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2 O JUN11968

CoA NOTE MAT. No. 18

^o2i> HS DELFT

.^^i?.-'

THE C O L L E G E OF A E R O N A U T I C S

C R A N F I E L D

THE DESIGN AND CONSTRUCTION OF A WELD H E A T - A F F E C T E D ZONE SIMULATOR

by

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CoA Note Mat. No, l 8 February_^_1968

THE COLLEGE OF AERONAUTICS DEPARTMENT OF MATERIALS

The d e s i g n and c o n s t r u c t i o n of a weld h e a t - a f f e c t e d zone s i m u l a t o r

b y

-T . E . C l i f t o n and M . J . George

S_U_M_M A R Y

I n v e s t i g a t i o n of t h e s t r u c t u r e and p r o p e r t i e s of the h e a t - a f f e c t e d zones i n welded j o i n t s i s u s u a l l y l i m i t e d by t h e i r s m a l l s i z e and t h e i r c o m p l e x i t y . One method of overcoming t h i s problem i s to s i m u l a t e t h e s t r u c t u r e a t a

p a r t i c u l a r p o i n t i n t h e h e a t - a f f e c t e d zone i n a specimen of l a r g e r s i z e by imposing on i t t h e t h e r m a l c y c l e s u s t a i n e d a t t h a t p o i n t .

The eqiiipment d e s c r i b e d i n t h i s n o t e u s e s a . c . r e s i s t a n c e h e a t i n g and w a t e r c o o l i n g to impose t h e r m a l c y c l e s on 2-5" x O.V x O.k" s p e c i m e n s , the

t h e r m a l c y c l e b e i n g chosen by a d j u s t m e n t of a bank of v a r i a b l e r e s i s t o r s t o c o n s t r u c t a v o l t a g e a n a l o g u e . C o n t r o l of specimen t e m p e r a t u r e i s a c h i e v e d u s i n g a t h y r i s t o r and two i g n i t r o n s t o c o n t i o l the i n p u t a t ^^i-OV. t o a

welding t r a n s f o r m e r . Feedback i s a p p l i e d from a thermocouple welded t o the specimen h o t - z o n e . The e q u i p n e n t h a s been shown t o produce the d e s i r e d t h e r m a l c y c l e s i n a r e p r o d u c i b l e manner.

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Summary

Introduction

The general principles of the design

The specimen grips

The control circuit

Assessment of simulator performance

Further applications of the simulator

Appendix

Acknowledgement s R e f e r e n c e s

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1

-Introduction

As welding techniques become more and more refined, and welded s t r u c t u r e s are put i n t o service in applications which demand increasing degrees of r e l i a b i l i t y e . g . n a t u r a l gas p i p e l i n e s , nuclear engineering, i t i s important t h a t a l l p o s s i b l e techniques should be used t o increase our understanding of the factors underlying s a t i s f a c t o r y welded-joint performance.

A welded j o i n t contains zones which have had widely differing

thermal h i s t o r i e s , and which may show, t h e r e f o r e , very d i f f e r e n t mechanical p r o p e r t i e s . Three major zones e x i s t :

-i ) The weld metal, wh-ich has been -in the molten s t a t e , and wh-ich shows the general c h a r a c t e r i s t i c s of cast m a t e r i a l ;

i i ) The parent m a t e r i a l , with microstructure and p r o p e r t i e s t o t a l l y unaffected by the heating sustained during welding;

i i i ) The h e a t - a f f e c t e d zone, which l i e s between the fusion boixndary on one side and the unaffected parent metal on the o t h e r . Figure 1 shows these zones in a section taken through a butt-weld.

The heat-affected zone m a t e r i a l generally forms a very small p a r t of a welded structure as a whole, but may decide the o v e r a l l perfoimance of the

s t r u c t u r e , on a 'weal:est-link' b a s i s . Many welded s t r u c t u r e s have f a i l e d , u s u a l l y with expensive r e s i o l t s , because of the effect of the welding process on the immediately adjacent m a t e r i a l i . e . the heat-affected zone, which led t o a l o c a l reduction i n d u c t i l i t y and f r a c t u r e toughness, and allowed easy propagation of f r a c t u r e s o r i g i n a t i n g a t some welding or m a t e r i a l d e f e c t . For t h i s reason, the i n t e g r i t y of an e n t i r e welded s t r u c t u r e may depend on

the production, in the HAZ, of s a t i s f a c t o r y mechanical p r o p e r t i e s by c o n t r o l l i n g the m i c r o s t r u c t u r e . In order t o do t h i s , however, one must know:

-a) the s t r u c t u r e and p r o p e r t i e s of the HAZ in a p a r t i c u l a r m a t e r i a l , and b) which structuTes w i l l be unacceptable, and how they may be modified, far

insteince, by weld pre-heat or post-heat treatment

Much of the i n v e s t i g a t i o n a l work on the common s t r u c t u r a l s t e e l s i s of an ad-hoc n a t u r e , designed e i t h e r to e s t a b l i s h a s a t i s f a c t o r y welding procedure or to solve some p a r t i c \ i l a r f a b r i c a t i o n problan, and there i s a need for longer-term i n v e s t i g a t i o n s i n t o t h e behaviour of even the best-known s t r u c t u r a l s t e e l s , to gain an understanding of the h e a t - a f f e c t e d zones.

However the h e a t a f f e c t e d zones axe usually only of the order of m i l l i -metres in width, and are completely inhanogeneous i n n a t u r e , since the thermal cycles sustained change continually across the width of the heat-affected zone. For these reasons, i t i s not l e a s i b l e to cut t e s t - p i e c e s for the usual

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mechanical t e s t s d i r e c t l y from a HAZ, although hardness surveys are

frequently c a r r i e d o u t , and notch toughness specimens have been cut t r a n s -versely from welded j o i n t s . Notches placed a t increasing distances from the weld fusion boundary give information on changes in impact toughness across the HAZ (l). However, these techniques a r e of limii:ed v a l u e .

A l t e r n a t i v e l y , we can aim to produce, in specimens l a r g e enough to allow conventional mechanical t e s t i n g , equivalent m i c r o s t r u c t u r e s , and hence mechanical p r o p e r t i e s , to those obtaining a t specific p o s i t i o n s

inside the HAZ, by Imposing the same thermal cycles sustained during welding. This note describes the design and construction of equipment to c a r r y out

such simulation.

Figure 2 shows the thermal cycles sustained a t various distances from the fusion boundary in a weld of 77>000 j / i n . heat input in -^f^' thick p l a t e , with no p r e - h e a t . The cycles were obtained by means of thermocouples

flash-welded i n t o p o s i t i o n p r i o r t o welding. The main feature i s a rapid r i s e to a peak temperature, which i s a function of distance from the fusion boundary, followed by cooling t o room temperature at an exponentially declining r a t e . In considering the v i s i b l e HAZ in s t e e l s , as shown i n Figure 1, we are concerned with peak tanperatures in t h e approximate range 7OO°-1500°C.

However, there appears t o e x i s t , outtide the v i s i b l e HAZ, a region of low d u c t i l i t y in which thermal s t r e s s i n g beyond the y i e l d p o i n t , at temperatures of around 100°-500''C, has produced s t r a i n ageing ( 2 ) , and which should

properly be included within the term' heat-affected zone' .

The peak temperature achieved, and the r a t e s of heating and cooling,

vary widely in welding as a whole, and are controlled by such process v a r i a b l e s as the type of welding process used, the heat input per inch of weld, the

p l a t e thickness and the degree of pre-heat used. In a d d i t i o n , there i s a r a p i d drop in peak temperature and heating and cooling r a t e s , as the distance from the fusion boundary increases (Figure 5 )

-Tne p r o p e r t i e s of the HAZ produced by a weld run a r e affected by the heating from subsequent r u n s , in a multi-run weld, and by any post-weld h e a t - t r e a t m e n t . In g e n e r a l , the effects of both of these are b e n e f i c i a l . The general p r i n c i p l e s of the design

In order to impose thermal cycles of the type shown in Figure 2, the prime requirement was the supply and a b s t r a c t i o n of large amounts of heat t o the specimen, i n a short time and in a c o n t r o l l e d fashion,

Tv/o p o s s i b l e methods of heating were high frequency induction heating and r e s i s t a n c e h e a t i n g . Induction heating at the necessary r a t e s would be d i f f i c u l t , and the well-kno^m h / f skin-heating effect could produce inhomogeneous temperature d i s t r i b u t i o n s w i t h i n the specimen. In a d d i t i o n , the c a p i t a l cost of heating equipment would be r e l a t i v e l y high. Neverthe-l e s s , h / f induction h e a t i n g was used for at Neverthe-l e a s t one HAZ simuNeverthe-lator ( 5 ) .

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5

-D.C. r e s i s t a n c e heating would be i d e a l in providing uniform heating a t the necessary r a t e s but the provision of the necessary power at low

impedance i s a considerable problem. A.C. r e s i s t a n c e h e a t i n g , using a welding transformer as an impedance converter, i s a ready source of the necessary power, although i t has the drawbacks of skin-heating e f f e c t s , the s e v e r i t y of which v a r i e s with temperature and heating r a t e s , and the p o s s i b i l i t y of i n t e r f e r e n c e , produced by the l a r g e a . c . f i e l d s , in the operation of e x t e r n a l c i r c u i t s , n e c e s s i t a t i n g shielding p r e c a u t i o n s .

However, low frequency a . c . heating has been used with success in developing other HAZ simulators (6,7) and t h i s technique was chosen for the present work.

Cooling was achieved by c i r c u l a t i n g water, a t f u l l mains pressiire, through copper specimen g r i p s , ensuilng t h a t the n a t u r a l cooling r a t e , i . e . in the absence of any h e a t i n g , was i n excess of those necessary f x simiilation of the required thermal cycles, so that control of the cooling r a t e could be maintained by a v a r i a b l e amount of heat input to t h e specimen during c o o l i n g .

The general design requirements w e r e :

-i ) a heat -input v a r -i a b l e over a w-ide range dur-ing the cycle; i i ) accurate control of heating and cooling r a t e s ;

i i i ) maximum r e p r o d u c i b i l i t y between successive runs a t a given s e t t i n g of the c o n t r o l s ;

iv) easy v a r i a t i o n of the demand c y c l e , with a minimum of readjustment; v) a record of the tsnperature cycle imposed on each specimen, as a check

on accuracy and r e p r o d u c i b i l i t y of the thermal c y c l e .

The specimen i s O.k" square by 2.5" long, l a r g e enough to allow a Charpy impact specimen or a small t e n s i l e specimen t o be machined from i t , a f t e r h e a t -treatment. The h e a t - t r e a t e d voliome i s approximately a O.V cube in the

specimen c e n t r e . Heating and cooling r a t e s were more l i k e l y t o be unifoim in a cube-shaped element.

3 . The specimen g r i p s

The specimen g r i p s c o n s i s t of four 2" x 2" x IT'/Q copper blocks, through which water i s c i r c u l a t e d at f u l l mains pressure . Each end of the specimen

i s gripped between two blocks by means of four 5/16" b o l t s (Figure k). In e a r l y t r i a l s , i t was found üiat the r e s i s t a n c e across the specimen grips

affected the peak temperature achieved a t a given control s e t t i n g , giving poor specimen-to-specimen repix)ducibility. To standardize r e s i s t a n c e as far as p o s s i b l e , soft aluminium packing pieces are used on each face of the specimen

in contact with a copper block, and the b o l t s a r e tightened t o 50 l b s - i n s . by means of a torque wrencn.

The copper blocks are moionted on a 1^/e" thick Tufnol block, backed with ^/e" s t e e l p l a t e to r e s t r a i n the thermal expansion of t h e specimen dialing c y c l i n g .

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This approximates, to some e x t e n t , at l e a s t , to the r e s t r a i n t on the HAZ i n an a c t u a l weld j o i n t .

Connections to the transformer were made as short and thick as

p o s s i b l e (l-g-" x l" x 5" long) to minimise the voltage drop. The voltage across the transformer output terminals i s kY. approx. and across the specimen grips 1.5 V. approx. Current taken during t h e heating portion of the cycle may be as higli as 15,000 A.

A modification t o t h i s arrangement was made during work on the effect of v a r i a t i o n i n r e s t r a i n t (U), in which one end of the specimen was allowed to move during expansion and contraction. One p a i r of blocks was mounted on a b a l l - b e a r i n g s l i d e and the power fed in via f l e x i b l e connections. k. The control c i r c u i t

B a s i c a l l y , the control c i r c u i t continually compares the specimen temperature, measured by a thermocouple, with the required thermal cycle, as given by a function generator. The p o l a r i s e d e r r o r s i g n a l thus obtained

i s used to control the heat input to t h e specimen.

This c o n t r o l c i r c u i t nay be considered in two s e c t i o n s : -a) The function generator and conparison network

I t was necessary to generate a voltage analogue of the required temperature c y c l e , which was then compared continuously with the e.m.f. produced by the thermocouple attached t o the specimen, i . e . with the specimen temperature. As the development of the simulator progressed, t h i s was achieved in three

d i f f e r e n t ways.

O r i g i n a l l y , a cam, obtained by p l o t t i n g the chosen experimental time-teniperature curve i n a polar fashion, was r o t a t e d through 560°C, at the correct constant speed. By connecting a cam follower to the wiper of a 10 KÜ l i n e a r potentiometer and using a s u i t a b l e voltage supply across the potentiometer, a voltage-time r e l a t i o n s h i p matching the desired temperature-time curve was produced. Owing to mechanical problems, such as backlash, and the labour of constructing t h e l a r g e number of cams required, t h i s method was eventually superseded. Correction of e r r o r s occurring in cycles with

rapid heating r a t e s (discussed l a t e r ) required on-the-spot ' t r i a l and e r r o r ' modifications of the ceim shape, and t h i s d i f f i c u l t y contributed to the decision

t o discard t h i s method. However, the cam u n i t served s a t i s f a c t o r i l y as the function generator during one programme of research (k).

I t was replaced by a simpler function generator, i n which a s i n g l e - t u r n potentiometer with Jik t a p s , equally spaced over i t s r e s i s t a n c e range,was driven a t a constant speed over i t s 5to°C a r c . Tl^e potentiometer (A) i s shown

with the driving motor ( B ) , in Figure 5- A v a r i a b l e r e s i s t o r was connected i n s e r i e s with the potentiometer and a s t a b i l i s e d d . c . p o t e n t i a l connected as shown in Figure 8, By adjusting the tap to which the p o s i t i v e voltage

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5

-connection to the network i s made, and by adjusting the value of the s e r i e s r e s i s t o r , the shape of the output function can be varied with respect to the proportion of the cycle time occupied in r i s i n g t o the pealc, and the

magnitude of the f i n a l output v o l t a g e , r e s p e c t i v e l y . F u r t h e r , by modifying the t o t a l r e s i s t a n c e value at each tap p o s i t i o n , by s m t a b l e p a r a l l e l fixed-value r e s i s t o r s , the voltage-time function can be modified to produce a shape equivalent to that of the required experimental curve. Although t h i s i s constructed from a s e r i e s of s t r a i g h t l i n e s between adjacent tap p o s i t i o n s , a very s a t i s f a c t o r y approximation i s obtained. The method used to c a l c u l a t e the values of the p a r a l l e l r e s i s t o r s i s ^own in the Appendix.

The major drawback was in the s e l e c t i o n of s u i t a b l e fixed value r e s i s t o r s , together with the labour of constructing a r e s i s t o r bank for each demand

cycle r e q u i r e d . Adjustment of e r r o r s produced by high heating and cooling r a t e s , as b e f o r e , was also d i f f i c u l t . Accordingly, the equipment i n i t s l a t e s t form, on the r i g h t of Figure 6, contains a bank of m u l t i - t u r n potentiometers connected in p a r a l l e l wiüi the segments of the function generator potentiometer. During the l a t t e r p a r t of the c y c l e , the slope of the required fimction i s generally small, requiring p a r a l l e l r e s i s t o r s of low value. For t h i s reason, several of the p a r a l l e l potentiometers span two segments towards the end of the cycle . A diagram showing the lay-out of the p a r a l l e l potentiometers, giving t h e i r values and span i s given in the Appendix. Sockets have been provided t o enable fixed value r e s i s t o r s to be connected in s e r i e s with the f i r s t six h e l i c a l potentiometers, when the calculated r e s i s t a n c e i s outside the range of the potentiometer.

Taps 2 to 7 ^^^ connected t o the supply p o s i t i v e through a s i n g l e pole six-way switch (C in Figure 5) which allows the peak p o s i t i o n to be s e l e c t e d . In a d d i t i o n , the r o t a t i o n a l speed of the function generator can be adjusted, allowing the s e t t i n g - u p of a wide v a r i e t y of cycles on the s i n g l e apparatus.

The voltage analogous t o the specimen ten^ierature, i . e . the feedback s i g n a l required to close the l o o p , i s obtained by amplifying the voltage output from a fine Chromel-Alimie] thermocouple, capacitor-discharge welded on to the centre of the heated zone of t h e specimen.

The thermocouple output i s connected i n t o a single channel Graphispot r e c o r d e r , shown on the l e f t in Figure 6 , which, as well as producing a record of the temperature cycle sustained by the specimen, gives an output voltage proportional t o the pen displacement. This i s achieved by using a 10 IÖÏ

l i n e a r potentiometer mechanically connected across the scale of the instrument, with t h e wiper connected t o the pen c a r r i a g e . The voltage across the

potentiometer i s provided e x t e r n a l l y , and can be varied a s r e q u i r e d , providing a high-gain d . c . amplifier for the thermocouple e.m.f.

The supply voltages across the function generator and Graphispot potentiometers are chosen to give e r r o r voltages of the correct magnitude t o feed d i r e c t l y i n t o the heat control u n i t , and thus are a means of c o n t r o l l i n g the s e n s i t i v i t y of the h e a t i n g c i r c u i t to d e v i a t i o n s from the required temperature.

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b) The h e a t - c o n t r o l unit

The h e a t - c o n t r o l unit was designed to accept signal voltages betvreen zero v o l t e (maximum power) and +10 v o l t s (minimum power). As the error s i g n a l approaches zero, the demand w i l l be f o r decreasing power, therefore a datum s h i f t , provided by a s u i t a b l y - p o l a r i s e d fixed-value d . c . v o l t a g e , i s r e q u i r e d .

The u n i t was o r i g i n a l l y supplied as a modification of a commercial s p o t -welder control u n i t , but a f t e r u n s a t i s f a c t o r y performance and frequent

component f a i l u r e , i t was redesigned by the Instrumentation Section of ElectricEil Department, for whose help we are most g r a t e f u l . The u n i t is now performing s a t i s f a c t o r i l y .

As the method used in c o n t r o l l i n g the power to the primary of the welding transformer i s r e l e v a n t t o many control problems encountered in welding

techniques, the type of c i r c u i t employed w i l l be described more f u l l y . A c i r c u i t diagram showing d e t a i l s of the heat control unit i s shown in Figure

9-A 12 volt r . m . s . voltage in phase with the i g n i t i o n supply is full-wave r e c t i f i e d to g i v e , v i a a pulse forming network, comprising t r a n s i s t o r Tx and a s s o c i a t e d components, a pulse of 100 c . p . s . on the base of t r a n s i s t o r T3. T r a n s i s t o r T2 i s a constant current generator charging the O.kJ iiF capacitor

to give a voltage remip dependent upon the time constant of öie network. The current i s turned on with the i n i t i a t i o n contacts closed. Normally, Tx is turned on, cutting off T3, so t h a t a t tiie beginning of each h a l f - c y c l e , the action of Tx and T3 i s to discharge the c a p a c i t o r . Therefore, a ramp i s produced which i s r e s e t at the beginning of each h a l f - c y c l e . This ramp i s applied, v i a an e m i t t e r follower t o a Schmitt t r i g g e r network whose hold off b i a s i s a function of the control s i g n a l .

By t h i s means the t r i g g e r i s made t o operate at a time a f t e r the beginning of each ^ cycle depending upon the value of the control v o l t a g e . The Schmitt t r i g g e r p\ilse f i r e s a blocking o s c i l l a t o r , which produces the necessary f i r i n g pulse for the t h y r i s t o r .

kkO volts i s connected, via the routing diodes Dx, D2, D3 and D4, t o the appropriate i g n i t r o n i g n i t o r , through the s i n g l e t h y r i s t o r , the magnitude of the r . m . s . current to the transformer primary being determined by the time delay, as set by the d . c . control voltage ( e r r o r s i g n a l ) . The function of the Zener diode, in s e r i e s with the t h y r i s t o r , i s t o ensure t h a t the t h y r i s t o r current goes to z e r o , and thus e x t i n g u i s h e s , a t the end of each h a l f - c y c l e . This is necessary because of the inductive nature of the load, which produces phase s h i f t between load current and v o l t a g e , and would normally prevent e x t i n c t i o n a f t e r each h a l f - c y c l e . The c a p a c i t o r - r e s i s t o r combination in p a r a l l e l with the t h y r i s t o r i s designed as a t r a n s i e n t f i l t e r , t o prevent

spurious voltage spikes from f i r i n g the device.

The power supply to t h e mains transformer i s therefore controlled by two I g n i t r o n s , connected back-to-back, so t h a t each f i r e s on successive h a l f - c y c l e s

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-of the supply voltage. The action -of the h e a t - c o n t r o l u n i t i s t o vary the proportion of each h a l f - c y c l e over which the i g n i t r o n s w i l l f i r e , as the s i g n a l voltage v a r i e s i n the range 0 to lOV.

The temperature control of the specimen i s therefore b a s i c a l l y proportional i n c h a r a c t e r , since the amount of power applied i s a d i r e c t function of the deviation of the specimen temperature from the instantaneous demand v a l u e . Because of the complex feedback loop, there i s a tendency t o introduce a

time-lag i n t o the response of the system. Further, since the desired temperature i s constantly changing the effect of a time-lag i s to d i s t o r t the thermal cycle imposed on the specimen. Since the l a g i s g r e a t e s t at high heating r a t e s , the effects are seen most in the peak temperature region. The parameters of the cycle most affected are the r a t e of h e a t i n g , which w i l l be higher than that required, and the peak temperature, which w i l l be exceeded-This effect i s p a r t i a l l y overcome by a l t e r i n g the voltage across the Graphispot

and function-generator potentiometers u n t i l the peak temperat\Are is achieved. Since the time-lag v a r i e s throughout the cycle with change i n heating and

cooling r a t e s , the voltage adjustment which gives the correct peak temperature gives an e r r o r elsewhere, notably a droop in the curve a t lower temperatures towards the end of the cycle. When cams were used, t h i s was corrected by modifying the appropriate section by f i l i n g and in t h e l a t e r v e r s i o n s , using the s e r i e s variable r e s i s t o r to give dhe correct voltage at the end of the c y c l e . This can be simplified by adding a d e r i v a t i v e control term to t h e basic

p r o p o r t i o n a l term, t o give an autonatic c o r r e c t i o n of the s i g n a l voltage, with a maximum effect at high heating r a t e s and a minimum at the lower r a t e s towards the end of cycle. I t was fo\md, however, t h a t the magnitude of the d e r i v a t i v e component required to achieve control of the i n i t i a l heating r a t e was so l a r g e as t o introduce i n s t a b i l i t y i n the degree of control elsewhere in the cycle, p a r t i c u l a r l y very near to the peak p o s i t i o n , where the d e r i v a t i v e canponent

i s removed very r a p i d l y , producing an o v e r - r e a c t i o n of the control system and a double-pealc effect on the specimen thermal cycle.

Ad-hoc modification of the shape of the thermal c y c l e , by alteririg the p a r a l l e l r e s i s t o r v a l u e s , achieves the same r e s u l t in a r e l a t i v e l y short time, and t h i s method of adjusting the shape of the thermal cycle proved a viable p r o p o s i t i o n , in p r a c t i c e .

5. Assessment of simulator performance i ) Heat control u n i t

The modified heat control u n i t operated very s a t i s f a c t o r i l y during the t e s t period. Adjustment of the heating r a t e during the cycle occurred smoothly and there \iBie a general lack of any random f i r i n g by mains t r a n s i e n t s which was

a too-frequent occurrence with the o r i g i n a l u n i t . i i ) Accuracy of Control

This was d i f f i c u l t to a s s e s s q u a n t i t a t i v e l y during a continuously changing demand cycle, b u t on a q u a l i t a t i v e b a s i s , the degree of control appeared to be

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s u f f i c i e n t , where a true control s i t u a t i o n applied, e . g . if the p o t e n t i o -meter drive motor was h a l t e d during the cooling p e r i o d , the specimen was held a t a constant temperature, with no noticeable f l u c t u a t i o n on the Graphispot record. The response of the control c i r c u i t is adjustable by v a r i a t i o n of the voltages across the function generator and Graphispot potentiometers, and an optimum range of values l i e s j u s t below voltages a t which o v e r - r e a c t i o n occurs, giving 'hunting' of the temperature.

I f true control could be achieved a t a l l points on the thermal cycle, as would be the case with slow heating r a t e s , the voltages across the function generator and Graphispot potentiometers would be approximately equal. With the heating r a t e s encountered i n the cycles sho-^m i n Figure 2, up to around 600°C/Eecond, a small time-lag b u i l t up in the peak temperature region, giving a peak temperature higher than the required v a l u e . Correction was applied by making the voltage across the function generator lower than t h a t across the Graphispot potentiometer. This then introduced d i s t o r t i o n in the l a t t e r part of the curve, where t n i e control was achieved.

i i i ) Reproducibility

Successive demand cycles were found to be e s s e n t i a l l y i d e n t i c a l .

Specimen-to-specimen f l u c t u a t i o n s of the thermal cycle produced did, however, occur, although these were f e l t t o be due more t o such factors as inconsisten-cies i n specimen set-up or i n mains v o l t a g e , r a t h e r than t o deficiency of any p a r t of the control c i r c u i t .

Heating, p a r t i c u l a r l y in the early s t a g e s , was observed t o occur mainly due to i n t e r f a c i a l heating,which could obviously vary from one specimen to the n e x t , affecting the efficiency of heating during the c r i t i c a l and l e a s t -c o n t r o l l e d se-conds leading up to the peak value. Aluminium pa-cking pie-ces were necessary to give even e l e c t r i c a l contact between the specimen and the water cooled blocks, i n order to prevent sparking during periods of high h e a t i n g r a t e s . To s t a n d a r d i s e , as f a r as p o s s i b l e , i n t e r - f a c i a l c o n d i t i o n s ,

fresh packing pieces were used for each specimen, and ihe clamping nuts tightened evenly and to a constant 50 l b . i n . torque, using a torque wrench.

Applying these p r e c a u t i o n s , i t was possible to produce sets of specimens with e s s e n t i a l l y i d e n t i c a l thermal cycles. For i n s t a n c e , 24 specimens were produced having had the 940°C peak temperature cycle, with pealc temperatures lying within ± 25°C of 9l<-0°C. Twelve specimens in which the peak temperatures a l l lay within ± 10°C of t h a t required, i . e . within an error of ± 1$ were

s e l e c t e d f o r Charpy impact t e s t i n g .

Because of the l a r g e s c a t t e r in the Charpy t e s t , i t was most important t h a t , as near as was p o s s i b l e , the specimens were i d e n t i c a l . The specimens with l e s s accurate cycles were kept for l e s s demanding u s e s , such as t e n s i l e

t e s t i n g and metallography.

iv) Variation of demand cycle

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9

-analogue of the desired cycle can be calculated, using the method given

i n the Appendix. Since velocity feedback proved impractible, the d i s t o r t i o n produced with f a s t heating r a t e s was corrected by t r i a l - a n d - e r r o r modification of the p a r a l l e l r e s i s t o r s in the d i s t o r t e d region. This modification was akin to the modification of cam shapes which was necessary when the driven-cam function generator was in use {k), but was much e a s i e r to carry out.

Depending on the degree and extent of d i s t o r t i o n p r e s e n t , 1 - 2 hours was s u f f i c i e n t to give a s a t i s f a c t o r y f i t to the experimental curve. A

subsequent specimen production r a t e of about 10 minutes per specimen enables a set of 2k specimens to be produced in 1 - 1-|- worMng days, thus providing the raw m a t e r i a l for a considerably longer period of further work. Specimen-production time i s , t h e r e f o r e , a r e l a t i v e l y small f r a c t i o n of the t o t a l time of a research programme. Figures 10, 11 and 12 show the three uppermost curves of Figure 2 , together with the simulated thermal cycles.

6. Further a p p l i c a t i o n s of the simulator

Because of the high heating and cooling r a t e s a v a i l a b l e , the close temperature c o n t r o l , and the a b i l i t y t o programme a heat treatment c y c l e , the simulator can be used q u i t e generally as a heat-treatment f a c i l i t y .

In p a r t i c u l a r heat-treatments r e q u i r i n g continuous or discontinuous v a r i a t i o n of temperature are e a s i l y and quickl--' c a r r i e d out, making i t a very useful research t o o l . . During long heating p e r i o d s , decarburisation and oxidation are l i k e l y to occur. The enclosure of the specimen g r i p s i n a vacuum chamber, allowing treatment in vacuo or under c o n t r o l l e d atmosphere, i s a possible

f u r t h e r development.

With f=uitable modification of the specimen g r i p s , other techniques which might be employed a r e , a) high speed dilatometry, t o a s c e r t a i n the true t r a n s -formation temperatures applying to the heating and cooling r a t e s encountered i n HAZ thermal c y c l e s , and b) t e n s i l e t e s t i n g a t high temperatures.

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Appendix

Calculation of r e s i s t a n c e analogue

Figure Al represents the function generator (tapped potentiometer) without the p a r a l l e l r e s i s t o r s .

With Ex = E2 With wiper B at A

E3 = 0

With wiper B at T2 and wiper X at Ta E3 = Ex = E2

With wiper B at C and wiper X a t T2

E3 = Ex - E2 (Ta-C/rp J)) (T2C represents t o t a l r e s i s t a n c e ^ between point T2 and C).

Figure A2 shows a s e r i e s of curves representing output voltage E3 p l o t t e d against wiper B p o s i t i o n , for d i f f e r e n t connections of wiper X. A similar graph may be constructed with r e s i s t a n c e between A and B, figure Al, replacing voltage on the Y a x i s . Then by modifying the r e s i s t a n c e value at tap

p o s i t i o n s , throughout the whole range of the potentiometer, a curve of the desired shape can be constructed. The curve w i l l be constructed from a

s e r i e s of s t r a i g h t l i n e s between adjacent tap p o s i t i o n s , as shovrn i n Figure A5. The p o s i t i o n chosen for wiper X (Figure Al) w i l l depend upon the shape of the thermal cycle r e q u i r e d .

As a general r u l e , for slow heating r a t e s a high tap p o s i t i o n should be s e l e c t e d , and for high heating r a t e s , a low tap p o s i t i o n i s more advantageous.

Figure 3 shows t h a t for slov/ heating r a t e s , e s p e c i a l l y when the heating curve deviates markedly from a s t r a i g h t l i n e , a g r e a t e r number of segaents are needed t o simulate closely the desired function.

The speed of r o t a t i o n of the function generator should be selected to s a t i s f y the following conditions:

(a) The peak of the r e s i s t a n c e ciurve should f a l l as nearly as possible to a tap p o s i t i o n , ( e s p e c i a l l y important for higli heating r a t e s ) ,

(b) The time for a complete revolution should correspond to the cycle time for the thermal cycle r e q u i r e d .

Having selected a p o s i t i o n of wiper X and the cycle time of the function g e n e r a t o r , the experimental temperature cycle should be p l o t t e d t o t h e above

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11

-tirüe b a s e , marking on t h e X a x i s t h e p o s i t i o n s of t h e p o t e n t i o m e t e r s t a p s . The Y a x i s i s t h e n c o n v e r t e d from thermocouple o u t p u t t o r e s i s t a n c e , u s i n g a peak value of between 7OO and 80Cn, and e v a l u a t e the r e s i s t a n c e a t t a p p o s i t i o n s .

The r e s i s t a n c e of t h e f u n c t i o n g e n e r a t o r p o t e n t i c m e t e r i s 2ÖKfl which g i v e s a r e s i s t a n c e of 590f^ between a d j a c e n t t a p s . For t h e m a j o r i t y of e x p e r i m e n t a l curves a peak v a l u e of 700 - 80Cfi g i v e s p a r a l l e l r e s i s t a n c e s

which a r e r e a l , and f a l l w i t h i n t h e range of t h e h e l i c a l p o t e n t i o m e t e r s f i t t e d . F i g u r e A^l- i s a t y p i c a l t e m p e r a t u r e time c u r v e , and t h e p r o c e d u r e f o r

c a l c u l a t i o n of p a r a l l e l r e s i s t a n c e v a l u e s i s d e t a i l e d below.

The p o s i t i o n of the X w i p e r i n t h e example was chosen f o r t a p 3^ w i t h the peak t e m p e r a t u r e c o n v e r t e d t o 800fi.

The r e s i s t a n c e a t t a p 1 must t o t a l l+lOfi.

i . e . 590fi i n p a r a l l e l w i t h r e s i s t o r Rx, must equal klCQ 590Ri

= ij-10 Rx- 134Cf2 590fRx

The r e s i s t a n c e a t t a p 2 must t o t a l 70Cfi

i.e.-59Cf2 i n p a r a l l e l w i t h r e s i s t o r R2 i n s e r i e s w i t h 4l0fi must e q u a l 7OOD

^1° ^ Ü f c = ^ ° ° ^2 - 570n

S i m i l a r l y t h e r e s i s t a n c e a t t a p 3 must t o t a l 80Cfi

7^°

+

5 9 ^ ^

="

ö°°

^^ - ^ ^

C o n t i n u i n g from the peak t a p p o s i t i o n t h e p r o c e d u r e i s somewhat m o d i f i e d . The peak i s c a l l e d z e r o , t h e curve i s i n v e r t e d ( V o l t a g e E2 opposes Ex) and t h e p a r a l l e l r e s i s t a n c e c a l c u l a t e d a s b e f o r e .

Figure A5 shows the i n v e r t e d curve of t h e example shown i n Figvire Ak The r e s i s t a n c e a t t a p k must t o t a l 6Cf2 ( i . e . 800-7*4-0)

| g j - = 60 R . - 66.SO

S i m i l a r l y t h e r e s i s t a n c e a t t a p 5 must t o t a l 2200 (8OO-580)

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The value of the s e r i e s r e s i s t o r (CD in f i g . A.1) i s calculated as follows.

Total value of r e s i s t a n c e from peak p o s i t i o n to f i n i s h must equal the value from peak to s t a r t , which i s , in the example considered, 800fi.

Therefore: Value of s e r i e s r e s i s t o r = 800 - value a t f i n a l t a p . The t a b l e shows the value of each p a r a l l e l h e l i c a l potentiometer and

the relevant tap p o s i t i o n . Each potentiometer requires 10 complete revolutions to scan the t o t a l range and the turns i n d i c a t o r f i t t e d shows the precise

p o s i t i o n of the wiper.

Figure A6 shows the potentiometer layout on t h e front panel.

Towards the end of the cooling curve, where the slope i s small, p a r a l l e l r e s i s t o r s have been connected t o span, in some c a s e s , two segments.

This must be taken i n t o consideration i n the c a l c u l a t i o n s . The fixed value w i l l , i n these cases, be ll80fi instead of 590^ ,

Acknowledgements

The authors wish t o thank E. S i l l s and B. Moffat of the Instrimientation Section for advice and p r a c t i c a l a s s i s t a n c e i n the redesign of the heat control u n i t , and T. Biston of the Department of M a t e r i a l s , for carrying out the construction of t h e simulator.

References

1. A.C. de Koning I . I . W . Document IX-i)-71-65

2 . C.F. Tipper B r i t . Weld. J . , 1966, 13, P- k6l-k66, 3 . M.J. George Unpublished work, Cranfield, I966. k. M.D. Coward M.Sc. T h e s i s , London University, I967. 5. M. Inagaki et a l . Trans. Nat. Res. I n s t , Met. (Japan),

196k, 6, p . 39.

6. E.F. Nippes and W.F. Savage Weld. J., 19'49, 28, p. 534s.

7. E. Fletcher and D. Shaw Swinden Laboratories, United Steel Go's. Ltd., 1961. (Private Communication).

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F!G. 1. MACROGRAPH OF BUTT WELD SHOWING POSITION OF HEAT AFFECTED ZONES ( x 2 MAGNIFICATION).

1200 r IBO XID 90O 700 500 I X • 300 K»L Distance Fusion 1 - T / j , 2-Vc2 3-T/c3 t-Vc5 5-T/r,6 6 - f / c 8 from OOS" 0 0 7 ' o-ir 0-13-O K ' 0 2 9 ' 15 20 25 10 35 1.0 i5

FIGURE 2 . EXPERIMENTALLY DETERMINED THERMAL CYaES.

50 55 Tim« (Sees)

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o 1250 a. E 1000 E 750 X o 500 \

V

1 ^.

<

k

\ V • ^ v ^ ^****«'«^^^ ~ — ~» 250 O 3 6 9 12 15 18 Distance from Weld Fusion Boundary, mms.

FIG. 3 RELATIONSHIP BETWEEN PEAK TEMPERATURE AND

THE DISTANCE FROM THE FUSION BOUNDARY. REFERENCE 4

FIG. 4 SPECIMEN GRIP DESIGN AND THE POSITION OF THE FEEDBACK THERMOCOUPLE

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A - MULTI - TAP POTENTIOMETER. B - SYNCHRONOUS MOTOR.

C - PEAK - POSITION SELECTOR SWITCH.

FIG 5. - DETAILS OF THE FUNCTION GENERATOR.

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DC. ERROR MOTOR THYRISTOR CIRCUIT I ; I TRANSFORMER IGNITRONS DC. ^ RFCORDFR POTENTIOMETER TEMPERATURE FEEDBACK 1 1 1 1 SF 1 =ECIMEN

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vy^ •J^j)^ </\^-^vi^. s/^/f\/\/\^

/ v V w v A

PEAK POSITION Sa.ECTOR SWITCH

[ A A A A A A A A A A A / W V ^ A

-FEEDBACK LINEAR POTENTIOMETER

SERES RESISTOR AMPUTIJOÉ LMrTtNG NETWORK 10 TURN neucAL POTENTIOMETER - + 50 VOLTS , to TURN HEUCAL POTENTIOMETER O U T P U T T O H E A T U N I T [ E R R O R ]

FIG. 8. C I R C U I T DIAGRAM OF SIMULATOR.

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E 200 IOC O \L

-1

!\ ^ ( — \ \ 1 _- : i ! 1 1

1

1

^

S

k

• ^ ^ ï ^ ? * ^ EXPERIMENTAL SfMULATED

1

1 50 55 Tins Eacs)

FIG to. OWPARISOrJ OF EXPERIMENTAL AND SIMULATED CYaES.

50 55 Time (Sees) I IG, 11. COMPARISON OF EXPERIMENTAL AND SIMULATED CYaES.

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1200 1100 . 900 u s a 800 0 5 600 u 1 (00 300 200 no i J

T

' \ \ \ 1 N^ J l ! • 2C • ? ..,,,. : 3 ) - • •• -j r-—• T! Distance from Fusion Boundary 3 - " C 3 0 11" SIMUtATED 1 1 ! i • -3 ^ -J -J ! sh ?

- J

—a Tim* (Sees)

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E3 E l / ' / ' / ^ * y \ i / 1 / I / / { ^ i I / A / ' ' / ' / / I / I ' / 1/ / ' / I ' y / / I ' / / / / ' I I / / ' / / ' I ' / / / / I t ' / //y I I ' if/At - T - --} - -T h h T^ WIPER B POSITDN FIG. A 2. RESISTANCE i i TAP POSITION (WIPER B ) FIG A3.

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6 8 TAP POSITION FIG. fKL. RESBTANCE TAP POSITION FIG. A 5.

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® 1 0 0 ^ 5 G n ® 50 n. ® lOOü SOxi. @ 50X1 ® 100x1. Son.

0

5 0 i V ® 100-n. 50 .n. 5 0 J I ® 50-n. SOJX. ® 50SL SERtS ® 50X1. 50..n. ® 500 XL RESISTOR FIG. A6. L A Y O U T O F H E L I C A L P O T E N T I O M E T E R S HELICAL POIfNTIOMETER 1 2 3 i. 5 6 7 8 9 10 11 12 13 U 15 16 17 18 19 20 21 22 23 24 WOE SI 100 2000 2000 100 100 100 100 100 100 100 50 50 60 50 50 50 50 50 50 5 0 5 0 50 50 500 TAPS 1 - 2 2 - 3 3 -i 4 - 5 5 - 6 6 - 7 7 - 8 8 - 9 9 - 1 0 1 0 - 1 1 1 1 - 1 2 12 - 13 • 13-14 1 4 - 1 5 1 5 - 1 6 1 7 - 1 9 1 9 - 2 1 2 1 - 2 3 2 3 - 2 5 2 5 - 2 7 27 - 2 9 2 9 - 3 1 3 1 - 3 3 SERIES RESISTOR F I G . A 7 V A L U E S Oh^ H K l . i r A I , I ' O T E N I ' I O M E T K R . S AND T H E I R T A P PCJ.SITIONS

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