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Delft University of Technology

Void fraction measurements in partial cavitation regimes by X-ray computed tomography

Jahangir, Saad; Wagner, Evert C.; Mudde, Robert F.; Poelma, Christian

DOI

10.1016/j.ijmultiphaseflow.2019.103085

Publication date

2019

Document Version

Final published version

Published in

International Journal of Multiphase Flow

Citation (APA)

Jahangir, S., Wagner, E. C., Mudde, R. F., & Poelma, C. (2019). Void fraction measurements in partial

cavitation regimes by X-ray computed tomography. International Journal of Multiphase Flow, 120, [103085].

https://doi.org/10.1016/j.ijmultiphaseflow.2019.103085

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International Journal of Multiphase Flow 120 (2019) 103085

ContentslistsavailableatScienceDirect

International

Journal

of

Multiphase

Flow

journalhomepage:www.elsevier.com/locate/ijmulflow

Void

fraction

measurements

in

partial

cavitation

regimes

by

X-ray

computed

tomography

Saad

Jahangir

a

,

Evert

C.

Wagner

b

,

Robert

F.

Mudde

b

,

Christian

Poelma

a,∗ a Department of Process & Energy (Faculty 3mE), Delft University of Technology, Leeghwaterstraat 21, 2628 CA Delft, The Netherlands

b Department of Chemical Engineering (Faculty of Applied Sciences), Delft University of Technology, Van der Maasweg 9, 2629 HZ Delft, The Netherlands

a

r

t

i

c

l

e

i

n

f

o

Article history:

Received 29 November 2018 Revised 9 June 2019 Accepted 3 August 2019 Available online 7 August 2019

Keywords:

X-Ray computed tomography Cavitation

Venturi Multiphase flow

a

b

s

t

r

a

c

t

Cavitation isacomplicated multiphasephenomenon,where the productionofvapor cavities leadsto anopaqueflow.Exploringtheinternalstructuresofthe cavitatingflows isoneofthemostsignificant challengesinthisfieldofstudy.Whileitisnotpossibletovisualizetheinteriorofthecavitywithvisible light,weuseX-raycomputedtomographytoobtainthetime-averagedvoidfraction distributioninan axisymmetricconverging-divergingnozzle(’venturi’).Thistechniqueisbasedontheamountofenergy absorbedbythematerial,whichinturndependsonitsdensityandthickness.Usingthistechnique,two differentpartialcavitationmechanismsareexamined:there-entrantjetmechanismandthebubblyshock mechanism.3DreconstructionoftheX-rayimagesisused(i)todifferentiatebetweenvaporandliquid phase,(ii)toobtainradialgeometricfeaturesoftheflow,and(iii)toquantifythelocalvoidfraction.The voidfractiondownstreamoftheventuriinthebubblyshockmechanismisfoundtobemorethantwice comparedtothere-entrantjetmechanism.Theresultsshow thepresenceofintensecavitationatthe wallsoftheventuri.Moreover,thevaporphasemixeswiththeliquidphasedownstreamoftheventuri, resultingincloud-likecavitation.

© 2019ElsevierLtd.Allrightsreserved.

1. Introduction

Cavitationinaflowoccurswhenthestaticpressureintheflow fallsbelowthevaporpressureoftheliquid,resultinginthe forma-tionofvaporbubbles.Inmanyhydrodynamicapplications,suchas shippropellers,hydroturbinesordiesel injectors,cavitationoften cannotbeavoidedduetotheiroperatingconditions.Ifacavitation bubbleorcloudcollapsescloseenoughtoasolidwall,itwill pro-duceahigh-speedmicro-jetandshockwaves,whichcanresultin erosion(FrancandMichel,2006;DularandPetkovšek,2015;Peng etal.,2018).Understandingthecorrectcavitationphysicsis impor-tant because then the adverse consequences such aserosion can bediminished.

It is of great importance to understand the development and dynamics of local void fractions in cavitating flows. Among the studiesoncavitation,high-speedvisualizationisthemostpopular techniquetoinvestigatethecavitationevolution(Laberteauxetal., 1998;Chenetal.,2015).Simpleopticalmethodsarelimitedto in-vestigatingcavitation occurringclosetothewall region.However, quantitative informationregardingthevoidfractionsisdifficultto obtain from high-speed imaging, because the cavitation bubbles

Corresponding author.

E-mail address: C.Poelma@tudelft.nl (C. Poelma).

blockandscatterlightandthusmaketheflowopaque(Dashetal., 2018).Due tothelackofpenetrabilityofvisiblelightinsuch op-tically opaque flows, advanced alternative techniques have been developed over the years to quantitatively characterize the phe-nomenaoccurringintheinterioroftheflowandtoquantifyvoid fractions.Broadly,thesetechniquesincludeopticalprobes, Electri-cal CapacitanceTomography,Radioactive ParticleTracking,(X-ray/ Gamma ray) Computed Tomography (CT), Magnetic Resonance Imaging, with each technique having its advantages and limita-tions. Quantitative non-intrusive techniques have been reviewed inliterature (Chaouki et al., 1997; Kastengrenand Powell, 2014). Impedance tomography systems have been developed to investi-gate multiphase flows, and they are reviewedby Holder (2004). Impedancetomographysystemsarerelativelycheap,butsuch sys-temsarelimitedbythenumberofelectrodesthatcanbe located on the boundary. This limits the spatial resolution that can be achieved in the reconstruction. Gamma and X-ray imaging have beenusedtostudymultiphaseflows suchascavitatingflowsand bubblyflows.X-rayimaginghasbeendemonstrated asa valuable techniqueto quantify the void fractions in various cavitation re-latedstudies(Baueretal.,2012;Mäkiharjuetal.,2013;Mitroglou etal., 2016;Khlifaetal., 2017). Void fractionsare ofhigh impor-tancefortheunderstandingofsheddingbehaviorinperiodic cav-itation.Recently Ganeshet al.(2016) foundthat under particular

https://doi.org/10.1016/j.ijmultiphaseflow.2019.103085

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Fig. 1. Dimensionless frequency of the cavitation shedding cycle as a function of the cavitation number for the venturi, replotted from Jahangir et al. (2018) . The red arrows show the cavitation numbers selected for the CT reconstruction. (For interpretation of the references to colour in this figure legend, the reader is referred to the web version of this article.)

conditions a condensation shock can be the dominant mecha-nismforperiodiccavitationshedding,insteadofthere-entrantjet. Time-resolvedX-raydensitometrywasusedtoinvestigatethelocal voidfractions inthe flowfield.Theyfoundthat voidfractions in-creasewithanincrease incavitation intensity.Theseexperiments were performed on a 2D wedge. A converging-diverging nozzle (‘venturi’)is used inthisstudy.Due to itshigh contractionratio, abroader cavitation dynamicrangecanbe attained. However, by usingastandard 2DX-raydensitometry system,only information integratedalong linesof sightaboutthe voidfraction withinthe regionofinterest canbedetermined fromasingleviewingangle. Itisunlikely toobtaininformationregardingthestructuresinside thecavitation.

X-ray CT is widely used in medical imaging. It uses the re-lationbetween thematerial properties andthe attenuation coef-ficientof X-rays. Images are created using the attenuation along thebeampaths recordedatvarious viewingangles. This capabil-ity inspired the idea to use X-ray CT to measure the void frac-tion distribution andradial geometric characteristics in the flow.

Baueretal.(2012)didthefirststudytoinvestigateaninternal cav-itationalflow with theX-ray CT-scanner ona purpose-built noz-zle.Mitroglouetal.(2016)alsoperformedX-rayCTmeasurements onasmallerscalenozzle(D=3mm).Frombothofthesestudies, theobtainedtime-averagedCTimagesgaveusefulinsightsonthe flowstructuresinsidethenozzle.However,allthepreviousstudies whichinvestigated the internal cavitational flow were performed onnozzles,tothebestofauthorsknowledge.Usinganozzlewith aconstantdiameter,itisimpossibletoobtaindifferentpartial cav-itationregimes.

Jahangir et al. (2018) used a venturi in combination with high-speedvisualizationtodistinguishbetweentwopartial cavita-tionregimes:there-entrantjetmechanismandthebubblyshock mechanism.Theauthorsfurthershowedthatthenon-dimensional frequency(Strouhalnumber)canbeusedtoidentifythetwo par-tialcavitationregimes.TheStrouhalnumber(St)isdefinedas:

St= fD0

u0 ,

(1) where D0 is the throat diameter, the shedding frequency of the cavitation cloudsis givenby fand u0 is the free streamvelocity ofthe flow in the venturi throat.In Fig. 1, the Strouhal number (St) is shownasa function ofthe cavitation number. The

cavita-tionnumber(

σ

)isdefinedas:

σ

= p1− pv

2

ρ

u20

, (2)

wherepisthedownstreampressure,pv isthevaporpressure1 of

the liquid at the temperature of the setup and

ρ

is the density ofthe fluid.The sheddingfrequencywasdetermined using high-speedshadowgraphy.DetailscanbefoundinJahangiretal.(2018). The studyfoundthat all pointscollapsedon a singlecurve,with the shedding frequency being a function of cavitation number. Fromvisualinspectionoftheshadowgraphydatatakenforvarious cases inFig. 1,two different cavitation mechanisms were identi-fiedasafunctionofcavitationnumber:for

σ

>0.95cloud cavita-tionsheddingisgovernedbythere-entrantjet mechanism.For

σ

<0.75cloud cavitationsheddingisgovernedbythebubblyshock mechanism.Thecavitation regioninbetweenisgovernedbyboth mechanisms, so it is called the transition region. In this study, we will examine thevoid fractions usingX-ray CTin the above-mentionedregimesusingthesamegeometry(see alsoFig.2, dis-cussedindetaillater). Tothat end,one oftherepresentativecase from both the re-entrant jet mechanism and the bubbly shock mechanism will be used for the determination of void fractions. Acasewith thecavitation numberof

σ

=1 fromthere-entrant jet mechanism isselected andanother casewith

σ

= 0.40from thebubbly shockmechanismisselected (shownwithred arrows inFig.1).

TheadvantageoftheX-rayCTisthatitdoesnotonlymeasure thespatialaverage ofthe voidfractionlikeit wouldbe for stan-dardX-rayimaging,butthevoidfractiondistributionalong differ-entcross-sectionsof theventuri.The dataisessential tovalidate ourassumptionsregardingthephysicalmechanisms.Furthermore, itiscurrentlybeingusedtovalidatenumericalmodels.

The manuscriptisorganizedinthe followingmanner. The ex-perimentaldetails aredescribedinSection2,while Section3 ex-plains indetail thedataprocessing andmethodsused to explain the flow dynamics. The calibration and results are reported in

Section4.TheconclusionsfollowinSection5.

2. Experimentaldetails

2.1. Flowfacility

Aschematicoverviewoftheflow setuputilizedforthe exper-iments is represented inFig. 2. The flow in the closed-loop sys-tem is driven by a centrifugalpump, anda flowmeter (KROHNE flowmeter, type:IFS 4000F/6)is used to measurethe volumetric flow rate (Q). The measurements from the downstream pressure transducer (calculated from P3 in Fig. 2), the flowmeter, andthe temperaturesensorare usedto determinethecavitation number. Awatercolumnpresentatan angle(due tospaceconstraints) is used to collect the airbubbles entrained in the flow during de-gasification,and to varythe globalstatic pressureof the system. Avacuum pumpisused tocontrol the globalstaticpressure be-low ambientpressuredown to20kPa absolute. The experimental setup shown in Fig. 2 had to be reoriented for the X-ray imag-ingmeasurementscomparedtoshadowgraphymeasurements per-formedbyJahangiretal.(2018)duetospacerestrictionsofthe X-rayfacility.Therefore,theentrancelengthhadtobereducedfrom 40Dto10D.Nevertheless,theflows fromthetwoexperimentsfor the samecavitation number were confirmedto be equivalent, as thepressurelosscoefficientsacrosstheventuri(K) werealikefor bothcases(explainedinSection4).ThepressurelosscoefficientK

1 The vapor pressure is calculated using the Antoine equation at the temperature

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S. Jahangir, E.C. Wagner and R.F. Mudde et al. / International Journal of Multiphase Flow 120 (2019) 103085 3

Fig. 2. Schematic overview of the experimental facility indicating essential components (dimensions not to scale). The inset shows the geometry and relevant dimensions of the converging-diverging section.

isgivenby:

K= 1



p

2

ρ

u20

, (3)

where



pisthepressurelossovertheventuri(calculatedfromP1 andP2 inFig.2).Avisual examinationalsoestablishedsymmetry ofthetopandbottomhalvesofthetime-averagedshadowgraphy imagesbyplacingamirroratanangleof45◦ belowtheventuriin the horizontal configuration.The side-viewand the bottom-view werevisualizedsimultaneously,inordertoverifywhetherthe cav-itation dynamics are axisymmetric. No significant difference was found,thereforeeffectsduetogravitycanbeneglected.

In Fig. 2(inset), a picture of the venturi can be seen with its geometrical parameters. The venturi is milled out from a block of polymethylmethacrylate (PMMA) and has a throat di-ameter (D0) of 16.67mm. The convergence and divergence an-gles are 18◦ and 8◦ to the axis, respectively (inspired by pre-vious studies: Long et al. (2017), Hayashi and Sato (2014), and

Tomovetal.(2016)).Anarearatioof1:9(areaofthethroatversus exitarea)ischosen.Theflowdirectionisfrombottomtotopinthe venturi.Furtherdetailsontheexperimentalsetupcanbefoundin

Jahangiretal.(2018).

2.2. Experimentalprocedure

Avacuumpumpisutilizedtodegasifythewaterbeforethe ex-periments. A watersample istaken forthe determination ofthe gas content in the system using an oxygen sensor (RDO PRO-X Probe). After runningthe setup for60 minutesatlower ambient pressure withcavitation, the oxygen content reduces from over-saturated to approximately40%. All themeasurements were per-formedatapproximatelythesameoxygencontent.

Thesetup isrunfor5minutesbeforethe measurementseries isstarted,inordertomixthewaterinthesystemandtoobtaina uniformwatertemperature. Theglobalstaticpressureofthe sys-temisfixed ata prescribedvalue. The measurementsare started whenthe pressurereadingsare constant.Forthe specifiedglobal staticpressure,measurements areconductedatdifferentflow ve-locities.Adataacquisitionsystemisusedtorecordall thesensor values (pressure, flow rate, and temperature). X-ray images (ex-plainedin theupcoming paragraph) are recordedsimultaneously. Intheend,theoxygencontentismeasuredagainbytakinga wa-tersamplefromthesetup.

2.3.X-rayimaging

Inthis study,the cavitating flow inside theventuri was mea-suredusingX-rayimaging.TheX-raysetuporiginallyconsistedof three standard industrial type X-ray sources (Yxlon International GmbH)withamaximumenergyof150keVworkinginconebeam mode.Each X-raysource generates a conebeam that canbe de-tected by a detector plate on the opposite side of each X-ray source.Forthisstudy,theexperiments wereperformedwithone X-raysourceandonedetectorplatetoobtaintheprojected2D out-putsignalsfromthe3Dcavitatingflow.

Fig.3(a) and(b)showa photographofthemeasurement sec-tion in the X-ray setup and schematic overview of the method, respectively.Asource-detectorpairis usedtomeasure the atten-uation of the X-rays through the cavitating venturi. For the ex-periments, the venturi is placed (inclination ± 1mm/m) in the center of the setup and 323± 2mm from the X-ray source and 584± 2mmfromthedetectorplate. TheX-raysource(Yxlon-Y.TU 160-D06)hasatungstenanode.Thesourceisoperatedat120keV and5mA inorder toachieve a high contrastbetweenthe liquid

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Detector Measurement section Source Water + Vapor PMMA 3.6° Intensity 584 mm 70 mm 323 mm Detector Measurement section Source Water + Va V V por PMMA 3.6° Intensity 584 mm 70 mm 323 mm

Detector

Source

Measurement

secon

(b)

(a)

Fig. 3. The basic arrangement and components of the X-ray setup and the flow facility. (a) Test-rig inside the X-ray setup. (b) Schematic of the X-ray imaging method with the source on the left, the measurement section in the middle, and the detector on the right indicating the intensity (dimensions not to scale).

andvaporphaseswithintheventuri.Theflatdetector,Xineos-3131 CMOSmodel,consistsofa307× 302mm2 sensitivearea.The de-tectorprovidesthetotalphotoncountintherangeof40–120keV. Fortheexperiments,a field ofview of1548× 660 pixels is cho-sen.Eachpixelhas asize of198× 198μm2 with14 bitsof pixel depth.

Theentireexperimentalprocedurewascontrolledwitha work-station outside the setup room (closed with a lead sheet) guar-anteeinga safe workingcondition. Using the workstation, it was possibletotriggertheX-raysourceandreadoutthesignalsfrom the detector plate. Further details on the X-ray setup and the measurement technique can be found in Mudde et al. (2008),

Maurer et al. (2015), and Helmi et al. (2017). The X-ray images arerecordedat61Hzduringapproximately1minute, which cor-respondsto 3700 images.Afterwards, theseimagesare averaged. Allresults reported in thepresent studyare based on the time-averagedX-rayimages.Asthetypicalsheddingfrequencyis40Hz at

σ

=0.46,thisensuresthatthestatisticsarebasedonsufficient sheddingcycles.

3. Dataprocessing

3.1.Imageprocessing

The raw images acquired by the X-ray detector need several post-processingsteps (black linescorrection, background subtrac-tion, andimage adjustment) before they can be used to explain thecavitationdynamics.Allofthefollowingstepswereperformed using MatlabR2017a (The Mathworks Inc., Natick, USA) andthe processis depictedinFig.4. Dueto theorientation ofventuri in theexperimentalsetup,theimagesobtainedfromtheX-ray detec-torshowtheventuriinaverticalposition.TheX-rayimageswere rotatedby 90◦;therefore,thebulk flowisfromleft torightinall imagesshowninthepaper.

The detector plateisconstructed by a combinationofsmaller detectorelements. Due to this construction, multiple black lines appearontheobtainedimages,asshowninFig.4(a).Theseblack lines consist of a single pixel in either direction (vertical direc-tionandhorizontal direction),andthey do not contain anydata. Thesewerereplacedwithintensitiesbylinearinterpolationofthe pixelintensitiesoneithersideofthelines,asshowninFig.4(b).In theX-rayimages,thevaporphasehashighergrayscaleintensities, while the liquidphase has lower grayscale intensities. This hap-pensbecausethepresenceofvapor leadstolower attenuationof theX-raysalongitspathlength(explainedinSection4.2).A back-ground correction is performed for the X-ray images, for which background images withonly the liquid phase without flow are captured.In orderto improve the contrast,an image adjustment

Fig. 4. Time-averaged X-ray images of cavitating flow in the venturi: (a) raw time- averaged image obtained from the detector, (b) corrected image after removing black lines, and (c) the image obtained after background correction as well as ad- justed to improve contrast (vapor is light gray, liquid is black). In all the images, the bulk flow occurs from the left to right.

operationis performedon images.Thisprocessinvolves rescaling thegrayscaleintensitiesinordertohave1%ofthedatabeing satu-ratedathighintensitiesand1%ofthedatacoveringlowintensities (Fig.4(c)).Thisarbitraryscalinghasnoinfluenceonthe quantita-tivevoidfraction,asthisisbasedonaseparate calibration proce-dure(discussedinSection4.2).

Asthe verticalaxisisnotused (aswillbe discussedlater), its originisset arbitrarily.The originofthehorizontalaxis, coincid-ingwiththeaxial/streamwisedirection,issetatthethroatofthe

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S. Jahangir, E.C. Wagner and R.F. Mudde et al. / International Journal of Multiphase Flow 120 (2019) 103085 5

Fig. 5. Convergence study of the time-averaged X-ray images, using three points on the centerline. The relative change is less than 0.1% after 3700 images.

venturi. The axial location (X) is made dimensionless using the lengthofthemeasuredpartofthedivergingsection(L=9.3cm).

A convergence studywasconducted on theX-ray data ofthe cavitating flow,asshowninFig. 5.Thetermon they-axis (‘rela-tive change’) iscalculatedasfollows: threepointsalong the cen-terlineare chosen:X/L =0.11,0.33 and0.55, whichcoverregions containing cavitation. The averaged grayscale intensities ofthese pointsarecomputedfromthefirst50X-rayimages.Subsequently, anadditional50imagesareusedtocalculatethenewmean inten-sities. The difference betweenthenewandold mean,divided by the old mean isshown asa function ofthe amountof total im-ages used.The relativeerrorreducesto lessthan0.1% after3700 images.Hence,thesamplingtimeofone minuteallows obtaining sufficientdataforstatisticswithaminimumerrorfromthemean. 3.2. Computedtomography

CT, also known as computed tomography, makes use of computer-processed combinations of many X-ray measurements taken from different angles to produce cross-sectional images

Fig. 7. Validation of the diameters from CT slices using the nominal geometry. See text for details.

(‘slices’).TheprocessofCTinvolvesacollectionofprojectionsfrom severalangles ofthe X-ray intensity attenuated by the object of interestonthedetector.Thecollecteddata(‘sinogram’)isthen re-constructedutilizingalgorithms,suchasfilteredbackprojection.

IntheX-rayimagingsystemusedinthisstudyshowninFig.3, thedistance betweenthedetectorandthe sourceis much larger than the measuring area, andthe viewing angle isminimal. The difference between the path lengths measured at the maximum angleandparalleltothedetectoris0.1%oftheparallelbeampath. Therefore,the cavitationcloud is assumedto beprojected to the detectorbyparallelX-raybeams(Wangetal.,2018).This assump-tion is also validated by comparing the reconstructed geometry againstthenominalgeometry,asshowninFig.7(explainedinthe upcomingparagraph). Asthemeasurement sectionis axisymmet-ric, we assume axisymmetry of the time-averagedflow. Fig. 6(a) showsatime-averagedX-rayimage,thestartingpointforour anal-ysis. Thered lines indicatethe overallshape ofthe venturi.Note that wehave shiftedtheselines outward by afew pixels sothat theydonotobscurethedata.Forallupcomingfigures thisminor

Fig. 6. Schematic of post-processing procedure followed to obtain a cross-sectional CT slice. (a) Time-averaged X-ray image of the cavitating venturi at σ= 0.40 (vapor is light gray, liquid is black). (b) Sinogram created from an axial location (red line in (a)). (c) Cross-sectional CT image presented as side-view cut. See text for details on this procedure. (For interpretation of the references to colour in this figure legend, the reader is referred to the web version of this article.)

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Fig. 8. (a) Cross-sectional CT images at different axial positions showing growth of the cavitation cloud at σ = 0.40. The contrast in the images is adjusted individually for each slice for clarity. (b) Cross-section through the x-z plane, showing the presence of cavitation bubbles in the center of the liquid core downstream of the venturi.

Fig. 9. The pressure loss coefficient ( K ) as a function of the cavitation number for the experiments performed by Jahangir et al. (2018) (open markers) and the present experiments (asterisks).

Fig. 10. Profiles of the absolute intensities recorded on the X-ray detectors at one streamwise location: the venturi throat. The two cases considered are when the venturi contains solely air and solely water.

Fig. 11. The logarithm of the ratio of intensities ( IX

IR ) versus the diameters of the

calibration cylinders representing the actual line-integrated void fractions. The mea- sured grayscale intensity is based on an average of 3700 images.

Fig. 12. (a) Time-averaged X-ray image of the calibration cylinder (air is light gray and liquid is black). (b) Cross-sectional CT image presented as a side-view cut with

α= 0.995 ± 0.004. The red region indicates the presence of vapor (air in this case) and the blue region indicates the presence of liquid. (For interpretation of the ref- erences to colour in this figure legend, the reader is referred to the web version of this article.)

shiftwasusedforclarity. Aslice(verticalred lineinFig.6(a)) is extractedfromthetime-averagedimageandstacked360timesto construct a sinogram of 600× 360 pixels as shownin Fig. 6(b). Thissinogramrepresentstheprojectionsfrom360◦.Thisisa nec-essary intermediate step before CT reconstruction usingthe par-ticular software used here. Filtered back projection is applied to thesinogramusingtheASTRAToolboxv1.8(vanAarleetal.,2016). ThisisaflexibleCTreconstructionopensourcetoolboxwhichuses

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S. Jahangir, E.C. Wagner and R.F. Mudde et al. / International Journal of Multiphase Flow 120 (2019) 103085 7

Fig. 13. Video frames of bubbly shock development at σ= 0.40. The light gray regions indicate the presence of liquid and the dark gray areas indicate the presence of cavity (vapor). (a,b) A growing cavity can be seen (left side of sub-panels) with the previously shedded cavity (right side of sub-panels). (c) In the subsequent frame the cavity collapses and a pressure wave is emitted (P). (d) Cavity detachment can be observed when the pressure wave reaches the throat.

CPUandGPUbasedreconstructionalgorithmsfor2Dand3Ddata sets. In the present study, we use a CPU based implementation ofthefilteredback projection(FBP)algorithm for2D datasets.It takesthesourceanddetectordataasinputandreturnsthe recon-struction. Forthis study,justthe sinogram wasused asan input andreconstructedCTslicewasreturned(Fig.6(c)).The reconstruc-tion algorithmresembles theinverse operationof aforward pro-jection.Butinsteadofeachdetectorgettingthelineintegralofthe objectfunction,eachpointontheobjectdomainreceivesthevalue ofthedetectorpointwhereitprojectsto.So,inessence,the detec-tive functionis smearedout overtheobject domain.Thisisthen doneoverallprojectionanglessummingupthevaluesineach di-rection(vanAarleetal.,2016).

A common causeof errors when reconstructing X-ray CT im-ageareartifactswithintheimage.Conventionalsourcesofartifacts are beam hardening and abrupt changes in density. Beam hard-eningis themostcommonartifact found inX-rayCT reconstruc-tion. It causes theedges ofthe scanned measurement section to appear brighterthanthe center,even forhomogeneous materials (Ketcham andCarlson, 2001). This effectis caused by the differ-enceinabsorptioncoefficientsforvariouswavelengthswhenusing a non-monochromatic source. An efficient wayto decrease beam hardening(whichismoresevereinmetalsthanplastics)isfiltering low-energysoftX-rayswithmetalfilters.Forthesemeasurements, no beam hardening filtration was used primarily due to the ab-senceofmetalswhichwouldresultinapotentialreductioninthe image contrastimposed by extra filtration. The absence of beam hardeningisalsoconfirmedfromthecalibrationplot,explainedin

Section4.2.

Two different tests were performed to check the quality of reconstruction. A check on the diameters from reconstructed CT slicesacross14differentaxialpositionsofthefulllengthofempty venturi was performed. The results were compared to the nom-inal diameters, asshown inFig. 7. The diameters from CTslices matchedquitewelltothenominalgeometry,amaximumerrorof lessthan1.2%ofthelocaldiameterwasfound.Anothercheckwas basedonthedistributionofvoidfractions

α

.Therelativeerrorwas foundtobelessthan0.9%,aswillbediscussedinSection4.2.

After constructing a single slice, the process is repeated and multipledensityslicesoftheventuriperpendiculartothe

center-lineaxisarecreated.Fig.8(a)showsreconstructedslicesat differ-entaxial positions,showing growthofthe cavitationcloud. Most ofthevaporisattachedtothenozzlewallandpersistsuntilfour diametersdownstream ofthe throat.This isthe pointwhere the cavitydetaches duringthe periodic shedding, which is also con-firmedby thehigh-speedimages(Jahangiretal., 2018). After de-taching,thevaporcloud movestowardsthecenterofthe venturi andmixeswiththe liquidcore. Fig. 8(b) showsthe cross-section throughthex-zplane. Fig.8(b)isthecross-section,andthus dis-tinctfromtheX-rayimageofFig.7(a).Ascanbeseeninthefigure, cavitationbubblesarealsopresentintheliquidcore,downstream oftheventuri.

4. Results

WiththeventurispecifiedinSection 2,itispossibletoinitiate partial cavitation mechanisms such as the re-entrant jet mecha-nismandthebubblyshockmechanismatdifferentcavitation num-bers.Anoverviewofthesecavitationmechanismscanbefoundin

Jahangiretal.(2018).

4.1. Pressurelosscoefficient

The strength of cavitation is expressed using the cavitation number.Withanincreaseintheflowvelocity,thecavitation num-berdecreases,implyingmorecavitation.Withadecreasing cavita-tionnumber,theeffectivethroatdiameterisnarrowedbythe pres-enceofthegrowingcavity.Becauseofthenarrowedthroat diam-eterfor decreasingcavitation number,the pressure loss over the venturi will be higher. This is visible from measurement results, showninFig. 9.Here, thecavitation number isvaried by chang-ingtheflowvelocityatdifferentstaticpressures,andthepressure losscoefficient Kis reported.This impliesthat flow blockageis a functionofcavitation number. Forboththe shadowgraphy exper-imentsperformedby Jahangiretal.(2018) andthepresentX-ray experiments, it can be seen that all points collapse on one line. Theflowsfromthetwoexperimentsforthesamecavitation num-bersaretherefore assumedtobe equivalent, asthepressure loss coefficientsacrosstheventuri(K)aresimilarforbothcases.

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Fig. 14. (Bottom) Time-averaged X-ray image of an experiment in the bubbly shock regime. The light gray regions indicate the presence of vapor and the black regions indicate the presence of liquid. The cavitation number is σ = 0.40 ( u 0 = 13.7 m/s and p = 40 kPa). (a-f) Quantitative measurements of time-averaged void fractions at six

different locations along the venturi.

4.2.CTvoidfractioncalibration

Variousapproachesexisttoobtainquantitativevaluesofthe lo-calattenuation coefficient(or density,forsimplicity).Inourcase, weoptedforthefollowingapproach:imagesarerecordedand di-vided by a reference image (IR) for the case of only water. The

‘intensity’ that remains is proportional to the amount of vapor presentbetweensource anddetector,asthishasa lower attenu-ationthanwater.Usingthisreferencemethod,allattenuation out-sidethe region ofinterest (such asthenon-axisymmetricPMMA partsofthetestsection)cancelsout.Theimagesareprocessed us-ing theCT algorithm,which provides a three-dimensional recon-struction. Each voxel in this reconstruction contains information aboutthe local attenuation coefficient. As our approach isbased onrelativeX-rayimage intensities,there isanunknown constant linking voxelvalues and theactual localattenuation. This coeffi-cientisobtainedfromcalibrationexperiments.

First, intensities were measured by the X-ray detector when the venturi contained only air and only water. Densities of air (1.27kg/m3) andwater vapor2 (0.804kg/m3) are far smaller than the density of water (997kg/m3). Therefore, air is a suitable al-ternative forwater vapor because of the negligible difference in their mass densities and hence similar linear absorption coeffi-cients(Mitroglouetal.,2016;Baueretal.,2018).Forthecalibration withair,theventuriwasleftemptyanditwasfilledwithfiltered waterfortheothercase.Themaximumintensitywasrecordedas 12,580forair,anditwas9045forwateratthestreamwise plane of the throat,as shownin Fig. 10. Approximately 21% ofthe to-talcapacityofthe14-bitdetectorwasutilizedhere.However,this range increasesin the downstream direction withthe increasing

2 The reported value for water vapor is at standard conditions. In reality, the pres-

sure (and density) will be lower, but this difference is negligible compared to the difference between water vapor and water.

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S. Jahangir, E.C. Wagner and R.F. Mudde et al. / International Journal of Multiphase Flow 120 (2019) 103085 9

Fig. 15. Time-averaged mean and maximum void fractions of vapor as a function of position for σ= 0.40.

Fig. 16. The total area covered by vapor ( A V ) and liquid ( A L ) as a function of posi-

tion for σ = 0.40. Also shown is the local cross-sectional area of the venturi geom- etry.

diameteroftheventuricross-section.Thewiggles inthe absolute intensities(Fig.10(inset))areduetodifferentsensitivitiesof mul-tiplepixels intheprimarydetector(describedinSection3.1) and notrandomnoise.

For purely monochromatic X-rays, this two-point calibration wouldhavebeensufficienttodetermineallpossiblevaluesin be-tweenvapor/airandwater.ToensureaccurateresultsforourX-ray source,additionalcalibrationexperimentswereperformedwith in-creasingvolumefractions inbetweenthe twoextremes.An addi-tional reason is that the expected void fractions are low,so we would be close to one of the calibration points, making the re-sultverysensitivetocalibrationerrors.Toperformtheseadditional calibrationexperiments,emptycalibrationcylinders(air-filled plas-ticcylinders)offourdifferentdiametersandnegligiblewall thick-nesses were insertedinto theventuri, whichwasfilled with wa-ter. The calibration cylinderswere alignedwiththe axis of sym-metry ofthe venturi.The diametersof calibrationcylinders were measuredwithanaccuracyof ± 0.5mm.Calibrationwasthen per-formed at multiple streamwise locations by recording the mean intensity along the centerline of the cylinders. As the diameters ofthecalibrationcylinders wereknown,theintensityatthe cen-ter ofthe cylinder is related to the line-integrated void fraction. InFig.11,thecalibrationrelationisshownforsevenX/Llocations selected fromthe full length of the venturi.The diameter ofthe venturi increases with increasing X/L, which corresponds to the different attenuation of X-rays dueto the presence of more

wa-terandlessPMMA.However,bydividingtherecordedintensityby thereferenceintensity thiseffectof differentattenuation cancels out.AlinearfitthroughmeancanbeseenintheFig.11.The stan-darderrorfromthemeanforthemeasuredintensitiesforthe var-iouscalibrationcylinderswasfoundtobelessthan3.65%,whichis consideredacceptable.Therelationshipobtainedbetweenthe log-arithm3 of the intensities in the X-ray images and the diameter

ofcalibrationcylinders(knownvoidfraction)isusedtodetermine thecalibrationconstant,whichisthenusedtocalculatethevapor distribution on the reconstructed CT slices(explained inthe up-comingparagraph).

Tousethesecalibrationresultsofline-integratedquantitiesfor ourCTresults,aprocedurewasfollowedthatisacommonmethod inthe X-ray community(selectively Mitroglou etal., 2016;Duke et al., 2015; Bauer et al., 2018). The images from the CT recon-structionprovide3Dinformation.Tofindthevoidfractionforeach voxel,wecollapsethedatabackto2DX-rayimages,i.e.projecting thetomographicreconstructionontoa2D plane.Wecanthen as-signan integratedvoid fractionto each projected intensityusing thecalibrationcurve.Thisintegratedvoidfractionissubsequently redistributed over the constructed slice, so that the sum of the voxelvaluesmatchestheprojectedvoidfraction.

Fig.12 (a) showsthetime-averagedX-ray intensitydatafora calibrationcylinder. This panel is before tomographic reconstruc-tioni.e.a projection along the linebetweensource anddetector.

Fig.12(b)showsthereconstructedCTsliceatanaxialposition(red line in Fig. 12(a)) with the void fractions. A very homogeneous distribution of air can be seen. Here,

α

= 0.995± 0.004, which showsamaximumerrorofapproximately0.9%withrespecttoreal voidfraction,whichisconsidered acceptable.Thiserroris associ-atedwithvariousfacts,themostnotablebeing:thereconstruction method,which is an approximate approach, andthe variation of noiseintheX-rayimages.Thediameterofthecylindermeasured fromtheCTslicealsocompares verywelltotheknowndiameter ofthecylinderwithanerroroflessthan1%.

4.3.Cross-sectionaldistributionofvoidfraction

This section presents the quantitative void fraction measure-ments for the bubbly shock mechanism and the re-entrant jet mechanism.Theresultsshownareamixofqualitativehigh-speed shadowgraphy imagesandquantitative time-averagedX-ray mea-surements.Their combination willassist ininterpreting the flow behaviorintheventuri.

High-speed shadowgraphy was performed in a prior study, which alsoprovides all relevant technicaldetails (Jahangir etal., 2018). Abright, uniformilluminationsource isplaced behindthe venturiandaCMOScameraisusedtocaptureimages.Vapor bub-bleswill block light andthus appearasdarkspots inthe image. Thisway the presence andposition of vapor cavities can be de-termined.Aframerateof9000Hzisusedincombinationwithan exposuretimeof1/9000Hz.

InFig.13,videoframesofthebubblyshockmechanismare pre-sented.Theflow directionis fromleftto right. Thelight gray re-gionsindicatethepresenceofliquidandthedarkgrayareas indi-catethepresenceofcavity(vapor).Acasewithcavitationnumber of

σ

=0.40(u0=13.7m/sandp=40kPa)isshown.InFig.13(a) and(b),agrowingcavitycanbeseen(leftsideofsub-panels)with the previously shedded cavity (right side of sub-panels). In the subsequentframe,thecavitycollapsesandemitsapressurewave. When the pressure wave reaches the venturi throat, the cavity

3 As the intensity decays exponentially in a given medium (cf. the Lamber-Beer

law), taking the logarithm of the intensity leads to a linear relation between atten- uation (and intensity) and the void fraction.

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Fig. 17. Video frames of re-entrant jet development at σ = 1. In (a) and (b), cavity development can be seen and the re-entrant jet starts to develop. The jet front can be recognized by the chaotic interface, which can be seen by the arrow. The propagation of the jet front towards the venturi throat can be seen in (c). In the end, cavity detachment is caused by the re-entrant jet as can be observed in (d).

Fig. 18. (Bottom) Time-averaged X-ray image of an experiment in the re-entrant jet regime. The light gray regions indicate the presence of vapor and the black regions indicate the presence of liquid. For this case σ= 1 (corresponding to: u 0 = 13.5 m/s and p = 90 kPa). (a-f) Quantitative measurements of time-averaged void fractions at six

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S. Jahangir, E.C. Wagner and R.F. Mudde et al. / International Journal of Multiphase Flow 120 (2019) 103085 11

detaches, asshowninFig. 13(d).Thisis thestart ofthe next cy-cleoftheperiodicsheddingprocess.

Thecorrespondingvoidfractiondistributionslicesforthe bub-blyshockmechanismareshowninFig.14(a)-(f).TheCTslicesare reconstructedattheaxialpositionsindicatedinthetime-averaged X-rayimage.Theflowdirectionisfromlefttoright.Thelightgray regionsindicatethepresenceofacavity(vapor)andtheblack ar-eas indicatethe presence ofliquidin the X-rayimage, whilethe red regions show cavity and blue regions show the presence of liquidintheCTslices.Quantitativemeasures forthe totalsurface area ofvapor andliquidAV andAL arealso obtainedforeachCT

slice. Thetotal surfacearea ofvapor foreach CTsliceisgivenby AV =

α(

y,z

)

dydz ≈ [

α

(y, z)]dydz,where dyanddz are the

physicaldimensionsofa reconstructedvoxel.AL followsfromthe

nominal localcross-sectional area ofthe venturi, minus the area coveredbyvapor.

A core of liquid can be seen in a short distance just down-stream of the venturi throat with a concentrated ring of cavita-tion around it (Fig. 14(a)). This thin film of cavitation has the maximum void fraction of

α

max = 0.86. The center of annulus consists of pure liquid without any cavitation (threshold of liq-uid being set at

α

= 0.016, explained in Section 4.2). Further downstreamoftheventurithroat,thevaporfilmstartstobecome morelikeacloudasitsthicknessincreases,asshowninFig.14(b) and (c). A decrease in the maximum void fraction can be seen; however, the average void fraction is similar in both CT slices (Fig.15).

The cavitation bubbles are present in the liquid core further downstream, hinting at the appearance of a thick cloud of va-por, as shown in Fig. 14(d) and (e). A diffused interface be-tween the liquidand vapor can be alsobe seen. The vapor film which was previously attached to the circumferential wall can now be seen turning into a cloud and detaching from the wall (Fig. 14(e)). The value of

α

max steadily decreases with increas-ing X/L. The cavitation cloud becomes thicker as the liquid core decreases. Note that these are time-averagedvoid fractions. This is relevant,in particular furtherdownstream, asthe cavitation is notpresentateach instanceforagivenlocation:italternates be-tween liquidandvapor (Fig.13). Theinstantaneousvoidfractions will likely be much higherthan the time-averageddatareported here.

In Fig.14(f),it canbe seen that onlycloud cavitation appears attheexitoftheventuri.Themaximumvoidfractions(

α

max),the meanvoidfractions(

α

mean)andthetotalsurfaceareas(AV andAL)

are shown in Figs. 15 and16. The value of AV rapidly increases

withtheincreaseinaxiallocationuntilX/L ≈ 0.65.Here,a maxi-mumofAV isfoundof134.7mm2.Withafurtherincrease inX/L,

aslightdecreaseinAV canbeseen.AtX/L=0.9,thevalueofAV is

129mm2,vaporandliquidarethoroughlymixedwithanaverage voidfractionofabout12%anda maximumvoidfractionofabout 16%.

Weshouldnotignorethefactthatsomepartofthesevoid frac-tions may be attributed to non-condensable gas, instead of just watervapor.Thediffusionrateintothecavityisrelatedtothe dis-solved gascontent,the localcavitypressure,andtheflow within andaroundthecavity(Leeetal.,2016).However,tominimizethis effect, the measurements were performed at relatively low dis-solvedgascontent(describedinSection2.2).

A second case is selected, but thistime in the re-entrant jet dominant regime. The video frames for

σ

= 1 (u0 = 13.5m/s and p = 90kPa) are shown in Fig. 17. One full cycle of the re-entrant jet mechanism and shedding can be observed. The re-entrant jet developswiththe growing cavity(Fig. 17(a) and(b)). There-entrantjetfrontcanberecognizedbythechaoticinterface, whichcanbeseenbythearrow.Thenthejetfrontstartsto prop-agateinthedirectionoftheventurithroat,asshowninFig.17(c).

Fig. 19. Time-averaged mean and maximum void fractions of vapor as a function of position for σ= 1.

The re-entrant jet reaches the throat and the entire cavity de-tachesfromthethroat(Fig.17(d)).Thismarksthestartofthenext cycle.

The corresponding void fraction distribution slices for the re-entrantjetmechanismareshowninFig.18(a)-(f).Notethe differ-enceincolorscalecomparedtoFig.14.TheCTslicesaresimilarly reconstructedattheaxialpositionsindicatedinthetime-averaged X-ray image. It is evident from the X-ray image that the cavity lengthissmallerascomparedtothebubblyshockcase.Therefore, theaxial locations forthe CT reconstruction are selected accord-ingly.

OnethingthatisclearlyvisiblewithintheCTslicesisthatthe

α

valuesforthisregimearesmallerthanthoseinthebubblyshock governedregime. Onceagain thecoreconsistingofliquid canbe seen in a short distance just downstream of the venturi throat (Fig. 18(a)).The cavitation ring atthe circumferential wall isstill present;however, its void fraction is lesspronounced, compared toFig. 14.Here, themaximum voidfractionis 45%, whichis ap-proximately half the void fraction ofthe bubbly shock governed case.Itcanalsobeseenthattheextentofthecavitationstructure is slightlygrowing fromFig. 18(a) to (c)but its shape is overall conserved.Adecreaseinthe

α

maxcanbeseendownstreamofthe venturithroat (Fig. 18(b)-(d)).However, the average voidfraction doesnot decrease within thesethree CT slices. InFig. 18(e) and (f),thecavitationringchangesintocloudcavitationbeforeit van-ishes.Thisprovesoncemorethecapabilitiesofthismeasurement method.

Themaximumandmeanvoidfractionsandthetotalsurface ar-easareshowninFigs.19and20.AV isthesameasthedifference

betweenAL andthenominallocalcross-sectionarea,representing

the flow blockage caused by cavitation. It is clear that the flow blockagecausedby thebubblyshockregime (Fig.16)ismore sig-nificantcomparedtothere-entrantjetregime(Fig.20).Thisagrees withthe observed difference in pressure drop,see the values of Kin the insetof Fig. 9.An increase inAV can be seen until X/L

≈ 0.3.Here, AV = 33.7mm2. The maximumvalue ofAV is found

tobe approximately4times smallerthanthe maximumvalue of AV in thebubbly shockcase. This is a major newinsight, asthe

high-speed shadowgraphy showed fairly similar (time-averaged) data.The value ofAV startstodecrease sharplyas we move

fur-ther downstream andreaches 17.8mm2 at X/L = 0.45. Here, the maximum void fraction is found to be 6% (Fig. 18(f)), which is quite low as compared to the bubbly shock case. It also hints atthe presenceof alower void fractiondownstream ofthe ven-turiinthere-entrantjetregimeascomparedtothebubblyshock regime.

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Fig. 20. The total area covered by vapor ( A V ) and liquid ( A L ) as a function of posi-

tion for σ = 1. Also shown is the local cross-sectional area of the venturi geometry.

5. Conclusionsandoutlook

In thisstudy,the phenomenonof cavitationwasexamined by CT measurements of the flow through a venturi. Time-averaged voidfractionswereobtainedafteradetailedimagecorrectionand calibrationprocedure. More information about the cavitation de-velopmentisextractedusingthecross-sectionalCTmeasurements ascomparedtothehigh-speedshadowgraphy.Wecannow quan-tifytheradial geometricfeatures ofthiscomplextwo-phase flow. Thevoidfractiondownstream ofthe venturiinthe bubblyshock mechanismis found tobe morethan twice compared to the re-entrantjetmechanism.Moreover,thevaporphasemixeswiththe liquidphasedownstreamoftheventuri,resultingincloud-like cav-itation.Thisdatawillbe essentialtovalidateourassumptions re-gardingthe physical mechanisms.Furthermore, itwill be helpful forthevalidationofnumericalstudies.

UsingtheCTreconstruction,weareabletoexploretheinternal structuresofthecavitatingflowandtoquantifythevoidfractions. The combination of high-speed shadowgraphy data and CT data givesunprecedentedinsightintothiscomplexmultiphaseflow. De-spitethenewinsightthatthisapproachgenerated,therestillisa majorlimitation:thecurrentstudywasperformedusingthe time-averaged X-raymeasurements; hence,further studies are needed toinvestigatethetransientbehaviorofthevaporcloud.These in-vestigationsareplannedandwillbeperformedusingphase-locked X-raymeasurements.

Acknowledgments

SJ has received funding from Marie Curie Horizon 2020 Re-searchandInnovationprogrammeGrant642536‘CaFE’.CPhas re-ceivedfundingfromERCConsolidatorGrant725183‘OpaqueFlows’. The authors would like to thank Willian Hogendoorn (TU Delft) for providing access to the high-speed shadowgraphy data. The authorsfurtherthankSören Schenke andAmitoshDash (bothTU Delft)formanyfruitfuldiscussions.

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