th e f a c t th a t se v e ra l very d u s ty o p e r a tio n s a re p e r fo rm e d . A n etw o rk o f d u e ts c o n n e c ts th e sp r a y booth, a u to m a tic w e ig h m a ch in e and trim m in g m a c h in e s w ith a la r g e bag- t v p e d u st c o llecto r. T b s d u st from th is c o lle c to r is d isp o se d o f in the sa m e m a n n er a s th e ta ilin g s fro m the tr im m in g m ach in es.

1 0 0

A U G U S T 19,'fS . C H E M I C A L & M E T A L L U R G I C A L E N G I N E E R I N G

(9)

Taken from the leh rs after a n n e a lin g , the rough b lock s are lo a d e d onto sk id platform s or tra v ellin g c o n v e y o r s for d e liv e r y to the fin a l trimming m a ch in e s. Lehrs are the recirculating ty p e sp e c ia lly d e sig n e d to g iv e a

26-in. free tunnel h eig h t thus provid in g g rea ter c a p a c ity

PROPERTIES

S a w s or a n y o th er o r d in a r y c u ttin g tool a re p e r f e c t ly s a tis fa c to r y fo r sh a p in g o r fittin g F o a m g la s blocks fo r in s ta lla tio n , a n d a sim p le a sp h a lt- eem en t m ix tu r e a p p lie d b etw een b lock s p r o v id e s a b o n d th a t is se cu r e and d u ra b le. T he in o r g a n ic n a tu re o f cel- lu la te d g la s s p r e clu d es th e p o s s ib ility o f a tta ck b y verm in and a lso p r o v id e s

C H E M I C A L & M E T A L L U R G I C A L E N G I N E E R I N G . A U G U S T 1 9 1 /S .

r es is ta n c e to a c id a tm o sp h e re s a nd o th e r c o rr o siv e m a ter ia ls . F o a m g la s is n o t o n ly n o n -co m b u stib le , b u t a lso a c ts a s a fire reta r d a n t, an im p o r ta n t fa c to r w h en it is to be u sed in co m ­ b in a tio n w ith c o m b u stib le m a ter ia l. I t s h e a t c o n d u c tiv ity , w h ich a t 70 d eg . F . is 0.45 B .t .u . / h r ./ s q .f t ./ d e g . F . / i n . , a n d a t 300 d eg . F ., 0.70, w ill n o t ch a n g e in s p ite o f th e p r e se n c e o f a n y a m o u n t o f m o istu e . O b v io u sly , th e r efo r e, in c a se s w h ere w a te r o r d a m p n e ss a c t to n u llif y th e in s u la tin g v a lu e o f o th er m a ter ia ls, F o a m g la s w ill p r o v e a boon to in d u str y .

T h e sp ec ific h e a t o f F o a m g la s ra n g es fr o m .16 to .1 0 B .t.u . p e r lb.

p e r d eg. F ., w h ile its co efficien t o f e x ­ p a n sio n (d o g . F .) is .0 0 0 0 0 4 6 . O n the o p p o s ite p a g e is a ta b le o f th e p h y ­ s ic a l p r o p e r tie s o f P C F o a m g la s g i v ­ in g c o m p lete d e ta ils w h ich sh o u ld be o f in te r e st to en g in e er s w h o d e sig n an d in sta ll in su la tio n o f a n y k in d . T h e siz e s c u rren tly a v a ila b le are a lso listed .

Left— F o a m g la s b lock in a n e d g e trimmer.

Rough blocks a s th e y com e from the lehrs h a v e u n ev en fa c e s an d ta p e red e d g e s w h ich must b e sq u a red off in fa c e trim­

m ers an d e d g e trimmers. The fin a l product a s sh o w n after trimming is a p er­

fect block 6 in. x 12 in. x 18 in.

B elow — Tem perature control a n d r e g u la ­ tion is centered in a g la ss -e n c lo se d room cen trally lo ca ted in the p la n t. H ere a battery of recorder controllers operate, the furnaces an d leh rs a n d forem en chart

variou s tem peratures in the p ro cess CONTROL

C en tra lly lo ca ted b etw een th e ro w s o f fu r n a c e s a n d leh rs is a n elev a ted g la ss-in c lo se d co n tr o l ro o m in su la ted w ith F o a m g la s . H e r e a r e in sta lle d v a r io u s record er co n tr o ller s f o r the g a s b u rn ers on each fu r n a c e a n d lehr.

N u m er o u s a d d itio n a l te m p e r a tu r e s are read on a n in d ic a tin g p y r o m e te r by m ea n s o f a se lec to r sw itch a n d p lo ts a r e m ad e o f th e tem p era tu re o f the F o a m g la s b lock s a s th ey m o v e th ro u g h th e leh rs. T h e se p erm a n en t reco rd s a d v ise each s h if t fo r em a n o f w h a t h as h a p p e n e d on th e p r e v io u s s h if t , and a lso p r o v id e in fo r m a tio n w h ich is in ­ v a lu a b le in q u a lity co n tr o l w ork. B y lo c a tin g this room c en tr a lly a b o v e the o p e r a tin g floor, a g o o d v ie w o f the e n tire p la n t is o b ta in ed , a n d a co n ­ sid e r a b le m a teria l s a v in g w a s m a d e in th e in itia l in s ta lla tio n o f le a d w ir e f o r the th erm o co u p les. T h e c o m p a n y ’s r esea rch a n d f a c to r y co n tr o l la b o r a ­ to r ie s a re h o u sed in a s e p a r a te b u ild ­ in g n ea rb y . A c o m p r eh en siv e p r o ­ g ra m o f fu r th e r resea rch on c ellu la r g la s s is u n d erw a y , d irected tow ard 'fin d in g n ew w a y s to m ak e th is u n iq u e p r o d u ct, a n d th e s o lu tio n o f th e p r o b ­ lem s c o n n ected w ith the p r o p e r a p p li­

ca tio n o f th e m a ter ia l to the m a n y co m m e rcia l u ses a lre a d y en cou n tered .

Cytaty

Powiązane dokumenty

In proportion al control, the final control valve position is determined by the temperature, which means that the rate o f valve movement is proportion al to

Special m ilitary requirements, dopes for the aviation industry, and lend-lease are given as reasons for the large increase in demand fo r butyl alcohol.. On the

Pumps designed es- ent from the data in the last two pecially for handling hot liquids, or columns of Table I I I that the pump liquids of high vapor

The lam inated resins serve m any purposes.. CHEMICAL & METALLURGICAL

After the outbreak of the war, the United States and Great Britain became the main suppliers of chemicals; at the same time Brazil started her own chemical

Over a period of years, chemical industry has established a fine record in the face of serious fire and explosion hazards th at are inherent in its processes

It is our firm conclusion that present processes for manufacturing synthetic rubber and the raw materials required (butadiene and styrene) must not at this late

Fortunately much of the equipment th a t is in contact with brine becomes coated with a calcium sulphate scale... However, the Armistice terminated operation o f