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C2CA Concrete Recycling Process

From Development To Demonstration

Lotfi, Somi

DOI

10.4233/uuid:70505a1f-c0d7-47c7-ab62-8d487761c021

Publication date

2016

Document Version

Final published version

Citation (APA)

Lotfi, S. (2016). C2CA Concrete Recycling Process: From Development To Demonstration.

https://doi.org/10.4233/uuid:70505a1f-c0d7-47c7-ab62-8d487761c021

Important note

To cite this publication, please use the final published version (if applicable).

Please check the document version above.

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This work is downloaded from Delft University of Technology.

(2)

C2CA Concrete Recycling Process

From Development To Demonstration

Despite the urgency of creating a sustainable solution for end of life concrete waste,

there has not been a large driving force for recycling it into prime grade materials. This

low motivation has a root in existing cultural, environmental, political and economic

constraints. For concrete to concrete recycling most of the time a lack of economic

bene-fits puts obstacles for the technology and the business model. This indicates that currently

the market for concrete recycling may not be large enough and needs innovations to

cre-ate more attractive products. The C2CA concrete to concrete recycling process delivers

such innovations.

The present research work investigated and developed the C2CA concrete recycling

process for recycling of end of life concrete to both recycled aggregates, with a quality

equivalent to natural aggregates and a hardened cement rich stream for low-CO

2

cement

production and other binder products.

Somayeh Lotfi

C2CA Concr

ete R

ecy

cling P

rocess

From D

ev

elopment

To D

emonstration

Somay

eh Lotf

i

Delft University of Technology

(3)
(4)
(5)
(6)

C2CA Concrete Recycling Process:

From Development To Demonstration

Proefschrift

ter verkrijging van de graad van doctor

aan de Technische Universiteit Delft,

op gezag van de Rector Magnificus prof.ir. K.C.A.M. Luyben;

voorzitter van het College voor Promoties,

in het openbaar te verdedigen op

maandag 21 november 2016 om 10:00 uur

door

Somayeh LOTFI

Master of Science in Materials Engineering,

University of Science and Research, Tehran

(7)

Copyright © 2016 by Somayeh Lotfi

Dit proefschrift is goedgekeurd door de:

Promotor: Prof. dr. P.C. Rem

Promotor: Prof. dr. J. Deja

Samenstelling promotiecommissie:

Rector Magnificus,

voorzitter

Prof. dr. P.C. Rem,

Technische Universiteit Delft, promotor

Prof. dr. J. Deja,

AGH University Poland, promotor

Onafhankelijke leden:

Prof. dr. ir. E. Schlangen,

Technische Universiteit Delft

Prof. dr. E. M. van Bueren,

Technische Universiteit Delft

Prof. dr. A. Bonoli,

University of Bologna, Italy

Prof. dr. G. Thenoux,

Pontifical Catholic University of Chile

Dr. ir. S. A.A.M. Fennis,

Rijkwaterstaat

Printed in the Netherlands by Optima First Printing, 2016

ISBN 978-94-6169-983-1

Copyright © 2016 by Somayeh Lotfi Email: lotfi.tud@gmail.com

All right reserved. No part of this publication may be reproduced, stored in a retrieval system of any nature, or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording or otherwise, without the prior written permission of the author.

This research was funded by the European Commission in the framework of the FP7 Collaborative project “Advanced Technologies for the Production of Cement and Clean Aggregates from Construction and Demolition Waste (C2CA)”, Grant Agreement No.265189. Also, this research has received funding from the European Commission under the framework of the Horizon 2020 research and innovation program “HISER project”, Grant agreement No 642085.

Dit proefschrift is goedgekeurd door de: Promotor: Prof. dr. P.C. Rem

Promotor: Prof. dr. J. Deja Samenstelling promotiecommissie:

Rector Magnificus, voorzitter

Prof. dr. P.C. Rem, Technische Universiteit Delft, promotor Prof. dr. J. Deja, AGH University Poland, promotor Onafhankelijke leden:

Prof. dr. ir. E. Schlangen, Technische Universiteit Delft Prof. dr. E. M. van Bueren, Technische Universiteit Delft Prof. dr. A. Bonoli, University of Bologna, Italy Prof. dr. G. Thenoux, Pontifical Catholic University of Chile Dr. ir. S. A.A.M. Fennis, Rijkwaterstaat

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(9)
(10)
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(12)

iii

(13)
(14)

Introduction

(15)

(16)

Introduction 3

(17)

(18)

Introduction 5

(19)

(20)

Introduction 7

Regulations & Standards Economy Environment & Ecology Barriers for Concrete to Concrete Recycling Cultural Considerations Technology

(21)

1.3.1 Regulations, standards and economy

(22)

Introduction 9

1.3.2 Technology and market barriers

(23)

1.3.3 Environmental and cultural aspects

(24)

Introduction 11

(25)

(26)

Introduction 13

1.4.1 Contribution of C2CA in CO

2

reduction

(27)

1.4.3 C2CA business model in brief

(28)

Introduction 15

(29)

(30)

Introduction 17

(31)

(32)

Introduction 19

(33)
(34)
(35)
(36)

Mechanical Recycling of EOL

Concrete into High-Grade

Aggregates

(37)
(38)

Mechanical Recycling of EOL Concrete into High-Grade Aggregates 25

(39)

(40)

Mechanical Recycling of EOL Concrete into High-Grade Aggregates 27

(41)

2.4.1 EOL concrete

(42)

Mechanical Recycling of EOL Concrete into High-Grade Aggregates 29

(43)

(44)

Mechanical Recycling of EOL Concrete into High-Grade Aggregates 31

(45)

Mill Input

Mill

Screen

ADR

1-4 mm

Fine

0-1 mm

Fine

4-16 mm

Coarse

+16 mm

Coarse

-16 mm

Coarse

0- 40 mm

Crushed concrete

(46)

Mechanical Recycling of EOL Concrete into High-Grade Aggregates 33

2.5.1 Performance of ADR

2.5.2 Properties of RA and performance of RAC

(47)

(48)

Mechanical Recycling of EOL Concrete into High-Grade Aggregates 35

(49)

(50)

Mechanical Recycling of EOL Concrete into High-Grade Aggregates 37

(51)

°

°

°

°

°

(52)
(53)
(54)

Performance of RAC based on the

type of cement and RA substitution

(55)
(56)

Performance of RAC based on type of cement and RA substitution 43

(57)

(58)

Performance of RAC based on type of cement and RA substitution 45

3.3.2 Concrete production

(59)
(60)

Performance of RAC based on type of cement and RA substitution 47

(61)
(62)

Performance of RAC based on type of cement and RA substitution 49

3.3.3 Performed Experiments

(63)

3.4.1 ADR input and outputs

(64)

Performance of RAC based on type of cement and RA substitution 51

3.4.2 Properties of RA

(65)

(66)

Performance of RAC based on type of cement and RA substitution 53

(67)

3.4.4 Properties of hardened concrete

3.4.4.1

Compressive Strength

(68)

Performance of RAC based on type of cement and RA substitution 55

(69)

3.4.4.3

Oxygen Permeability

(70)

Performance of RAC based on type of cement and RA substitution 57

(71)

(72)

Performance of RAC based on type of cement and RA substitution 59

(73)

(74)

Performance of RAC based on type of cement and RA substitution 61

3.4.4.6

Rapid chloride migration

(75)

3.4.4.7

Two electrodes method (TEM)

(76)

Performance of RAC based on type of cement and RA substitution 63

3.4.4.8

Abrasion resistance

(77)

(78)

Performance of RAC based on type of cement and RA substitution 65

3.4.4.9

Summary of the durability impact

(79)
(80)
(81)
(82)

Effects of shear-compression on

hardened cement recovery

(83)
(84)

Effects of shear-compression on hardened cement recovery 71

4.3.1 Parent concrete and primary crushing

4.3.2 Set-up for applying shear and compression force

(85)

(86)

Effects of shear-compression on hardened cement recovery 73

4.3.3 Experimental design

j i j i j i i i ii i i i

x

x

2

x

x

0

β

i

β

ij

β

ij

(87)

4.3.4 Analysis of the experimental samples

4.4.1 Interpretation of the regression analysis

(88)

Effects of shear-compression on hardened cement recovery 75

(89)

(90)

Effects of shear-compression on hardened cement recovery 77

4.4.2 Interpretation of surface and contour plots

(91)
(92)

Effects of shear-compression on hardened cement recovery 79

4.4.3 Main effect plot

4.4.4 Normal probability plot

(93)
(94)

Effects of shear-compression on hardened cement recovery 81

(95)
(96)

The relation between input

variables and output quality in the

C2CA process

(97)
(98)
(99)

5.3.1 Parent Concrete

(100)

The relation between input variables and output quality in the C2CA process 87

(101)
(102)

The relation between input variables and output quality in the C2CA process 89

(103)
(104)

The relation between input variables and output quality in the C2CA process 91

5.3.2 Concrete Recycling Procedure

(105)

(106)

The relation between input variables and output quality in the C2CA process 93

5.3.3 Experimental Design

(107)

Parent concrete

SCM setting (degree of milling)

Coding of ADR input samples

Coding of corresponding produced RA Corre-sponding produced RAC Shear: Duration (min) Compression: Force (KN) Coding

PC1 - - no milling PC1-No Milling RA-PC1-

No Milling - PC1 7.12 6.30 HS-LC PC1-HS-LC RA-PC1-HS-LC - PC1 5.00 18.60 MS-MC PC1-MS-MC RA-PC1-MS-MC RAC1 PC2 7.12 6.30 HS-LC PC2-HS-LC RA-PC2-HS-LC - PC2 5.00 18.60 MS-MC PC2-MS-MC RA-PC2-MS-MC RAC2 PC2 5.00 30.90 MS-HC PC2-MS-HC RA-PC2-MS-HC - PC3 7.12 6.30 HS-LC PC3-HS-LC RA-PC3-HS-LC RAC3 and RAC5 PC3 5.00 18.60 MS-MC PC3-MS-MC RA-PC3-MS-MC RAC4

(108)

The relation between input variables and output quality in the C2CA process 95

5.3.4 RAC production

(109)

(110)

The relation between input variables and output quality in the C2CA process 97

5.4.1 ADR Performance

5.4.2 Properties of RA

(111)

(112)

The relation between input variables and output quality in the C2CA process 99

(113)

Properties

Moisture content[wt.%] 5.7 5.8 5.8 5.6 5.5 5.7 4.6 4.1

Density of grains[kg/m3] 2626 2628 2629 2626 2629 2611 2626 2625

Density of grains dried

in an oven[kg/m3] 2265 2256 2249 2266 2290 2262 2330 2358 Density of grains

satu-rated and surface-dried

[kg/m3] 2402 2397 2393 2403 2419 2395 2442 2460 Water absorption[ wt.%] 6.06 6.26 6.41 6.04 5.62 5.89 4.82 4.30 Freezing-thawing weight loss (8-16mm) [wt.%] 1.06 0.75 0.91 2.14 3.53 2.32 1.3 1.22 Freezing-thawing weight loss (4-8mm) [wt.%] 1.86 1.69 1.96 5.40 6.01 7.43 2.54 2.35 Index of aggregate

crushing for non-fractioned sample [wt.%] 14.42 14.6 14.43 13.74 13.79 13.16 13.21 13.98 Index of aggregate crushing for 4-8 mm fraction[wt.%] 13.49 13.84 13.38 14.02 13.32 13.31 12.74 13.04 Index of aggregate crushing for 8-16 mm fraction[wt.%] 15.65 15.88 15.86 13.31 14.37 12.95 13.93 13.65 Fines content[wt.%] (wet analysis) 0.63 0.23 0.37 0.29 0.31 0.43 0.40 0.34 R A -P C 1-N o m illi ng RA -P C 1-HS -LC RA -P C 1-MS -MC RA -P C 2-HS - LC LC RA -P C 2-MS -MC LC R A -P C 2-MS -H C LC RA -P C 3-HS -L C RA -P C 3-MS - MC

(114)

The relation between input variables and output quality in the C2CA process 101

(115)

5.5.1 Fresh and hardened concrete mechanical properties

(116)

The relation between input variables and output quality in the C2CA process 103

(117)

(118)

The relation between input variables and output quality in the C2CA process 105

(119)

(120)

The relation between input variables and output quality in the C2CA process 107

5.5.2 Durability properties of RAC

(121)

(122)

The relation between input variables and output quality in the C2CA process 109

(123)

5.5.3 Discussion of the variables impacts

(124)

The relation between input variables and output quality in the C2CA process 111

(125)
(126)

The relation between input variables and output quality in the C2CA process 113

(127)
(128)
(129)
(130)

Assessment of contaminants level

and removal from RA

(131)
(132)

Assessment of contaminants level and removal from RA 119

6.2.1 End of life building (case study in Groningen)

(133)

(134)

Assessment of contaminants level and removal from RA 121 Legend Case study in Groningen Smart Dismantling & Selective Demolition Hazardous (asbestos,...),Contaminants (gypsum, tapestry,…),Equipment (heating, airco,…) Large recyclables (steel, wood,

brick) Rebar steel ADR processing Processing 4-16 mm contaminants clean RA Sensor sorting Wind sifting +16 mm Contaminants +16 mm contaminants clean RA Crushing Attrition Milling & Screening On 16mm +16 mm Fraction -16 mm Fraction 0-4mm fraction 0.250-4 mm clean RS 0-0.250 mm Ca rich fraction

Removing external materials or contaminants

Clean products Process

Quality control

Products mixed with contaminants

(135)

(136)

Assessment of contaminants level and removal from RA 123

(137)

6.2.5 Screening and ADR processing

(138)
(139)
(140)

Assessment of contaminants level and removal from RA 127

6.2.6 NIR sensor sorting and wind sifting to remove contaminants

from +16mm RA

(141)

(142)

Assessment of contaminants level and removal from RA 129

(143)

(144)

Assessment of contaminants level and removal from RA 131

-

-

-

-

(145)
(146)

Recycling of ADR fines into

hard-ened cement and clean sand

(HAS technology)

(147)
(148)

Recycling of ADR fines into hardened cement and clean sand 135

7.2.1 Current research background

(149)

(150)

Recycling of ADR fines into hardened cement and clean sand 137

(151)

7.3.2 AF Recycling set-up

(152)

Recycling of ADR fines into hardened cement and clean sand 139

(153)

7.3.3 Experimental Design

7.4.1 Heating-Air classification System (HAS) Performance

(154)

Recycling of ADR fines into hardened cement and clean sand 141

Legend

ADR Fines (AF) (HAS input) Heating Air classification system (HAS) (Temperature is varied from 105°C to750°C ) Finer Fraction(FF) And contaminants 0-0.250 mm Coarser Fraction (CF) 0.250-4mm Coarser Fraction (CF) 0.250-4mm Finer Fraction(FF) 0-0.250 mm Screen Ball Mill (BM) (Milling time is varied

from 0 to 300 seconds) Cement Kiln or other applications Pre-cast concrete Production

Materials Process Application ADR

Recycled coarse aggregate

(155)

(156)

Recycling of ADR fines into hardened cement and clean sand 143

(157)

(158)

Recycling of ADR fines into hardened cement and clean sand 145

(159)
(160)

Recycling of ADR fines into hardened cement and clean sand 147

(161)

(162)

Recycling of ADR fines into hardened cement and clean sand 149

(163)

7.4.3 Properties of the recycled fractions

(164)

Recycling of ADR fines into hardened cement and clean sand 151

α

α

α

α

(165)

(166)

Recycling of ADR fines into hardened cement and clean sand 153

(167)
(168)

Recycling of ADR fines into hardened cement and clean sand 155

(169)
(170)
(171)
(172)

Summary & Follow-up research

(173)
(174)

Summary 161

(175)
(176)
(177)
(178)

Summary 165

(179)
(180)

Samenvatting 167

(181)
(182)
(183)
(184)

Samenvatting 171

(185)
(186)
(187)
(188)
(189)

C2CA Concrete Recycling Process

From Development To Demonstration

low motivation has a root in existing cultural, environmental, political and economic

constraints. For concrete to concrete recycling most of the time a lack of economic

bene-fits puts obstacles for the technology and the business model. This indicates that currently

the market for concrete recycling may not be large enough and needs innovations to

cre-ate more attractive products. The C2CA concrete to concrete recycling process delivers

such innovations.

The present research work investigated and developed the C2CA concrete recycling

process for recycling of end of life concrete to both recycled aggregates, with a quality

equivalent to natural aggregates and a hardened cement rich stream for low-CO

2

cement

production and other binder products.

Somayeh Lotfi

ete R

ecy

cling P

rocess

From D

ev

elopment

To D

emonstration

Somay

eh Lotf

i

Delft University of Technology

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